IN2014CN04151A - - Google Patents

Info

Publication number
IN2014CN04151A
IN2014CN04151A IN4151CHN2014A IN2014CN04151A IN 2014CN04151 A IN2014CN04151 A IN 2014CN04151A IN 4151CHN2014 A IN4151CHN2014 A IN 4151CHN2014A IN 2014CN04151 A IN2014CN04151 A IN 2014CN04151A
Authority
IN
India
Prior art keywords
alkylene glycol
dialkyl carbonate
carbonate
material flow
alkylene
Prior art date
Application number
Inventor
Andrea Schmidt
Michael Bock
Roderich Röttger
Robert Baumann
Axel Franzke
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of IN2014CN04151A publication Critical patent/IN2014CN04151A/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/141Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/36Azeotropic distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/86Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C68/00Preparation of esters of carbonic or haloformic acids
    • C07C68/06Preparation of esters of carbonic or haloformic acids from organic carbonates
    • C07C68/065Preparation of esters of carbonic or haloformic acids from organic carbonates from alkylene carbonates
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C68/00Preparation of esters of carbonic or haloformic acids
    • C07C68/08Purification; Separation; Stabilisation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The invention relates to a method for obtaining a dialkyl carbonate and an alkylene glycol from a material flow containing dialkyl carbonate alkylene carbonate alkylene glycol and alcohol said method having the following steps: (a) separating a material flow (5) containing dialkyl carbonate and alkylene glycol in the form of a heteroazeotrope from the material flow containing dialkyl carbonate alkylene carbonate alkylene glycol and alcohol in a distillative manner in a first distillation stage (1) and (b) separating the material flow (5) containing dialkyl carbonate and alkylene glycol in the form of a heteroazeotrope into a first raw product flow (27) which substantially contains dialkyl carbonate and a second raw product flow (29) which substantially contains alkylene glycol in a device for the purpose of a phase separation (25).
IN4151CHN2014 2011-12-05 2012-12-05 IN2014CN04151A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP11191894 2011-12-05
PCT/EP2012/074478 WO2013083618A1 (en) 2011-12-05 2012-12-05 Method for obtaining a dialkyl carbonate and an alkylene glycol

Publications (1)

Publication Number Publication Date
IN2014CN04151A true IN2014CN04151A (en) 2015-07-17

Family

ID=47351616

Family Applications (1)

Application Number Title Priority Date Filing Date
IN4151CHN2014 IN2014CN04151A (en) 2011-12-05 2012-12-05

Country Status (7)

Country Link
EP (1) EP2788315A1 (en)
JP (1) JP2015504855A (en)
KR (1) KR20140113931A (en)
CN (1) CN104203899A (en)
BR (1) BR112014013557A2 (en)
IN (1) IN2014CN04151A (en)
WO (1) WO2013083618A1 (en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104220405B (en) * 2012-04-04 2016-08-17 旭硝子株式会社 Glycol and the separation method of dibutyl carbonate, purification process and manufacture method
WO2017071909A1 (en) 2015-10-28 2017-05-04 Carebay Europe Ltd Medicament container holder
US10399004B2 (en) 2016-09-08 2019-09-03 Eastman Chemical Company Thermally integrated distillation systems and processes using the same
CN108440297A (en) * 2017-03-23 2018-08-24 秦燕雯 A kind of device energy-saving for carbonate device
EP4038046A1 (en) * 2019-10-03 2022-08-10 Shell Internationale Research Maatschappij B.V. Process for preparing dialkyl carbonate and alkanediol
EP3831805A1 (en) * 2019-12-06 2021-06-09 Shell Internationale Research Maatschappij B.V. Process for the preparation of a dialkyl carbonate and an alkanediol
WO2021110627A1 (en) * 2019-12-06 2021-06-10 Shell Internationale Research Maatschappij B.V. Process for removing an ether alkanol impurity from an organic carbonate stream
CN115594585B (en) * 2022-12-13 2023-04-07 江苏华盛锂电材料股份有限公司 Method for synthesizing and purifying methyl trifluoroethyl carbonate in one step

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3642858A (en) * 1969-02-12 1972-02-15 Dow Chemical Co Carbonate synthesis from alkylene carbonates
US5489703A (en) 1995-05-19 1996-02-06 Amoco Corporation Reaction extraction of alkyl carbonate
DE69620470T2 (en) 1995-12-22 2002-11-21 Asahi Kasei Kabushiki Kaisha, Osaka METHOD FOR THE CONTINUOUS PRODUCTION OF DIALKYL CARBONATES AND DIOLS
CN1145600C (en) 1998-06-10 2004-04-14 旭化成株式会社 Process for continuous production of dialkyl carbonate and diol
AU2827900A (en) 1999-03-03 2000-09-21 Asahi Kasei Kabushiki Kaisha Process for continuously producing dialkyl carbonate and diol
US6166240A (en) * 2000-02-22 2000-12-26 Mobil Oil Corporation Process for co-production of dialkyl carbonate and alkanediol
US6573396B2 (en) 2001-10-12 2003-06-03 Exxonmobil Chemical Patents Inc. Co-production of dialkyl carbonates and diols with treatment of hydroxy alkyl carbonate
JP2003300918A (en) * 2002-04-11 2003-10-21 Mitsui Chemicals Inc Method for continuous and simultaneous production of dialkyl carbonate and glycol
US6620959B1 (en) 2002-04-16 2003-09-16 Exxonmobil Chemical Patents Inc. Process for the production of unsymmetric and/or symmetric dialkyl carbonates and diols
JP4000912B2 (en) * 2002-05-30 2007-10-31 三菱化学株式会社 Method for producing dimethyl carbonate
JP4424898B2 (en) * 2002-10-08 2010-03-03 旭化成ケミカルズ株式会社 Process for producing dialkyl carbonates and diols
JP2006023065A (en) 2004-06-10 2006-01-26 Mitsubishi Electric Corp Ventilation function-equipped air conditioner, ventilation device for ventilation function-equipped air conditioner and ventilation method for ventilation function-equipped air conditioner
JP2006206497A (en) * 2005-01-28 2006-08-10 Asahi Kasei Chemicals Corp Method for producing dialkyl carbonate and diol
EA012027B1 (en) 2005-12-12 2009-06-30 Асахи Касеи Кемикалз Корпорейшн Process for production of dialkyl carbonate and diol in industrial scale
TW200732291A (en) 2005-12-14 2007-09-01 Asahi Kasei Chemicals Corp Process for production of dialkyl carbonate and diol in industrial scale and with high yield
TWI383976B (en) 2006-02-22 2013-02-01 Shell Int Research Process for the production of dialkyl carbonate and alkanediol
JP5094459B2 (en) 2007-03-09 2012-12-12 ローム アンド ハース カンパニー An improved method for converting alkanes to unsaturated carboxylic acids.
DE102009030680A1 (en) * 2009-06-26 2010-12-30 Bayer Materialscience Ag Process for the preparation of dialkyl carbonates from alkylene carbonates and alcohols
DE102009053370A1 (en) 2009-11-14 2011-05-19 Bayer Materialscience Ag Process for the purification of dialkyl carbonates
TWI473786B (en) 2009-11-16 2015-02-21 Shell Int Research Process for preparing alkanediol and dialkyl carbonate

Also Published As

Publication number Publication date
EP2788315A1 (en) 2014-10-15
WO2013083618A1 (en) 2013-06-13
KR20140113931A (en) 2014-09-25
BR112014013557A2 (en) 2017-06-13
JP2015504855A (en) 2015-02-16
CN104203899A (en) 2014-12-10

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