CN104155163A - 鸡肉中妥曲珠利、妥曲珠利砜残留冻干粉标准样品的制法 - Google Patents
鸡肉中妥曲珠利、妥曲珠利砜残留冻干粉标准样品的制法 Download PDFInfo
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- CN104155163A CN104155163A CN201410418914.XA CN201410418914A CN104155163A CN 104155163 A CN104155163 A CN 104155163A CN 201410418914 A CN201410418914 A CN 201410418914A CN 104155163 A CN104155163 A CN 104155163A
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- toltrazuril
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- 229960000898 toltrazuril Drugs 0.000 title claims abstract description 43
- OCINXEZVIIVXFU-UHFFFAOYSA-N 1-methyl-3-[3-methyl-4-[4-(trifluoromethylthio)phenoxy]phenyl]-1,3,5-triazinane-2,4,6-trione Chemical compound CC1=CC(N2C(N(C)C(=O)NC2=O)=O)=CC=C1OC1=CC=C(SC(F)(F)F)C=C1 OCINXEZVIIVXFU-UHFFFAOYSA-N 0.000 title claims abstract description 42
- 239000000843 powder Substances 0.000 title claims abstract description 19
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- 241000287828 Gallus gallus Species 0.000 claims abstract description 37
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- 239000003814 drug Substances 0.000 claims abstract description 16
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 11
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- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229930003268 Vitamin C Natural products 0.000 claims abstract description 4
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- VBUNOIXRZNJNAD-UHFFFAOYSA-N ponazuril Chemical compound CC1=CC(N2C(N(C)C(=O)NC2=O)=O)=CC=C1OC1=CC=C(S(=O)(=O)C(F)(F)F)C=C1 VBUNOIXRZNJNAD-UHFFFAOYSA-N 0.000 claims description 32
- 230000005477 standard model Effects 0.000 claims description 31
- 229960003508 ponazuril Drugs 0.000 claims description 30
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 20
- 238000012360 testing method Methods 0.000 claims description 14
- 238000004108 freeze drying Methods 0.000 claims description 11
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- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 claims description 11
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- QWKYIPKCLAUFCM-UHFFFAOYSA-N 1-methyl-3-[3-methyl-4-[4-(trifluoromethylsulfinyl)phenoxy]phenyl]-1,3,5-triazinane-2,4,6-trione Chemical compound CC1=CC(N2C(N(C)C(=O)NC2=O)=O)=CC=C1OC1=CC=C(S(=O)C(F)(F)F)C=C1 QWKYIPKCLAUFCM-UHFFFAOYSA-N 0.000 description 3
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- ZSZFUDFOPOMEET-UHFFFAOYSA-N 2-(4-chlorophenyl)-2-[2,6-dichloro-4-(3,5-dioxo-1,2,4-triazin-2-yl)phenyl]acetonitrile Chemical compound C1=CC(Cl)=CC=C1C(C#N)C1=C(Cl)C=C(N2C(NC(=O)C=N2)=O)C=C1Cl ZSZFUDFOPOMEET-UHFFFAOYSA-N 0.000 description 2
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CN201410418914.XA CN104155163B (zh) | 2014-08-22 | 2014-08-22 | 鸡肉中妥曲珠利、妥曲珠利砜残留冻干粉标准样品的制法 |
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CN201410418914.XA CN104155163B (zh) | 2014-08-22 | 2014-08-22 | 鸡肉中妥曲珠利、妥曲珠利砜残留冻干粉标准样品的制法 |
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CN104155163A true CN104155163A (zh) | 2014-11-19 |
CN104155163B CN104155163B (zh) | 2015-10-28 |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104596824A (zh) * | 2015-02-14 | 2015-05-06 | 福建出入境检验检疫局检验检疫技术中心 | 含金刚烷胺和利巴韦林的鸡肉基体标准物质及其制备方法 |
CN104764835A (zh) * | 2015-04-28 | 2015-07-08 | 中华人民共和国福清出入境检验检疫局 | 含氟吗啉残留的马铃薯粉基体标准样品及其制备方法 |
CN105547788A (zh) * | 2016-02-23 | 2016-05-04 | 蒋丹 | 豆粉中串珠镰刀菌定性标准样品及其制备方法 |
CN106568861A (zh) * | 2016-11-04 | 2017-04-19 | 辽宁省检验检疫科学技术研究院 | 鸡肉中氯羟吡啶标准样品、制备方法及应用 |
CN106596215A (zh) * | 2015-11-02 | 2017-04-26 | 中国检验检疫科学研究院 | 含有呋喃它酮代谢物兽药残留能力验证样品及其制备方法 |
CN107041422A (zh) * | 2017-06-12 | 2017-08-15 | 和县金城米业有限责任公司 | 新收绿豆储存方法 |
CN107251945A (zh) * | 2017-06-12 | 2017-10-17 | 和县金城米业有限责任公司 | 一种绿豆入库前处理方法 |
CN107741502A (zh) * | 2017-10-12 | 2018-02-27 | 中国农业科学院农业质量标准与检测技术研究所 | 一种牛肉蛋白中碳、氮稳定同位素标准样品的制备方法 |
Citations (3)
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CN1837771A (zh) * | 2006-04-19 | 2006-09-27 | 姚家彪 | 肉粉中兽药残留分析样品及制备工艺 |
CN102323123A (zh) * | 2011-07-19 | 2012-01-18 | 时文春 | 一种鲤鱼肌肉中环丙沙星、恩诺沙星残留冻干粉标准样品的制备方法 |
CN102323122A (zh) * | 2011-07-19 | 2012-01-18 | 时文春 | 一种鲤鱼肌肉中磺胺甲恶唑残留冻干粉标准样品的制备方法 |
-
2014
- 2014-08-22 CN CN201410418914.XA patent/CN104155163B/zh not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1837771A (zh) * | 2006-04-19 | 2006-09-27 | 姚家彪 | 肉粉中兽药残留分析样品及制备工艺 |
CN102323123A (zh) * | 2011-07-19 | 2012-01-18 | 时文春 | 一种鲤鱼肌肉中环丙沙星、恩诺沙星残留冻干粉标准样品的制备方法 |
CN102323122A (zh) * | 2011-07-19 | 2012-01-18 | 时文春 | 一种鲤鱼肌肉中磺胺甲恶唑残留冻干粉标准样品的制备方法 |
Non-Patent Citations (2)
Title |
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JING YU SHEN 等: "Supercritical fluid extraction of the fluoroquinolones norfloxacin and ofloxacin from orally treated-chicken breast muscles", 《ANALYTICA CHIMICA ACTA》 * |
王凤池等: "《SN/T2318-2009》", 7 July 2009 * |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104596824A (zh) * | 2015-02-14 | 2015-05-06 | 福建出入境检验检疫局检验检疫技术中心 | 含金刚烷胺和利巴韦林的鸡肉基体标准物质及其制备方法 |
CN104764835A (zh) * | 2015-04-28 | 2015-07-08 | 中华人民共和国福清出入境检验检疫局 | 含氟吗啉残留的马铃薯粉基体标准样品及其制备方法 |
CN104764835B (zh) * | 2015-04-28 | 2016-07-06 | 中华人民共和国福清出入境检验检疫局 | 含氟吗啉残留的马铃薯粉基体标准样品及其制备方法 |
CN106596215A (zh) * | 2015-11-02 | 2017-04-26 | 中国检验检疫科学研究院 | 含有呋喃它酮代谢物兽药残留能力验证样品及其制备方法 |
CN105547788A (zh) * | 2016-02-23 | 2016-05-04 | 蒋丹 | 豆粉中串珠镰刀菌定性标准样品及其制备方法 |
CN105547788B (zh) * | 2016-02-23 | 2019-06-04 | 蒋丹 | 豆粉中串珠镰刀菌定性标准样品及其制备方法 |
CN106568861A (zh) * | 2016-11-04 | 2017-04-19 | 辽宁省检验检疫科学技术研究院 | 鸡肉中氯羟吡啶标准样品、制备方法及应用 |
CN107041422A (zh) * | 2017-06-12 | 2017-08-15 | 和县金城米业有限责任公司 | 新收绿豆储存方法 |
CN107251945A (zh) * | 2017-06-12 | 2017-10-17 | 和县金城米业有限责任公司 | 一种绿豆入库前处理方法 |
CN107741502A (zh) * | 2017-10-12 | 2018-02-27 | 中国农业科学院农业质量标准与检测技术研究所 | 一种牛肉蛋白中碳、氮稳定同位素标准样品的制备方法 |
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Inventor after: Yang Lijun Inventor after: Wang Jing Inventor after: Xu Li Inventor after: Liu Yumin Inventor after: Hu Qiaoru Inventor after: Li Zhaojie Inventor after: Wang Meiling Inventor before: Yang Lijun Inventor before: Wang Jing Inventor before: Liu Yumin Inventor before: Hu Qiaoru Inventor before: Li Zhaojie Inventor before: Wang Meiling |
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Free format text: CORRECT: INVENTOR; FROM: YANG LIJUN WANG JING LIU YUMIN HU QIAORU LI ZHAOJIE WANG MEILING TO: YANG LIJUN WANG JING XU LI LIU YUMIN HU QIAORU LI ZHAOJIE WANG MEILING |
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