CN104126617B - A kind of fruit tree fleahopper agent for killing and its preparation method - Google Patents
A kind of fruit tree fleahopper agent for killing and its preparation method Download PDFInfo
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- CN104126617B CN104126617B CN201410334071.5A CN201410334071A CN104126617B CN 104126617 B CN104126617 B CN 104126617B CN 201410334071 A CN201410334071 A CN 201410334071A CN 104126617 B CN104126617 B CN 104126617B
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- fleahopper
- agent
- fruit tree
- killing
- fruit
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- 235000013399 edible fruits Nutrition 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- NWWZPOKUUAIXIW-DHZHZOJOSA-N (E)-thiamethoxam Chemical compound [O-][N+](=O)/N=C/1N(C)COCN\1CC1=CN=C(Cl)S1 NWWZPOKUUAIXIW-DHZHZOJOSA-N 0.000 claims abstract description 19
- 239000005874 Bifenthrin Substances 0.000 claims abstract description 19
- 244000044425 Quisqualis indica Species 0.000 claims abstract description 19
- 241000405414 Rehmannia Species 0.000 claims abstract description 19
- 240000004460 Tanacetum coccineum Species 0.000 claims abstract description 19
- 235000008326 Trichosanthes anguina Nutrition 0.000 claims abstract description 19
- 244000078912 Trichosanthes cucumerina Species 0.000 claims abstract description 19
- ROVGZAWFACYCSP-MQBLHHJJSA-N [2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OC1C(C)=C(C\C=C/C=C)C(=O)C1 ROVGZAWFACYCSP-MQBLHHJJSA-N 0.000 claims abstract description 19
- OMFRMAHOUUJSGP-IRHGGOMRSA-N bifenthrin Chemical compound C1=CC=C(C=2C=CC=CC=2)C(C)=C1COC(=O)[C@@H]1[C@H](\C=C(/Cl)C(F)(F)F)C1(C)C OMFRMAHOUUJSGP-IRHGGOMRSA-N 0.000 claims abstract description 19
- 229940015367 pyrethrum Drugs 0.000 claims abstract description 19
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 16
- HRYILSDLIGTCOP-UHFFFAOYSA-N N-benzoylurea Chemical compound NC(=O)NC(=O)C1=CC=CC=C1 HRYILSDLIGTCOP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000000284 extract Substances 0.000 claims description 25
- 239000007788 liquid Substances 0.000 claims description 18
- 239000012530 fluid Substances 0.000 claims description 16
- 239000012141 concentrate Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- UISUNVFOGSJSKD-UHFFFAOYSA-N chlorfluazuron Chemical compound FC1=CC=CC(F)=C1C(=O)NC(=O)NC(C=C1Cl)=CC(Cl)=C1OC1=NC=C(C(F)(F)F)C=C1Cl UISUNVFOGSJSKD-UHFFFAOYSA-N 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 8
- KDGQGEKLPWYCGO-UHFFFAOYSA-N 1-butoxybutane;urea Chemical compound NC(N)=O.CCCCOCCCC KDGQGEKLPWYCGO-UHFFFAOYSA-N 0.000 claims description 5
- 239000005942 Triflumuron Substances 0.000 claims description 5
- RGNPBRKPHBKNKX-UHFFFAOYSA-N hexaflumuron Chemical compound C1=C(Cl)C(OC(F)(F)C(F)F)=C(Cl)C=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F RGNPBRKPHBKNKX-UHFFFAOYSA-N 0.000 claims description 5
- XAIPTRIXGHTTNT-UHFFFAOYSA-N triflumuron Chemical compound C1=CC(OC(F)(F)F)=CC=C1NC(=O)NC(=O)C1=CC=CC=C1Cl XAIPTRIXGHTTNT-UHFFFAOYSA-N 0.000 claims description 5
- 239000000839 emulsion Substances 0.000 claims description 2
- 239000004530 micro-emulsion Substances 0.000 claims description 2
- 230000002045 lasting effect Effects 0.000 abstract description 3
- 230000000857 drug effect Effects 0.000 abstract description 2
- 238000003912 environmental pollution Methods 0.000 abstract description 2
- 231100000572 poisoning Toxicity 0.000 abstract description 2
- 230000000607 poisoning effect Effects 0.000 abstract description 2
- 244000144977 poultry Species 0.000 abstract description 2
- 229920000742 Cotton Polymers 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 241000283615 Taylorilygus apicalis Species 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 244000126002 Ziziphus vulgaris Species 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- JVGPVVUTUMQJKL-UHFFFAOYSA-N 2-(2-butoxyethoxy)ethyl thiocyanate Chemical compound CCCCOCCOCCSC#N JVGPVVUTUMQJKL-UHFFFAOYSA-N 0.000 description 1
- 244000144730 Amygdalus persica Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 235000016623 Fragaria vesca Nutrition 0.000 description 1
- 240000009088 Fragaria x ananassa Species 0.000 description 1
- 235000011363 Fragaria x ananassa Nutrition 0.000 description 1
- 244000020551 Helianthus annuus Species 0.000 description 1
- 235000003222 Helianthus annuus Nutrition 0.000 description 1
- 235000011430 Malus pumila Nutrition 0.000 description 1
- 244000070406 Malus silvestris Species 0.000 description 1
- 235000015103 Malus silvestris Nutrition 0.000 description 1
- 240000000249 Morus alba Species 0.000 description 1
- 235000008708 Morus alba Nutrition 0.000 description 1
- 241000819999 Nymphes Species 0.000 description 1
- 235000006040 Prunus persica var persica Nutrition 0.000 description 1
- 241000220324 Pyrus Species 0.000 description 1
- 108700019146 Transgenes Proteins 0.000 description 1
- 235000010726 Vigna sinensis Nutrition 0.000 description 1
- 244000042314 Vigna unguiculata Species 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 235000008529 Ziziphus vulgaris Nutrition 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 238000001647 drug administration Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 230000012447 hatching Effects 0.000 description 1
- 235000021017 pears Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000009897 systematic effect Effects 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Medicines Containing Plant Substances (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention discloses a kind of fruit tree fleahopper agent for killing; it is characterized in that, it is primarily of made by following component: benzoyl urea 2 parts, bifenthrin 1-5 part, Diacloden 1-5 part, pyrethrum 30-40 part, Snakegourd Root 20-40 part, glutinous rehmannia 30-50 part, Rangooncreeper Fruit's 10-20 part, Cortex Meliae 10-20 part. The invention also discloses the preparation method of described fruit tree fleahopper agent for killing. Relative to prior art, the fruit tree fleahopper agent for killing of gained of the present invention, to person poultry harmless, farm crop are not produced poisoning, and its lasting period is long, it is possible to effectively kill fruit tree fleahopper, on the basis improving drug effect, it is possible to reduce the possibility that fleahopper produces resistance, reduce environmental pollution.
Description
Technical field
The present invention relates to a kind of sterilant, it is specifically related to a kind of containing the high efficiency composition sterilant of natural extract and multiple sterilant, is applied to agriculture field.
Background technology
Fleahopper huge number is widely distributed, is worldwide Agricultural pests, it is possible to various crop and the economic plants such as harm cotton, fruit tree, vegetables, tealeaves, mulberry tree, strawberry, herbage, Sunflower Receptacle. In recent ten years, along with the big area of transgene cotton in China is promoted, fleahopper population is in the outburst in cotton region, the report endangering fruit tree about fleahopper also occurs in a large number, and scope involves the vast planting fruit trees districts such as North China, East China, northwest, the object of harm also relates to north major part fruit variety, and existing result of study display, the hazard rating of jujube, grape, apple, peach and pears is increased sharply by fleahopper.
Due in China fleahopper main harm cotton all the time, therefore main research also concentrates on cotton field fleahopper, in view of present fleahopper is in fruit tree outburst harm, but its systematic study is also relatively less, and Prevention Technique is also main based on chemical prevention, then due to life-time service, make fleahopper that polytype sterilant is produced resistance, therefore, seek novel fleahopper agent for killing, it is worth research further.
Summary of the invention
Goal of the invention: in order to overcome the deficiencies in the prior art, the present invention provides a kind of fruit tree specific complex sterilant.
Technical scheme: for achieving the above object, the present invention provides a kind of fruit tree fleahopper agent for killing, and it is primarily of made by following component:
Benzoyl urea 2 parts, bifenthrin 1-5 part, Diacloden 1-5 part, pyrethrum 30-40 part,
Snakegourd Root 20-40 part, glutinous rehmannia 30-50 part, Rangooncreeper Fruit's 10-20 part, Cortex Meliae 10-20 part.
As preferably, described fruit tree fleahopper agent for killing is primarily of made by following component:
Benzoyl urea 2 parts, bifenthrin 2-4 part, Diacloden 2-4 part, pyrethrum 32-38 part,
Snakegourd Root 25-35 part, glutinous rehmannia 35-45 part, Rangooncreeper Fruit's 12-18 part, Cortex Meliae 12-18 part.
As another kind preferably, described benzoyl urea is the one in chlorfluazuron, HEXAFLUMURON, triflumuron, butyl ether urea.
As another kind preferably, the concentration of described benzoyl urea in described sterilant is (0.2-1) %.
Present invention also offers the preparation method of described fruit tree fleahopper agent for killing, it mainly comprises the following steps:
(1) pyrethrum, Snakegourd Root, glutinous rehmannia, Rangooncreeper Fruit and Cortex Meliae clean, dry, pulverize, add the water of 6-10 times of volume, extract 1-3 time, each 1-3 hour, united extraction liquid, concentrate to relative density when 30 DEG C be the fluid extract of 1.05-1.10;
(2) by above-mentioned fluid extract and benzoyl urea, bifenthrin, Diacloden, liquid preparation is conventionally made.
As preferably, described liquid preparation is suspensoid, emulsion, water dispersant or microemulsion.
Useful effect: the present invention is relative to prior art, and the fruit tree fleahopper agent for killing of gained, to person poultry harmless, farm crop are not produced poisoning, and its lasting period is long, it is possible to effectively kill fruit tree fleahopper, on the basis improving drug effect, it is possible to reduce the possibility that fleahopper produces resistance, reduce environmental pollution.
Embodiment
Below in conjunction with embodiment, the present invention is further described.
Embodiment 1:
Prescription: chlorfluazuron 2kg, bifenthrin 1kg, Diacloden 1kg, pyrethrum 30kg,
Snakegourd Root 20kg, glutinous rehmannia 30kg, Rangooncreeper Fruit 10kg, Cortex Meliae 10kg.
Preparation method:
(1) pyrethrum, Snakegourd Root, glutinous rehmannia, Rangooncreeper Fruit and Cortex Meliae clean, dry, pulverize, add the water of 6 times of volumes, extract 1 time, each 3 hours, united extraction liquid, concentrate to relative density when 30 DEG C be the fluid extract of 1.05;
(2) by above-mentioned fluid extract and chlorfluazuron, bifenthrin, Diacloden, liquid preparation is conventionally made.
The concentration of described chlorfluazuron in described sterilant is 0.2%.
Embodiment 2:
Prescription: HEXAFLUMURON 2kg, bifenthrin 5kg, Diacloden 5kg, pyrethrum 40kg,
Snakegourd Root 40kg, glutinous rehmannia 50kg, Rangooncreeper Fruit 20kg, Cortex Meliae 20kg.
Preparation method:
(1) pyrethrum, Snakegourd Root, glutinous rehmannia, Rangooncreeper Fruit and Cortex Meliae clean, dry, pulverize, add the water of 10 times of volumes, extract 3 times, each 1 hour, united extraction liquid, concentrate to relative density when 30 DEG C be the fluid extract of 1.10;
(2) by above-mentioned fluid extract and HEXAFLUMURON, bifenthrin, Diacloden, liquid preparation is conventionally made.
The concentration of described HEXAFLUMURON in described sterilant is 1%.
Embodiment 3:
Prescription: triflumuron 2kg, bifenthrin 3kg, Diacloden 3kg, pyrethrum 35kg,
Snakegourd Root 30kg, glutinous rehmannia 40kg, Rangooncreeper Fruit 15kg, Cortex Meliae 15kg.
Preparation method:
(1) pyrethrum, Snakegourd Root, glutinous rehmannia, Rangooncreeper Fruit and Cortex Meliae clean, dry, pulverize, add the water of 8 times of volumes, extract 2 times, each 2 hours, united extraction liquid, concentrate to relative density when 30 DEG C be the fluid extract of 1.08;
(2) by above-mentioned fluid extract and triflumuron, bifenthrin, Diacloden, liquid preparation is conventionally made.
The concentration of described triflumuron in described sterilant is 0.6%.
Embodiment 4:
Prescription: butyl ether urea 2kg, bifenthrin 2kg, Diacloden 2kg, pyrethrum 32kg,
Snakegourd Root 25kg, glutinous rehmannia 35kg, Rangooncreeper Fruit 12kg, Cortex Meliae 12kg.
Preparation method:
(1) pyrethrum, Snakegourd Root, glutinous rehmannia, Rangooncreeper Fruit and Cortex Meliae clean, dry, pulverize, add the water of 7 times of volumes, extract 2 times, each 2 hours, united extraction liquid, concentrate to relative density when 30 DEG C be the fluid extract of 1.06;
(2) by above-mentioned fluid extract and butyl ether urea, bifenthrin, Diacloden, liquid preparation is conventionally made.
The concentration of described butyl ether urea in described sterilant is 0.4%.
Embodiment 5:
Prescription: chlorfluazuron 2kg, bifenthrin 4kg, Diacloden 4kg, pyrethrum 38kg,
Snakegourd Root 35kg, glutinous rehmannia 45kg, Rangooncreeper Fruit 18kg, Cortex Meliae 18kg.
Preparation method:
(1) pyrethrum, Snakegourd Root, glutinous rehmannia, Rangooncreeper Fruit and Cortex Meliae clean, dry, pulverize, add the water of 9 times of volumes, extract 2 times, each 1 hour, united extraction liquid, concentrate to relative density when 30 DEG C be the fluid extract of 1.09;
(2) by above-mentioned fluid extract and chlorfluazuron, bifenthrin, Diacloden, liquid preparation is conventionally made.
The concentration of described chlorfluazuron in described sterilant is 0.8%.
The effect experiment of fleahopper larva be the results are shown in Table 1 by experimental example gained sterilant of the present invention
Jujube tree gathers the 1st generation nymph after the hatching of green plant bug hibernating egg, in room conditions (photoperiod is L: D=14: 10 for temperature 24��26 DEG C, relative humidity 60%��80%), adopt cowpea to raise many generations, choose the consistent examination worm of the physiological status getting its suitable length of time for examination;
Control group A uses not containing organic synthetics sterilant, refers to according to prescription of the present invention and method, does not add benzoyl urea, bifenthrin and Diacloden gained sterilant;
Control group B uses simple lethane, refers to that, according to prescription of the present invention and method, the equal simply immersing of pyrethrum, Snakegourd Root, glutinous rehmannia, Rangooncreeper Fruit and Cortex Meliae, soak solution and other compositions simply mix, and to obtain final product;
Mortality ratio after medicine: refer to after drug administration after certain time, death toll accounts for the per-cent of total test number.
Table 1 gained sterilant of the present invention is to the effect experiment result of green plant bug larva
Note: compared with control group A or control group B, * P < 0.05
As seen from the above table, comparing with control group B with control group A, the sterilant of embodiment 1-5 group, for green plant bug larva, after medicine, after 3 days and medicine, 7 days mortality ratio significantly improve, and illustrate that sterilant killing rate fleahopper effect of the present invention is relatively by force, and the lasting period is permanent.
Claims (6)
1. a fruit tree fleahopper agent for killing, it is characterised in that, it is primarily of made by following component:
Benzoyl urea 2 parts, bifenthrin 1-5 part, Diacloden 1-5 part, pyrethrum 30-40 part,
Snakegourd Root 20-40 part, glutinous rehmannia 30-50 part, Rangooncreeper Fruit's 10-20 part, Cortex Meliae 10-20 part;
Described fruit tree fleahopper agent for killing is by made by following step:
(1) pyrethrum, Snakegourd Root, glutinous rehmannia, Rangooncreeper Fruit and Cortex Meliae clean, dry, pulverize, add the water of 6-10 times of volume, extract 1-3 time, each 1-3 hour, united extraction liquid, concentrate to relative density when 30 DEG C be the fluid extract of 1.05-1.10;
(2) by above-mentioned fluid extract and benzoyl urea, bifenthrin, Diacloden, liquid preparation is conventionally made.
2. a kind of fruit tree fleahopper agent for killing according to claim 1, it is characterised in that: it is primarily of made by following component:
Benzoyl urea 2 parts, bifenthrin 2-4 part, Diacloden 2-4 part, pyrethrum 32-38 part,
Snakegourd Root 25-35 part, glutinous rehmannia 35-45 part, Rangooncreeper Fruit's 12-18 part, Cortex Meliae 12-18 part.
3. a kind of fruit tree fleahopper agent for killing according to claim 1, it is characterised in that: described benzoyl urea is the one in chlorfluazuron, HEXAFLUMURON, triflumuron, butyl ether urea.
4. a kind of fruit tree fleahopper agent for killing according to claim 1, it is characterised in that: with parts by weight, the concentration of described benzoyl urea in described sterilant is (0.2-1) %.
5. the preparation method of fruit tree fleahopper agent for killing described in the arbitrary item of claim 1-4, it is characterised in that, it mainly comprises the following steps:
(1) pyrethrum, Snakegourd Root, glutinous rehmannia, Rangooncreeper Fruit and Cortex Meliae clean, dry, pulverize, add the water of 6-10 times of volume, extract 1-3 time, each 1-3 hour, united extraction liquid, concentrate to relative density when 30 DEG C be the fluid extract of 1.05-1.10;
(2) by above-mentioned fluid extract and benzoyl urea, bifenthrin, Diacloden, liquid preparation is conventionally made.
6. the preparation method of fruit tree fleahopper agent for killing according to claim 5, it is characterised in that: described liquid preparation is suspensoid, emulsion or microemulsion.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410334071.5A CN104126617B (en) | 2014-07-14 | 2014-07-14 | A kind of fruit tree fleahopper agent for killing and its preparation method |
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| CN201410334071.5A CN104126617B (en) | 2014-07-14 | 2014-07-14 | A kind of fruit tree fleahopper agent for killing and its preparation method |
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| CN104126617A CN104126617A (en) | 2014-11-05 |
| CN104126617B true CN104126617B (en) | 2016-06-08 |
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| CN104839231A (en) * | 2015-05-15 | 2015-08-19 | 卞佳林 | Maize Athetis lepigone insecticide |
| CN105145668A (en) * | 2015-07-29 | 2015-12-16 | 句容市茅山镇恒泰家庭农场 | Green drug for controlling grape apolygus lucorum and preparation method thereof |
| CN105123809A (en) * | 2015-08-27 | 2015-12-09 | 蚌埠龙达农业专业合作社 | Biological insecticide for floriculture and preparation method thereof |
| CN106508952A (en) * | 2016-10-26 | 2017-03-22 | 河南科技学院 | Pesticide composition for preventing and treating cotton field miridae |
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| CN1281138C (en) * | 2005-03-23 | 2006-10-25 | 赵尚学 | Plant insects protecting agent |
| CN102273444A (en) * | 2011-09-13 | 2011-12-14 | 广西田园生化股份有限公司 | Ultralow volume liquid containing thiamethoxam |
| CN103651615B (en) * | 2013-12-18 | 2015-08-05 | 青岛百瑞吉生物工程有限公司 | A kind of biological insecticides containing lycopene and preparation method thereof |
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