CN1040783A - 2，2-二氯-1，1，1-三氟乙烷的提纯 - Google Patents
2，2-二氯-1，1，1-三氟乙烷的提纯 Download PDFInfo
- Publication number
- CN1040783A CN1040783A CN89107051A CN89107051A CN1040783A CN 1040783 A CN1040783 A CN 1040783A CN 89107051 A CN89107051 A CN 89107051A CN 89107051 A CN89107051 A CN 89107051A CN 1040783 A CN1040783 A CN 1040783A
- Authority
- CN
- China
- Prior art keywords
- chloro
- halothane
- olefinic
- metal permanganate
- permanganate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229960003132 halothane Drugs 0.000 title claims abstract description 46
- 238000000746 purification Methods 0.000 title abstract description 7
- 229910052751 metal Inorganic materials 0.000 claims abstract description 21
- 239000002184 metal Substances 0.000 claims abstract description 21
- 150000008282 halocarbons Chemical class 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 17
- 239000007788 liquid Substances 0.000 claims abstract description 6
- 239000012286 potassium permanganate Substances 0.000 claims description 5
- JYLNVJYYQQXNEK-UHFFFAOYSA-N 3-amino-2-(4-chlorophenyl)-1-propanesulfonic acid Chemical group OS(=O)(=O)CC(CN)C1=CC=C(Cl)C=C1 JYLNVJYYQQXNEK-UHFFFAOYSA-N 0.000 claims description 2
- 239000000243 solution Substances 0.000 description 15
- 239000003795 chemical substances by application Substances 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000012043 crude product Substances 0.000 description 6
- 229910052783 alkali metal Inorganic materials 0.000 description 4
- 150000001340 alkali metals Chemical class 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 4
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- IAQRGUVFOMOMEM-UHFFFAOYSA-N butene Natural products CC=CC IAQRGUVFOMOMEM-UHFFFAOYSA-N 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- UUAGAQFQZIEFAH-UHFFFAOYSA-N chlorotrifluoroethylene Chemical group FC(F)=C(F)Cl UUAGAQFQZIEFAH-UHFFFAOYSA-N 0.000 description 3
- 230000002939 deleterious effect Effects 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 2
- KYKAJFCTULSVSH-UHFFFAOYSA-N chloro(fluoro)methane Chemical compound F[C]Cl KYKAJFCTULSVSH-UHFFFAOYSA-N 0.000 description 2
- 238000004587 chromatography analysis Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 231100000734 genotoxic potential Toxicity 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000005057 refrigeration Methods 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- JRENXZBKMHPULY-UPHRSURJSA-N (z)-2-chloro-1,1,1,4,4,4-hexafluorobut-2-ene Chemical compound FC(F)(F)\C=C(/Cl)C(F)(F)F JRENXZBKMHPULY-UPHRSURJSA-N 0.000 description 1
- WFLOTYSKFUPZQB-UHFFFAOYSA-N 1,2-difluoroethene Chemical group FC=CF WFLOTYSKFUPZQB-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 229920004449 Halon® Polymers 0.000 description 1
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 229910052728 basic metal Inorganic materials 0.000 description 1
- 150000003818 basic metals Chemical class 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- QDGONURINHVBEW-UHFFFAOYSA-N dichlorodifluoroethylene Chemical group FC(F)=C(Cl)Cl QDGONURINHVBEW-UHFFFAOYSA-N 0.000 description 1
- PXBRQCKWGAHEHS-UHFFFAOYSA-N dichlorodifluoromethane Chemical compound FC(F)(Cl)Cl PXBRQCKWGAHEHS-UHFFFAOYSA-N 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- BNBLBRISEAQIHU-UHFFFAOYSA-N disodium dioxido(dioxo)manganese Chemical compound [Na+].[Na+].[O-][Mn]([O-])(=O)=O BNBLBRISEAQIHU-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 150000005826 halohydrocarbons Chemical class 0.000 description 1
- 229910000039 hydrogen halide Inorganic materials 0.000 description 1
- 239000012433 hydrogen halide Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- BNIXVQGCZULYKV-UHFFFAOYSA-N pentachloroethane Chemical compound ClC(Cl)C(Cl)(Cl)Cl BNIXVQGCZULYKV-UHFFFAOYSA-N 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 229950011008 tetrachloroethylene Drugs 0.000 description 1
- CYRMSUTZVYGINF-UHFFFAOYSA-N trichlorofluoromethane Chemical compound FC(Cl)(Cl)Cl CYRMSUTZVYGINF-UHFFFAOYSA-N 0.000 description 1
- 229940029284 trichlorofluoromethane Drugs 0.000 description 1
- -1 trifluorochloroethylene, 1,1-dichloro difluoroethylene Chemical group 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/395—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to a chemical modification of at least one compound
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
- C07C19/10—Acyclic saturated compounds containing halogen atoms containing fluorine and chlorine
- C07C19/12—Acyclic saturated compounds containing halogen atoms containing fluorine and chlorine having two carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US23956888A | 1988-09-01 | 1988-09-01 | |
| US239,568 | 1988-09-01 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1040783A true CN1040783A (zh) | 1990-03-28 |
Family
ID=22902728
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN89107051A Pending CN1040783A (zh) | 1988-09-01 | 1989-09-01 | 2，2-二氯-1，1，1-三氟乙烷的提纯 |
Country Status (9)
| Country | Link |
|---|---|
| EP (1) | EP0357328A1 (enrdf_load_stackoverflow) |
| JP (1) | JPH02282338A (enrdf_load_stackoverflow) |
| KR (1) | KR900004657A (enrdf_load_stackoverflow) |
| CN (1) | CN1040783A (enrdf_load_stackoverflow) |
| AR (1) | AR245433A1 (enrdf_load_stackoverflow) |
| AU (1) | AU4093389A (enrdf_load_stackoverflow) |
| BR (1) | BR8904367A (enrdf_load_stackoverflow) |
| IN (1) | IN171828B (enrdf_load_stackoverflow) |
| ZA (1) | ZA896726B (enrdf_load_stackoverflow) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE68916756D1 (de) * | 1988-11-22 | 1994-08-18 | Du Pont | Verfahren zur Reinigung von gesättigten Halokohlenwasserstoffen. |
| US5189230A (en) * | 1990-12-21 | 1993-02-23 | Hoechst Aktiengesellschaft | Process for the removal of olefinic impurities from hydrochlorofluorocarbons |
| JPH07121881B2 (ja) * | 1991-03-26 | 1995-12-25 | 信越化学工業株式会社 | 含フッ素有機基を有するエチレン化合物に含まれるヨウ素を除去する方法 |
| IT1251951B (it) * | 1991-10-18 | 1995-05-27 | Ausimont Spa | Procedimento per purificare 1,1,1-trifluoro-,2,2 dicloroetano dall`isomero 1,1,2-trifluoro-1,2-dicloroetano. |
| US5569797A (en) * | 1992-01-07 | 1996-10-29 | E. I. Du Pont De Nemours And Company | Method of removing olefinic impurities from hydrochlorofluorocarbons |
| JPH06271487A (ja) * | 1993-03-22 | 1994-09-27 | Central Glass Co Ltd | １，１−ジクロロ−１−フルオロエタンの精製法 |
| FR2749581B1 (fr) * | 1996-06-06 | 1998-08-14 | Atochem Elf Sa | Procede de purification d'hydrofluorocarbures satures |
| FR2754816B1 (fr) * | 1996-10-18 | 1998-12-04 | Atochem Elf Sa | Procede de purification d'hydrogenochlorofluoroethanes |
| GB0107705D0 (en) * | 2001-03-28 | 2001-05-16 | Ineos Fluor Ltd | Purification of saturated halocarbons |
| DE10351194B4 (de) * | 2003-10-30 | 2006-07-27 | Hadinek, Lutz, Dipl.-Chem. | Verfahren zur Reinigung fluorierter Kohlenwasserstoffe |
| WO2006119213A2 (en) * | 2005-05-03 | 2006-11-09 | Albemarle Corporation | 1-bromopropane having low acidity |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2286379A (en) * | 1941-05-01 | 1942-06-16 | Dow Chemical Co | Purification of ethyl chloride |
| GB1067811A (en) * | 1965-01-01 | 1967-05-03 | Ici Ltd | Purification of halothane |
| AU518050B2 (en) * | 1977-02-17 | 1981-09-10 | Imperial Chemical Industries Limited | Manufacture of 1,1,1,2-tetrafluoro ethane & method of reducing amount of 1,1,difluord-chldro ethlene impurity |
| US4129603A (en) * | 1978-02-07 | 1978-12-12 | Imperial Chemical Industries Limited | Manufacture of halogenated compounds |
| DD233839A1 (de) * | 1985-01-08 | 1986-03-12 | Akad Wissenschaften Ddr | Verfahren zur abtrennung von perfluoralkanen aus einem gemisch hoehermolekularer aliphatischer perfluoralkane und perfluoralkene |
-
1989
- 1989-08-23 EP EP89308541A patent/EP0357328A1/en not_active Withdrawn
- 1989-08-28 IN IN700/CAL/89A patent/IN171828B/en unknown
- 1989-08-30 BR BR898904367A patent/BR8904367A/pt not_active Application Discontinuation
- 1989-08-31 AU AU40933/89A patent/AU4093389A/en not_active Abandoned
- 1989-08-31 KR KR1019890012586A patent/KR900004657A/ko not_active Withdrawn
- 1989-08-31 AR AR89314815A patent/AR245433A1/es active
- 1989-09-01 CN CN89107051A patent/CN1040783A/zh active Pending
- 1989-09-01 JP JP1227294A patent/JPH02282338A/ja active Pending
- 1989-09-01 ZA ZA896726A patent/ZA896726B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| AR245433A1 (es) | 1994-01-31 |
| IN171828B (enrdf_load_stackoverflow) | 1993-01-23 |
| AU4093389A (en) | 1990-03-08 |
| BR8904367A (pt) | 1990-04-24 |
| JPH02282338A (ja) | 1990-11-19 |
| ZA896726B (en) | 1991-05-29 |
| EP0357328A1 (en) | 1990-03-07 |
| KR900004657A (ko) | 1990-04-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |