CN104066681B - 制备具有特定形态、微粒大小及孔隙度的沉淀二氧化硅的方法 - Google Patents
制备具有特定形态、微粒大小及孔隙度的沉淀二氧化硅的方法 Download PDFInfo
- Publication number
- CN104066681B CN104066681B CN201380006522.6A CN201380006522A CN104066681B CN 104066681 B CN104066681 B CN 104066681B CN 201380006522 A CN201380006522 A CN 201380006522A CN 104066681 B CN104066681 B CN 104066681B
- Authority
- CN
- China
- Prior art keywords
- acid
- concentration
- silicate
- reaction medium
- stage
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/126—Preparation of silica of undetermined type
- C01B33/128—Preparation of silica of undetermined type by acidic treatment of aqueous silicate solutions
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
- C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
- C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1200211A FR2985990B1 (fr) | 2012-01-25 | 2012-01-25 | Nouveau procede de preparation de silices precipitees a morphologie, granulometrie et porosite particulieres |
| FR1200211 | 2012-01-25 | ||
| PCT/EP2013/051233 WO2013110654A1 (fr) | 2012-01-25 | 2013-01-23 | Procédé de préparation de silices précipitées à morphologie, granulométrie porosité particulières |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104066681A CN104066681A (zh) | 2014-09-24 |
| CN104066681B true CN104066681B (zh) | 2018-04-24 |
Family
ID=47598855
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201380006522.6A Expired - Fee Related CN104066681B (zh) | 2012-01-25 | 2013-01-23 | 制备具有特定形态、微粒大小及孔隙度的沉淀二氧化硅的方法 |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US9695053B2 (enExample) |
| EP (1) | EP2807115B1 (enExample) |
| KR (1) | KR20140116530A (enExample) |
| CN (1) | CN104066681B (enExample) |
| AU (1) | AU2013211586A1 (enExample) |
| BR (1) | BR112014017994A8 (enExample) |
| CA (1) | CA2862467A1 (enExample) |
| FR (1) | FR2985990B1 (enExample) |
| MX (1) | MX353387B (enExample) |
| RU (1) | RU2578309C1 (enExample) |
| TW (1) | TWI490165B (enExample) |
| WO (1) | WO2013110654A1 (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2607741C2 (ru) | 2011-12-23 | 2017-01-10 | Родиа Операсьон | Новый способ получения диоксидов кремния |
| FR2984870B1 (fr) | 2011-12-23 | 2014-03-21 | Rhodia Operations | Nouveau procede de preparation de silices precipitees. |
| FR2985993B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2985991B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2985992B1 (fr) | 2012-01-25 | 2015-03-06 | Rhodia Operations | Nouveau procede de preparation de silices precitees |
| EP3619165B1 (en) | 2017-05-05 | 2025-02-12 | Rhodia Operations | Precipitated silica and process for its manufacture |
| PL3619164T3 (pl) | 2017-05-05 | 2025-04-07 | Rhodia Operations | Krzemionka strącona i sposób jej wytwarzania |
| EP3894354A1 (en) * | 2018-12-11 | 2021-10-20 | Rhodia Operations | Precipitated silica for battery separator |
| CN110078083A (zh) * | 2019-06-05 | 2019-08-02 | 确成硅化学股份有限公司 | 一种高抗湿滑性轮胎专用白炭黑及其制备方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101970354A (zh) * | 2008-03-10 | 2011-02-09 | 罗地亚管理公司 | 制备沉淀二氧化硅的新方法,具有特殊的形态、粒度和孔隙率的沉淀二氧化硅及其用途,尤其用于增强聚合物 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3639845A1 (de) | 1986-11-21 | 1988-06-01 | Degussa | Faellungskieselsaeuren, verfahren zu ihrer herstellung und verwendung |
| FR2646673B1 (fr) * | 1989-05-02 | 1991-09-06 | Rhone Poulenc Chimie | Silice sous forme de bille, procede de preparation et son utilisation au renforcement des elastomeres |
| FR2678259B1 (fr) | 1991-06-26 | 1993-11-05 | Rhone Poulenc Chimie | Nouvelles silices precipitees sous forme de granules ou de poudres, procedes de synthese et utilisation au renforcement des elastomeres. |
| ES2194874T3 (es) * | 1993-09-29 | 2003-12-01 | Rhodia Chimie Sa | Silice precipitada. |
| US6169135B1 (en) | 1993-09-29 | 2001-01-02 | Rhone Poulenc Chimie | Precipitated silica |
| DE19526476A1 (de) | 1995-07-20 | 1997-01-23 | Degussa | Fällungskieselsäure |
| FR2763581B1 (fr) * | 1997-05-26 | 1999-07-23 | Rhodia Chimie Sa | Silice precipitee utilisable comme charge renforcante pour elastomeres |
| AU2002211736A1 (en) | 2000-10-13 | 2002-04-22 | University Of Cincinnati | Methods for synthesizing precipitated silica and use thereof |
| FR2818966B1 (fr) * | 2000-12-28 | 2003-03-07 | Rhodia Chimie Sa | Procede de preparation de silice precipitee contenant de l'aluminium |
| ES2610590T3 (es) * | 2001-08-13 | 2017-04-28 | Rhodia Chimie | Procedimiento de preparación de sílices con distribución granulométrica y/o reparto de poros particulares |
| US6869595B2 (en) * | 2001-12-21 | 2005-03-22 | J.M. Huber Corporation | Abrasive compositions for clear toothpaste |
| FR2902781B1 (fr) * | 2006-06-27 | 2008-09-05 | Rhodia Recherches Et Technologies Sas | Silice precipitee pour application papier |
| CN102137813A (zh) | 2008-09-01 | 2011-07-27 | 赢创德固赛有限责任公司 | 制备沉淀二氧化硅的方法、沉淀二氧化硅及其用途 |
| FR2949455B1 (fr) * | 2009-09-03 | 2011-09-16 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2962996B1 (fr) | 2010-07-23 | 2012-07-27 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2984870B1 (fr) | 2011-12-23 | 2014-03-21 | Rhodia Operations | Nouveau procede de preparation de silices precipitees. |
| RU2607741C2 (ru) | 2011-12-23 | 2017-01-10 | Родиа Операсьон | Новый способ получения диоксидов кремния |
| FR2985991B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2985993B1 (fr) | 2012-01-25 | 2014-11-28 | Rhodia Operations | Nouveau procede de preparation de silices precipitees |
| FR2985992B1 (fr) | 2012-01-25 | 2015-03-06 | Rhodia Operations | Nouveau procede de preparation de silices precitees |
-
2012
- 2012-01-25 FR FR1200211A patent/FR2985990B1/fr not_active Expired - Fee Related
-
2013
- 2013-01-23 CN CN201380006522.6A patent/CN104066681B/zh not_active Expired - Fee Related
- 2013-01-23 WO PCT/EP2013/051233 patent/WO2013110654A1/fr not_active Ceased
- 2013-01-23 CA CA2862467A patent/CA2862467A1/fr not_active Abandoned
- 2013-01-23 EP EP13700923.9A patent/EP2807115B1/fr active Active
- 2013-01-23 RU RU2014134460/05A patent/RU2578309C1/ru not_active IP Right Cessation
- 2013-01-23 AU AU2013211586A patent/AU2013211586A1/en not_active Abandoned
- 2013-01-23 MX MX2014008999A patent/MX353387B/es active IP Right Grant
- 2013-01-23 BR BR112014017994A patent/BR112014017994A8/pt not_active Application Discontinuation
- 2013-01-23 KR KR1020147023312A patent/KR20140116530A/ko not_active Abandoned
- 2013-01-23 US US14/373,791 patent/US9695053B2/en not_active Expired - Fee Related
- 2013-01-24 TW TW102102714A patent/TWI490165B/zh not_active IP Right Cessation
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101970354A (zh) * | 2008-03-10 | 2011-02-09 | 罗地亚管理公司 | 制备沉淀二氧化硅的新方法,具有特殊的形态、粒度和孔隙率的沉淀二氧化硅及其用途,尤其用于增强聚合物 |
Also Published As
| Publication number | Publication date |
|---|---|
| MX2014008999A (es) | 2015-02-10 |
| KR20140116530A (ko) | 2014-10-02 |
| TWI490165B (zh) | 2015-07-01 |
| EP2807115A1 (fr) | 2014-12-03 |
| US20150030518A1 (en) | 2015-01-29 |
| WO2013110654A1 (fr) | 2013-08-01 |
| CA2862467A1 (fr) | 2013-08-01 |
| US9695053B2 (en) | 2017-07-04 |
| RU2578309C1 (ru) | 2016-03-27 |
| FR2985990A1 (fr) | 2013-07-26 |
| EP2807115B1 (fr) | 2020-04-08 |
| BR112014017994A2 (enExample) | 2017-06-20 |
| MX353387B (es) | 2018-01-10 |
| AU2013211586A1 (en) | 2014-08-21 |
| BR112014017994A8 (pt) | 2017-07-11 |
| CN104066681A (zh) | 2014-09-24 |
| FR2985990B1 (fr) | 2014-11-28 |
| TW201343551A (zh) | 2013-11-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180424 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |