CN104024945B - 化学制备的包含硼砂偶联剂的调色剂制剂 - Google Patents
化学制备的包含硼砂偶联剂的调色剂制剂 Download PDFInfo
- Publication number
- CN104024945B CN104024945B CN201280065435.3A CN201280065435A CN104024945B CN 104024945 B CN104024945 B CN 104024945B CN 201280065435 A CN201280065435 A CN 201280065435A CN 104024945 B CN104024945 B CN 104024945B
- Authority
- CN
- China
- Prior art keywords
- toner
- weight
- mixture
- polymer adhesive
- core
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 235000010339 sodium tetraborate Nutrition 0.000 title claims abstract description 61
- 229910021538 borax Inorganic materials 0.000 title claims abstract description 56
- 239000004328 sodium tetraborate Substances 0.000 title claims abstract description 55
- 239000007822 coupling agent Substances 0.000 title claims abstract description 46
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 239000000126 substance Substances 0.000 title claims abstract description 19
- 239000000203 mixture Substances 0.000 title claims description 76
- 238000009472 formulation Methods 0.000 title description 12
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 70
- 229920000642 polymer Polymers 0.000 claims abstract description 61
- 239000000853 adhesive Substances 0.000 claims abstract description 43
- 230000001070 adhesive effect Effects 0.000 claims abstract description 43
- 238000004040 coloring Methods 0.000 claims abstract description 21
- 238000004519 manufacturing process Methods 0.000 claims abstract description 16
- 239000004645 polyester resin Substances 0.000 claims description 54
- 229920001225 polyester resin Polymers 0.000 claims description 54
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 13
- 125000000524 functional group Chemical group 0.000 claims description 10
- 150000001875 compounds Chemical class 0.000 claims description 6
- 239000010419 fine particle Substances 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 2
- 239000000839 emulsion Substances 0.000 description 98
- 239000002245 particle Substances 0.000 description 88
- 229920000728 polyester Polymers 0.000 description 54
- 239000002253 acid Substances 0.000 description 43
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 36
- 229920005989 resin Polymers 0.000 description 36
- 239000011347 resin Substances 0.000 description 36
- 239000007787 solid Substances 0.000 description 36
- 230000002776 aggregation Effects 0.000 description 35
- 238000004220 aggregation Methods 0.000 description 34
- 230000000052 comparative effect Effects 0.000 description 33
- 230000004927 fusion Effects 0.000 description 31
- 239000006185 dispersion Substances 0.000 description 29
- 239000000049 pigment Substances 0.000 description 27
- 238000000034 method Methods 0.000 description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 25
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 20
- -1 dichloromethane Alkane Chemical class 0.000 description 17
- 239000002270 dispersing agent Substances 0.000 description 17
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 15
- 239000011230 binding agent Substances 0.000 description 15
- 239000001993 wax Substances 0.000 description 15
- 238000007639 printing Methods 0.000 description 14
- 238000012360 testing method Methods 0.000 description 14
- 239000008367 deionised water Substances 0.000 description 13
- 229910021641 deionized water Inorganic materials 0.000 description 13
- 230000009477 glass transition Effects 0.000 description 12
- 238000006243 chemical reaction Methods 0.000 description 11
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 9
- 239000003086 colorant Substances 0.000 description 8
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 8
- 229910000368 zinc sulfate Inorganic materials 0.000 description 8
- 229960001763 zinc sulfate Drugs 0.000 description 8
- 230000029219 regulation of pH Effects 0.000 description 7
- 230000003678 scratch resistant effect Effects 0.000 description 7
- 239000000654 additive Substances 0.000 description 6
- 239000000084 colloidal system Substances 0.000 description 6
- 239000000178 monomer Substances 0.000 description 6
- 230000001681 protective effect Effects 0.000 description 6
- 239000004094 surface-active agent Substances 0.000 description 6
- 239000002202 Polyethylene glycol Substances 0.000 description 5
- 238000005755 formation reaction Methods 0.000 description 5
- 239000004816 latex Substances 0.000 description 5
- 229920000126 latex Polymers 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 230000003472 neutralizing effect Effects 0.000 description 5
- 239000003960 organic solvent Substances 0.000 description 5
- 229920001223 polyethylene glycol Polymers 0.000 description 5
- 150000003839 salts Chemical class 0.000 description 5
- 239000003381 stabilizer Substances 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- WAKTWVHWRCNIKU-UHFFFAOYSA-N S(=O)(=O)(O)O.[AlH3] Chemical compound S(=O)(=O)(O)O.[AlH3] WAKTWVHWRCNIKU-UHFFFAOYSA-N 0.000 description 4
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 4
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 4
- 230000000996 additive effect Effects 0.000 description 4
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 238000009826 distribution Methods 0.000 description 4
- 238000006116 polymerization reaction Methods 0.000 description 4
- 238000007790 scraping Methods 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 125000000129 anionic group Chemical group 0.000 description 3
- 239000003945 anionic surfactant Substances 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000005189 flocculation Methods 0.000 description 3
- 230000016615 flocculation Effects 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000005012 migration Effects 0.000 description 3
- 238000013508 migration Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 229920001909 styrene-acrylic polymer Polymers 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- 239000002250 absorbent Substances 0.000 description 2
- 230000002745 absorbent Effects 0.000 description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical class C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 2
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 2
- 125000002091 cationic group Chemical group 0.000 description 2
- 238000004132 cross linking Methods 0.000 description 2
- YMWUJEATGCHHMB-UHFFFAOYSA-N dichloromethane Natural products ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 230000002209 hydrophobic effect Effects 0.000 description 2
- 229910052738 indium Inorganic materials 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 2
- 229910052753 mercury Inorganic materials 0.000 description 2
- 239000004014 plasticizer Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000006641 stabilisation Effects 0.000 description 2
- 238000011105 stabilization Methods 0.000 description 2
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- JYEUMXHLPRZUAT-UHFFFAOYSA-N 1,2,3-triazine Chemical compound C1=CN=NN=C1 JYEUMXHLPRZUAT-UHFFFAOYSA-N 0.000 description 1
- OTEKOJQFKOIXMU-UHFFFAOYSA-N 1,4-bis(trichloromethyl)benzene Chemical compound ClC(Cl)(Cl)C1=CC=C(C(Cl)(Cl)Cl)C=C1 OTEKOJQFKOIXMU-UHFFFAOYSA-N 0.000 description 1
- FKKAGFLIPSSCHT-UHFFFAOYSA-N 1-dodecoxydodecane;sulfuric acid Chemical class OS(O)(=O)=O.CCCCCCCCCCCCOCCCCCCCCCCCC FKKAGFLIPSSCHT-UHFFFAOYSA-N 0.000 description 1
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 1
- OELQSSWXRGADDE-UHFFFAOYSA-N 2-methylprop-2-eneperoxoic acid Chemical compound CC(=C)C(=O)OO OELQSSWXRGADDE-UHFFFAOYSA-N 0.000 description 1
- WVRNUXJQQFPNMN-VAWYXSNFSA-N 3-[(e)-dodec-1-enyl]oxolane-2,5-dione Chemical compound CCCCCCCCCC\C=C\C1CC(=O)OC1=O WVRNUXJQQFPNMN-VAWYXSNFSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 229930185605 Bisphenol Natural products 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 239000006173 Good's buffer Substances 0.000 description 1
- FZERHIULMFGESH-UHFFFAOYSA-N N-phenylacetamide Chemical compound CC(=O)NC1=CC=CC=C1 FZERHIULMFGESH-UHFFFAOYSA-N 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 239000002174 Styrene-butadiene Substances 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 239000004840 adhesive resin Substances 0.000 description 1
- 229920006223 adhesive resin Polymers 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 150000008052 alkyl sulfonates Chemical class 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 239000000908 ammonium hydroxide Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229920006318 anionic polymer Polymers 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- MTAZNLWOLGHBHU-UHFFFAOYSA-N butadiene-styrene rubber Chemical compound C=CC=C.C=CC1=CC=CC=C1 MTAZNLWOLGHBHU-UHFFFAOYSA-N 0.000 description 1
- 238000007707 calorimetry Methods 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 239000004203 carnauba wax Substances 0.000 description 1
- 235000013869 carnauba wax Nutrition 0.000 description 1
- 238000010538 cationic polymerization reaction Methods 0.000 description 1
- 238000004581 coalescence Methods 0.000 description 1
- 229920000891 common polymer Polymers 0.000 description 1
- 230000001143 conditioned effect Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- UQGFMSUEHSUPRD-UHFFFAOYSA-N disodium;3,7-dioxido-2,4,6,8,9-pentaoxa-1,3,5,7-tetraborabicyclo[3.3.1]nonane Chemical compound [Na+].[Na+].O1B([O-])OB2OB([O-])OB1O2 UQGFMSUEHSUPRD-UHFFFAOYSA-N 0.000 description 1
- AJFXNBUVIBKWBT-UHFFFAOYSA-N disodium;boric acid;hydrogen borate Chemical compound [Na+].[Na+].OB(O)O.OB(O)O.OB(O)O.OB([O-])[O-] AJFXNBUVIBKWBT-UHFFFAOYSA-N 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 239000005007 epoxy-phenolic resin Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000005562 fading Methods 0.000 description 1
- 239000001530 fumaric acid Substances 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 229920000578 graft copolymer Polymers 0.000 description 1
- 229920001519 homopolymer Polymers 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 150000001261 hydroxy acids Chemical group 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 150000007529 inorganic bases Chemical class 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 230000000670 limiting effect Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 150000004291 polyenes Chemical class 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 229920000570 polyether Polymers 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- 238000002310 reflectometry Methods 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- DCKVNWZUADLDEH-UHFFFAOYSA-N sec-butyl acetate Chemical compound CCC(C)OC(C)=O DCKVNWZUADLDEH-UHFFFAOYSA-N 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000003019 stabilising effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000011115 styrene butadiene Substances 0.000 description 1
- 229920003048 styrene butadiene rubber Polymers 0.000 description 1
- 150000003440 styrenes Chemical class 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 230000000930 thermomechanical effect Effects 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- SRPWOOOHEPICQU-UHFFFAOYSA-N trimellitic anhydride Chemical compound OC(=O)C1=CC=C2C(=O)OC(=O)C2=C1 SRPWOOOHEPICQU-UHFFFAOYSA-N 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 238000004017 vitrification Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/093—Encapsulated toner particles
- G03G9/09392—Preparation thereof
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/093—Encapsulated toner particles
- G03G9/09307—Encapsulated toner particles specified by the shell material
- G03G9/09314—Macromolecular compounds
- G03G9/09328—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/093—Encapsulated toner particles
- G03G9/0935—Encapsulated toner particles specified by the core material
- G03G9/09357—Macromolecular compounds
- G03G9/09371—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/093—Encapsulated toner particles
- G03G9/0935—Encapsulated toner particles specified by the core material
- G03G9/09385—Inorganic compounds
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Inorganic Chemistry (AREA)
- Developing Agents For Electrophotography (AREA)
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US13/339,565 | 2011-12-29 | ||
US13/339,705 | 2011-12-29 | ||
US13/339,565 US8669035B2 (en) | 2011-12-29 | 2011-12-29 | Process for preparing toner including a borax coupling agent |
US13/339,705 US9023569B2 (en) | 2011-12-29 | 2011-12-29 | Chemically prepared toner formulation including a borax coupling agent |
PCT/US2012/071932 WO2013101995A1 (en) | 2011-12-29 | 2012-12-28 | Chemically prepared toner formulation including a borax coupling agent |
Publications (2)
Publication Number | Publication Date |
---|---|
CN104024945A CN104024945A (zh) | 2014-09-03 |
CN104024945B true CN104024945B (zh) | 2017-08-04 |
Family
ID=48698629
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201280065435.3A Active CN104024945B (zh) | 2011-12-29 | 2012-12-28 | 化学制备的包含硼砂偶联剂的调色剂制剂 |
CN201280065216.5A Active CN104024944B (zh) | 2011-12-29 | 2012-12-28 | 用于制备包含硼砂偶联剂的调色剂的方法 |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201280065216.5A Active CN104024944B (zh) | 2011-12-29 | 2012-12-28 | 用于制备包含硼砂偶联剂的调色剂的方法 |
Country Status (13)
Country | Link |
---|---|
EP (3) | EP2798404A4 (es) |
JP (2) | JP6059251B2 (es) |
CN (2) | CN104024945B (es) |
AU (2) | AU2012362372B2 (es) |
BR (2) | BR112014015643B1 (es) |
CA (2) | CA2858392C (es) |
CL (2) | CL2014001687A1 (es) |
CO (2) | CO6990704A2 (es) |
HK (3) | HK1203641A1 (es) |
IN (2) | IN2014DN05929A (es) |
MX (2) | MX349651B (es) |
WO (2) | WO2013101995A1 (es) |
ZA (2) | ZA201404263B (es) |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1449929A (zh) * | 2002-04-09 | 2003-10-22 | 伊斯曼柯达公司 | 使用稳定化聚合物颗粒的墨打印方法 |
CN101231480A (zh) * | 2007-01-25 | 2008-07-30 | 京瓷美达株式会社 | 调色剂、调色剂的制造方法以及图像形成装置 |
Family Cites Families (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS603647A (ja) * | 1983-06-22 | 1985-01-10 | Fuji Xerox Co Ltd | マイクロカプセルトナ− |
JPS63264367A (ja) * | 1987-04-23 | 1988-11-01 | Canon Inc | 記録方法および記録装置 |
US5714538A (en) | 1995-12-26 | 1998-02-03 | Lexmark International, Inc. | Polymeric dispersants for pigmented inks |
GB9708815D0 (en) | 1997-05-01 | 1997-06-25 | Zeneca Ltd | Process for making particulate compositions |
JPH10330466A (ja) * | 1997-06-04 | 1998-12-15 | Polyplastics Co | ポリエステル樹脂の製造法 |
GB9806934D0 (en) | 1998-04-01 | 1998-05-27 | Zeneca Ltd | Process for making particulate compositions |
JP3721915B2 (ja) * | 2000-02-02 | 2005-11-30 | 日本ゼオン株式会社 | 電子写真用現像剤、その製法及び該現像剤を用いた画像形成方法 |
JP4207383B2 (ja) * | 2000-12-25 | 2009-01-14 | 日本ゼオン株式会社 | トナーの製造方法 |
JP2002278150A (ja) * | 2001-03-22 | 2002-09-27 | Nippon Zeon Co Ltd | トナーの製造方法 |
US6991884B2 (en) | 2001-08-03 | 2006-01-31 | Lexmark International, Inc. | Chemically prepared toner and process therefor |
JP2003295510A (ja) * | 2002-03-28 | 2003-10-15 | Nippon Zeon Co Ltd | トナーの製造方法 |
JP4192717B2 (ja) * | 2002-11-29 | 2008-12-10 | 富士ゼロックス株式会社 | 静電荷像現像用トナー、並びに、これを用いた静電荷像現像剤及び画像形成方法 |
WO2005001579A1 (ja) * | 2003-03-17 | 2005-01-06 | Zeon Corporation | 静電荷像現像用トナー |
JP2004279771A (ja) * | 2003-03-17 | 2004-10-07 | Nippon Zeon Co Ltd | 静電荷像現像用トナー |
JP4111035B2 (ja) * | 2003-03-31 | 2008-07-02 | 日本ゼオン株式会社 | 重合トナーの製造方法 |
JP2005301061A (ja) * | 2004-04-14 | 2005-10-27 | Seiko Epson Corp | トナー用粒子の製造方法 |
JP2007121946A (ja) * | 2005-10-31 | 2007-05-17 | Nippon Zeon Co Ltd | 静電荷像現像用トナー |
US7939236B2 (en) | 2007-02-22 | 2011-05-10 | Lexmark International, Inc. | Chemically prepared toner and process therefor |
JP4964834B2 (ja) * | 2007-06-29 | 2012-07-04 | 三洋化成工業株式会社 | 樹脂粒子 |
US20090011352A1 (en) * | 2007-07-02 | 2009-01-08 | John Francis Cooper | Process for preparing novel composite imaging materials and novel composite imaging materials prepared by the process |
US7923191B2 (en) * | 2007-07-26 | 2011-04-12 | Lexmark International, Inc. | Polyester resin toner produced by emulsion aggregation |
JP2010160451A (ja) * | 2009-01-09 | 2010-07-22 | Sharp Corp | トナー、二成分現像剤、現像装置および画像形成装置 |
US8377619B2 (en) * | 2009-07-03 | 2013-02-19 | Konica Minolta Business Technologies, Inc. | Toner and toner manufacturing method |
JP5227929B2 (ja) * | 2009-09-28 | 2013-07-03 | シャープ株式会社 | カプセルトナーの製造方法 |
US8715897B2 (en) * | 2009-11-16 | 2014-05-06 | Xerox Corporation | Toner compositions |
US7977025B2 (en) * | 2009-12-03 | 2011-07-12 | Xerox Corporation | Emulsion aggregation methods |
JP2012047914A (ja) * | 2010-08-25 | 2012-03-08 | Fuji Xerox Co Ltd | 静電荷像現像用トナー、静電荷像現像剤、画像形成方法、トナーカートリッジ、プロセスカートリッジ、及び画像形成装置 |
-
2012
- 2012-12-28 AU AU2012362372A patent/AU2012362372B2/en active Active
- 2012-12-28 CA CA2858392A patent/CA2858392C/en active Active
- 2012-12-28 BR BR112014015643-3A patent/BR112014015643B1/pt active IP Right Grant
- 2012-12-28 WO PCT/US2012/071932 patent/WO2013101995A1/en active Application Filing
- 2012-12-28 CN CN201280065435.3A patent/CN104024945B/zh active Active
- 2012-12-28 CN CN201280065216.5A patent/CN104024944B/zh active Active
- 2012-12-28 JP JP2014550487A patent/JP6059251B2/ja active Active
- 2012-12-28 MX MX2014007713A patent/MX349651B/es active IP Right Grant
- 2012-12-28 EP EP12863957.2A patent/EP2798404A4/en active Pending
- 2012-12-28 JP JP2014550489A patent/JP6077567B2/ja active Active
- 2012-12-28 EP EP12863417.7A patent/EP2798403A4/en active Pending
- 2012-12-28 EP EP15161170.4A patent/EP2919069A1/en active Pending
- 2012-12-28 AU AU2012362368A patent/AU2012362368B2/en active Active
- 2012-12-28 CA CA2858396A patent/CA2858396C/en active Active
- 2012-12-28 BR BR112014016235-2A patent/BR112014016235B1/pt active IP Right Grant
- 2012-12-28 IN IN5929DEN2014 patent/IN2014DN05929A/en unknown
- 2012-12-28 WO PCT/US2012/071926 patent/WO2013101991A1/en active Application Filing
- 2012-12-28 IN IN5924DEN2014 patent/IN2014DN05924A/en unknown
- 2012-12-28 MX MX2014007718A patent/MX348569B/es active IP Right Grant
-
2014
- 2014-06-10 ZA ZA2014/04263A patent/ZA201404263B/en unknown
- 2014-06-10 ZA ZA2014/04264A patent/ZA201404264B/en unknown
- 2014-06-20 CO CO14134581A patent/CO6990704A2/es unknown
- 2014-06-20 CO CO14134601A patent/CO6990743A2/es unknown
- 2014-06-23 CL CL2014001687A patent/CL2014001687A1/es unknown
- 2014-06-23 CL CL2014001691A patent/CL2014001691A1/es unknown
-
2015
- 2015-05-05 HK HK15104290.2A patent/HK1203641A1/xx unknown
- 2015-05-05 HK HK15104292.0A patent/HK1203642A1/xx unknown
-
2016
- 2016-03-10 HK HK16102761.5A patent/HK1214867A1/zh unknown
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1449929A (zh) * | 2002-04-09 | 2003-10-22 | 伊斯曼柯达公司 | 使用稳定化聚合物颗粒的墨打印方法 |
CN101231480A (zh) * | 2007-01-25 | 2008-07-30 | 京瓷美达株式会社 | 调色剂、调色剂的制造方法以及图像形成装置 |
Also Published As
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US9023569B2 (en) | Chemically prepared toner formulation including a borax coupling agent | |
US9612544B2 (en) | Electrostatic image developing toner | |
US8669035B2 (en) | Process for preparing toner including a borax coupling agent | |
JP2014164274A (ja) | 静電荷像現像用トナー | |
JP6019919B2 (ja) | 液体現像剤、現像剤カートリッジ、プロセスカートリッジ、画像形成装置および画像形成方法 | |
JP4998216B2 (ja) | 静電荷像現像用トナーの製造方法 | |
KR101545903B1 (ko) | 정전화상 현상용 토너 및 그의 제조방법 | |
CN104024945B (zh) | 化学制备的包含硼砂偶联剂的调色剂制剂 | |
US10108101B2 (en) | Toner formulation using crystalline polyester encapsulated with a styrene acrylate latex and method of preparing the same | |
US10133202B2 (en) | Toner formulation having a silane surface treated on its outer surface and method of preparing the same | |
US10133203B2 (en) | Toner formulation having a silane surface treated on its outer surface and method of preparing the same | |
US9733582B2 (en) | Toner formulation using wax encapsulated with a styrene acrylate latex formulation and method of preparing the same | |
US20170131651A1 (en) | Toner formulation using crystalline polyester encapsulated with a styrene acrylate latex formulation and method of preparing the same | |
JP2017182056A (ja) | 画像形成方法及び画像形成装置 | |
US9798261B2 (en) | Toner formulation using wax encapsulated with a styrene acrylate latex and method of preparing the same | |
WO2014112488A1 (ja) | 樹脂粒子分散液の製造方法及び静電荷像現像用トナーの製造方法 | |
JP5885632B2 (ja) | 静電潜像現像用トナーの製造方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant |