CN104004176B - 制备聚醚多元醇的方法 - Google Patents

制备聚醚多元醇的方法 Download PDF

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Publication number
CN104004176B
CN104004176B CN201410058928.5A CN201410058928A CN104004176B CN 104004176 B CN104004176 B CN 104004176B CN 201410058928 A CN201410058928 A CN 201410058928A CN 104004176 B CN104004176 B CN 104004176B
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CN
China
Prior art keywords
weight
ethylene oxide
reaction
koh
block
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CN201410058928.5A
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English (en)
Chinese (zh)
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CN104004176A (zh
Inventor
K.洛伦茨
M.艾希曼
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Covestro Deutschland AG
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Bayer MaterialScience AG
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Publication of CN104004176A publication Critical patent/CN104004176A/zh
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Expired - Fee Related legal-status Critical Current
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/487—Polyethers containing cyclic groups
    • C08G18/4883—Polyethers containing cyclic groups containing cyclic groups having at least one oxygen atom in the ring
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
    • C08G65/2609—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/30—Post-polymerisation treatment, e.g. recovery, purification, drying
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/02—Acyclic radicals, not substituted by cyclic structures
    • C07H15/04—Acyclic radicals, not substituted by cyclic structures attached to an oxygen atom of the saccharide radical
    • C07H15/08—Polyoxyalkylene derivatives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2650/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G2650/22—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the initiator used in polymerisation
    • C08G2650/26—Sugars or saccharides used as initiators
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyethers (AREA)
  • Polyurethanes Or Polyureas (AREA)
CN201410058928.5A 2013-02-22 2014-02-21 制备聚醚多元醇的方法 Expired - Fee Related CN104004176B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP13156343.9 2013-02-22
EP13156343 2013-02-22

Publications (2)

Publication Number Publication Date
CN104004176A CN104004176A (zh) 2014-08-27
CN104004176B true CN104004176B (zh) 2018-05-25

Family

ID=47748512

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410058928.5A Expired - Fee Related CN104004176B (zh) 2013-02-22 2014-02-21 制备聚醚多元醇的方法

Country Status (8)

Country Link
US (1) US9006499B2 (enExample)
EP (1) EP2770009B1 (enExample)
JP (1) JP2014162924A (enExample)
KR (1) KR20140105401A (enExample)
CN (1) CN104004176B (enExample)
BR (1) BR102014003800A2 (enExample)
MX (1) MX337785B (enExample)
SG (1) SG2014013254A (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SG2014014567A (en) * 2013-02-22 2014-09-26 Bayer Materialscience Ag Process for preparing polyether polyols
RU2641304C1 (ru) * 2016-11-02 2018-01-17 федеральное государственное автономное образовательное учреждение высшего образования "Казанский (Приволжский) федеральный университет" (ФГАОУ ВО КФУ) Ингибитор атф-зависимых обратных транспортеров клеток и способ его получения
CN109134804B (zh) 2016-12-19 2021-10-22 科思创德国股份有限公司 聚氨酯水性分散体
CN112513122B (zh) 2018-06-15 2022-11-15 科思创知识产权两合公司 涂料组合物
EP3599254A1 (en) 2018-07-23 2020-01-29 Covestro Deutschland AG Coating composition
US10633406B1 (en) 2018-11-15 2020-04-28 Covestro Llc Water processes for producing polyether polyols from solid polyhydroxyl compounds
CN113667111A (zh) * 2021-08-31 2021-11-19 山东一诺威新材料有限公司 山梨醇基高分子量聚醚多元醇的制备方法

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2902478A (en) 1957-05-09 1959-09-01 Dow Chemical Co Oxyalkylation of solid polyols
US3190927A (en) 1960-04-13 1965-06-22 Wyandotte Chemicals Corp Process for oxyalkylating solid polyols
US3085085A (en) 1960-05-03 1963-04-09 Pittsburgh Plate Glass Co Method of preparing polyethers of mono and disaccharides
FR1285708A (fr) 1961-04-05 1962-02-23 Wyandotte Chemicals Corp Perfectionnements apportés aux procédés pour l'oxyalcoylation de polyols normalement solides et aux polyols oxyalcoylés ainsi obtenus
US3823145A (en) 1968-07-26 1974-07-09 Basf Wyandotte Corp Removal of impurities from polyols
US4332936A (en) 1978-10-16 1982-06-01 Mobay Chemical Corporation Method of making polyether polyols from solid hydroxyl containing initiators
DE3229216A1 (de) 1982-08-05 1984-02-09 Basf Ag, 6700 Ludwigshafen Verfahren zur reinigung von rohen polyether-polyolen
US4430490A (en) 1982-08-10 1984-02-07 Ppg Industries, Inc. Polyether polyols and their method of preparation
US4521548A (en) 1983-04-12 1985-06-04 The Dow Chemical Company Preparation of polyether polyols
JPH07113060B2 (ja) * 1988-02-09 1995-12-06 日本ペイント株式会社 ポリエーテルポリオールの製法
JP3263450B2 (ja) 1992-11-27 2002-03-04 三井化学株式会社 粗ポリオキシプロピレンポリオールの精製方法
DE4310504A1 (de) * 1993-03-31 1994-10-06 Bayer Ag Niedrigviskose, hochfunktionelle, helle Polyether auf Saccharose-Basis
JP3981162B2 (ja) 1994-07-18 2007-09-26 旭硝子株式会社 ポリエーテルの製造方法
WO1996020972A2 (en) 1995-01-05 1996-07-11 Bayer Corporation A PROCESS FOR THE REMOVAL OF A pH-BASIC MATERIAL FROM A POLYETHER POLYOL
US5786405A (en) 1996-11-01 1998-07-28 Bayer Corporation Amine-initiated polyether polyols and a process for their production
US6376625B1 (en) 1999-08-25 2002-04-23 The Dow Chemical Company Process for purifying polyethers
RO118433B1 (ro) 2000-03-03 2003-05-30 Sc Oltchim Sa Procedeu de obtinere a polieterilor polioli, pe baza de zaharoza, pentru spume poliuretanice rigide
DE10024313A1 (de) 2000-05-17 2001-11-22 Basf Ag Verfahren zur Abtrennung von Alkalimetallionen aus Alkoxylaten
US6869543B2 (en) 2003-02-21 2005-03-22 Bayer Polymers Llc Amine-initiated polyether polyols and a process for their production
US6962967B2 (en) 2004-03-31 2005-11-08 Basf Corporation Method of purifying polyether polyols of non-volatile impurities
DE102006024025A1 (de) * 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Herstellung von Polyetherpolyolen
DE102007038436A1 (de) 2007-08-16 2009-02-19 Bayer Materialscience Ag Verfahren zur Herstellung von Polyolen
DE102008011683A1 (de) 2008-02-28 2009-09-03 Bayer Materialscience Ag Verfahren zur Herstellung von Polyolen
DE102008028555A1 (de) 2008-06-16 2009-12-17 Bayer Materialscience Ag Verfahren zur Herstellung von Polyolen
DE102009043616A1 (de) 2009-09-29 2011-03-31 Bayer Materialscience Ag Verfahren zur Herstellung von aminogruppenhaltigen Polyolen

Also Published As

Publication number Publication date
US20140243559A1 (en) 2014-08-28
JP2014162924A (ja) 2014-09-08
SG2014013254A (en) 2014-09-26
BR102014003800A2 (pt) 2020-07-21
EP2770009A1 (de) 2014-08-27
US9006499B2 (en) 2015-04-14
CN104004176A (zh) 2014-08-27
EP2770009B1 (de) 2016-04-06
MX337785B (es) 2016-03-18
MX2014001673A (es) 2014-09-03
KR20140105401A (ko) 2014-09-01

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Address after: Germany Leverkusen

Applicant after: COVESTRO DEUTSCHLAND AG

Address before: Germany Leverkusen

Applicant before: BAYER MATERIALSCIENCE AG

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Granted publication date: 20180525