CN103788874A - Ginseng seed treatment agent and preparation method thereof - Google Patents
Ginseng seed treatment agent and preparation method thereof Download PDFInfo
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- CN103788874A CN103788874A CN201210433551.8A CN201210433551A CN103788874A CN 103788874 A CN103788874 A CN 103788874A CN 201210433551 A CN201210433551 A CN 201210433551A CN 103788874 A CN103788874 A CN 103788874A
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- wax
- treatment agent
- seed treatment
- ginseng seed
- ginseng
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Abstract
The invention discloses a ginseng seed treatment agent and a preparation method thereof. The ginseng seed treatment agent is an emulsion prepared from a wax substance, a moisturizing agent, fatty acid, a bactericide, a surfactant and distilled water. The preparation method includes: preparing a substance A, an oil phase substance and a water phase substance respectively, and then performing mixing dispersion emulsification, thus obtaining the final ginseng seed treatment agent. Applying the treatment agent provided by the invention to ginseng seeds can inhibit transpiration of water in the ginseng seeds so as to make the seeds contain enough water, promote early maturing of the seeds, and reduce the ripening and seedling raising time of the ginseng seeds.
Description
Technical field
The invention belongs to plant growing field, particularly relate to a kind of ginseng seed treatment agent, be applicable to the seed treatment of panax ginseng in jiljn, Radix Ginseng's (having another name called: Radix Ginseng, not directly ginseng) and Radix Panacis Quinquefolii.
Background technology
In recent years, along with the increase of scientific and technical progress, material and economic capability, improving constantly of living standards of the people, people are also constantly increasing the conciliation supply of quality of life and health, demand to various natural tonics and quality are also being on the increase raising, and the rare medicinal herbs class tonics such as ginseng, Winter-Spring summer grass, cynomorium songaricum have entered among the daily life of ordinary people.But natural ginseng, because being subject to the increase of mankind's activity scope, has become fewer and feweri, and the ginseng of perennial high-quality is even very rare.People start artificial culture plantation ginseng for this reason, and along with the grasp of artificial culture plantation ginseng technology improves, artificial culture plantation ginseng is very general, and economic benefit is also considerable.But in artificial culture of ginseng planting process, because ginseng seed has embryo after-ripening, two processes of physiology after-ripening, complete the certain temperature of this process need, humidity condition, its seed treatment is cumbersome work, improve raising ginseng seed treatment technology and seem particularly important in culture of ginseng plantation, new technological invention research also has certain importance.Ginseng seed processing is at present traditional method of accelerating the ripening of watering, and also there is no special preparation for ginseng seed processing.The disclosed a kind of seed treatment of Chinese patent CN12288661 is processed and all be there is no desirable effect for ginseng seed by the patent of invention of Wax emulsion and preparation and application and other various preparations for plant seed processing.
Summary of the invention
For the deficiencies in the prior art, the invention provides a kind of ginseng seed treatment agent, for the treatment of ginseng seed.
The invention provides a kind of ginseng seed treatment agent, comprise in mass
Wax 6%~10%
Wetting Agent for Printing Inks 4%~8%
Lipid acid 6%~12%
Sterilant 0.1%~2.0%
Tensio-active agent 6%~8%
Distilled water surplus.
A kind of ginseng seed treatment agent of the present invention, wherein said Wax is one or more in vegetable wax, animal wax, oxidized petroleum wax.Described vegetable wax is one or more in carnauba wax (Ka Naba wax), gama wax, rice bran wax, sugar-cane wax, laurel wax, Semen Ricini wax, lacquer tree fat, George Simond haze tallow, ouricury wax, Pseudotsuga menziesii (Mirbel) Franco wax, described animal wax is one or more in beeswax, wool wax, insect wax, spermaceti, and described oxidized petroleum wax is 60~No. 70 oxidized petroleum waxs.
A kind of ginseng seed treatment agent of the present invention, wherein said lipid acid is chain saturated fatty acids, can be stearic acid and/or Palmiticacid.
A kind of ginseng seed treatment agent of the present invention, wherein said wetting Agent for Printing Inks is dibasic alcohol and/or polyvalent alcohol.
A kind of ginseng seed treatment agent of the present invention, wherein said tensio-active agent is anion surfactant and/or nonionic surface active agent, wherein, anion surfactant can be one or more in morpholine, Sodium dodecylbenzene sulfonate and sodium lauryl sulphate, and nonionic surface active agent can be one or more in fatty alcohol-polyoxyethylene ether, polyoxyethylene carboxylate, alkylphenol polyoxyethylene.
A kind of ginseng seed treatment agent of the present invention, wherein said sterilant is metconazole or cyazofamid.
The preparation method of ginseng seed treatment agent of the present invention comprises the steps:
(1) take wetting Agent for Printing Inks according to proportioning and lipid acid joins in container, be heated to 115~145 ℃, reaction 205~245min, obtains A material;
(2) take Wax according to proportioning and join in reactor, be heated to 115~145 ℃, then the A material obtaining in step (1) is joined in reactor, at 115~145 ℃, stirring reaction 20~50min, obtains oil phase substance;
(3) according to proportioning, tensio-active agent is joined in distilled water, be heated to 80~96 ℃, obtain aqueous phase substance;
(4) gained oil phase substance in step (2) is joined under high-speed stirring condition to mixing and emulsifying in the aqueous phase substance of gained in step (3), after emulsification completes at 93~97 ℃ of temperature, stir constant 30~50min, adding sterilant to stir 8~22min according to proportioning, cool to 38~52 ℃ through homogenizer, be final treatment agent product.
The present invention selects Wax, lipid acid and wetting Agent for Printing Inks as ginseng seed treatment agent main component; the reactant that is characterized in Wax, lipid acid and wetting Agent for Printing Inks sticks to ginseng seed surface; form hydrophobicity protective layer; can suppress the moisture transpiration in ginseng seed; make seed contain short enough moisture; impel seed precocity, reduce the ginseng seed seedling raise period that accelerates the ripening.Not only fungicidal activity is high but also consumption is low as sterilant to select metconazole.Select anion surfactant morpholine and nonionic surface active agent fatty alcohol-polyoxyethylene ether (peregal) to make product easily make microemulsion, ginseng seed surface is not produced to injury or impact, and play the effect of protection.
Embodiment
Illustrate a kind of ginseng seed treatment agent of the present invention with specific embodiment below, per-cent is wherein massfraction.
Embodiment 1
6% Ka Naba wax T3#(Brazil produces);
5.0% Palmiticacid (the Ministry of Chemical Industry of Duo Lijia trade Co., Ltd of jiangsu wuxi city professional production);
2.5% Rugao, stearic acid 1801(Jiangsu grease company);
6.0% standard dibasic alcohol SGH210N(Shanghai Yi Zhu Industrial Co., Ltd.);
8% morpholine (production of Kai Tong Fine Chemical Co., Ltd of Wuhan City);
1.5% metconazole (reagent company in the future);
Distilled water surplus.
Take lipid acid and wetting Agent for Printing Inks joins in container in the ratio of embodiment 1, be heated to 135 ℃ of reaction 245min, make A material.Take Wax in the ratio of embodiment 1 and join in reactor, be heated to 132 ℃, then A material is joined in wax material, stirring reaction 45min at 122 ℃, makes oil phase substance.In the ratio of embodiment 1, tensio-active agent is joined in distilled water and is heated to 84 ℃, make aqueous phase substance.Mixing and emulsifying during oil phase substance is joined to water under high-speed stirring, after completing, emulsification stirs constant 30min at 94 ℃, then add sterilant to stir again constant 12min, then cool to 42 ℃ through homogenizer, be a kind of ginseng seed treatment agent product of the present invention.
Embodiment 2:
4% beeswax (KLK-F) (production of Beijing Li Kang great achievement Science and Technology Ltd.);
3.0 %62 oxidized petroleum waxs (Fushun Petrochemical Research Institute);
4.5% Palmiticacid (the Ministry of Chemical Industry of Duo Lijia trade Co., Ltd of jiangsu wuxi city professional production);
4.5% Rugao, stearic acid 1801(Jiangsu grease company);
4.0% standard trivalent alcohol SGH320T(Shanghai Yi Zhu Industrial Co., Ltd.);
3.0% standard dibasic alcohol SGH210N(Shanghai Yi Zhu Industrial Co., Ltd.);
5.5% morpholine (production of Kai Tong Fine Chemical Co., Ltd of Wuhan City);
2.5% peregal A-20(Fushun Chemical Co., Ltd. of Konka produces);
2.0% metconazole (reagent company in the future);
Distilled water surplus.
Take lipid acid and wetting Agent for Printing Inks joins in container in the ratio of embodiment 2, be heated to 124 ℃ of reaction 244min, make A material.Take Wax in the ratio of embodiment 1 and join in reactor, be heated to 118 ℃, then A material is joined in wax material, stirring reaction 24min at 121 ℃, makes oil phase substance.In the ratio of embodiment 2, tensio-active agent is joined in distilled water and is heated to 89 ℃, make aqueous phase substance.Mixing and emulsifying during oil phase substance is joined to water under high-speed stirring, after completing, emulsification stirs constant 44min at 96 ℃, then add sterilant to stir again constant 18min, then cool to 49 ℃ through homogenizer, be a kind of ginseng seed treatment agent product of the present invention.
Embodiment 3:
6.0% Ka Naba wax T1#(Brazil produces);
2.0% beeswax (KLK-F) (production of Beijing Li Kang great achievement Science and Technology Ltd.);
6.5% Palmiticacid (the Ministry of Chemical Industry of Duo Lijia trade Co., Ltd of jiangsu wuxi city professional production);
4.0% Rugao, stearic acid 1801(Jiangsu grease company);
8.0% standard trivalent alcohol SGH320T(Shanghai Yi Zhu Industrial Co., Ltd.);
6% morpholine (production of Kai Tong Fine Chemical Co., Ltd of Wuhan City);
2.0% peregal A-20(Fushun Chemical Co., Ltd. of Konka produces);
2.0% cyazofamid (Shanghai crystallite biological reagent company limited);
Distilled water surplus.
Take lipid acid and wetting Agent for Printing Inks joins in container in the ratio of embodiment 3, be heated to 123 ℃ of reaction 235min, make A material.Take Wax in the ratio of embodiment 3 and join in reactor, be heated to 115 ℃, then A material is joined in wax material, stirring reaction 28min at 121 ℃, makes oil phase substance.In the ratio of embodiment 2, tensio-active agent is joined in distilled water and is heated to 92 ℃, make aqueous phase substance.Mixing and emulsifying during oil phase substance is joined to water under high-speed stirring, after completing, emulsification stirs constant 38min at 95 ℃, then add sterilant to stir again constant 20min, then cool to 40 ℃ through homogenizer, be a kind of ginseng seed treatment agent product of the present invention.
Embodiment 4:
No. 5%66 oxidized petroleum waxs (Fushun Petrochemical Research Institute);
4% beeswax (KLK-F) (production of Beijing Li Kang great achievement Science and Technology Ltd.);
8.0% Palmiticacid (the Ministry of Chemical Industry of Duo Lijia trade Co., Ltd of jiangsu wuxi city professional production);
4.0% Rugao, stearic acid 1801(Jiangsu grease company);
4.0% standard trivalent alcohol SGH320T(Shanghai Yi Zhu Industrial Co., Ltd.);
0.5% metconazole (reagent company in the future);
5% morpholine (production of Kai Tong Fine Chemical Co., Ltd of Wuhan City);
2.0% peregal A-20(Fushun Chemical Co., Ltd. of Konka produces);
Distilled water surplus.
Take lipid acid and wetting Agent for Printing Inks joins in container in the ratio of embodiment 4, be heated to 139 ℃ of reaction 242min, make A material.Take Wax in the ratio of embodiment 4 and join in reactor, be heated to 121 ℃, then A material is joined in wax material, stirring reaction 48min at 141 ℃, makes oil phase substance.In the ratio of embodiment 4, tensio-active agent is joined in distilled water and is heated to 93 ℃, make aqueous phase substance.Mixing and emulsifying during oil phase substance is joined to water under high-speed stirring, after completing, emulsification stirs constant 45min at 94 ℃, then add sterilant to stir again constant 19min, then cool to 38 ℃ through homogenizer, be a kind of ginseng seed treatment agent product of the present invention.
Embodiment 5:
10.0% beeswax (KLK-F) (production of Beijing Li Kang great achievement Science and Technology Ltd.);
4.0% Palmiticacid (the Ministry of Chemical Industry of Duo Lijia trade Co., Ltd of jiangsu wuxi city professional production);
2.0% Rugao, stearic acid 1801(Jiangsu grease company);
2.0% standard trivalent alcohol SGH320T (Shanghai Yi Zhu Industrial Co., Ltd.);
3.0% standard dibasic alcohol SGH210N ((Shanghai Yi Zhu Industrial Co., Ltd.);
4.5% morpholine (production of Kai Tong Fine Chemical Co., Ltd of Wuhan City);
2.5% peregal A-20(Fushun Chemical Co., Ltd. of Konka produces);
1.2% cyazofamid (Shanghai crystallite biological reagent company limited);
Distilled water surplus.
Take lipid acid and wetting Agent for Printing Inks joins in container in the ratio of embodiment 5, be heated to 144 ℃ of reaction 201min, make A material.Take Wax in the ratio of embodiment 4 and join in reactor, be heated to 123 ℃, then A material is joined in wax material, stirring reaction 50min at 142 ℃, makes oil phase substance.In the ratio of embodiment 5, tensio-active agent is joined in distilled water and is heated to 88 ℃, make aqueous phase substance.Mixing and emulsifying during oil phase substance is joined to water under high-speed stirring, after completing, emulsification stirs constant 50min at 96 ℃, then add sterilant to stir again constant 21min, then cool to 51 ℃ through homogenizer, be a kind of ginseng seed treatment agent product of the present invention.
The applicable cases of following test-results explanation embodiment:
Table 1 ginseng seed germinating time result:
Sample | Blank (my god) | After processing (my god) |
Embodiment 1 | 610 | 590 |
Embodiment 2 | 610 | 585 |
Embodiment 3 | 610 | 584 |
Embodiment 4 | 610 | 586 |
Embodiment 5 | 610 | 585 |
Mean value | 610 | 586 |
The ginseng seed that test-results explanation is used said preparation to process, germinating time all shortens to some extent.This impels ginseng seed precocity, reduces the ginseng seed seedling raise period that accelerates the ripening.
Claims (9)
1. a ginseng seed treatment agent, is characterized in that: comprise in mass
Wax 6%~10%
Wetting Agent for Printing Inks 4%~8%
Lipid acid 6%~12%
Sterilant 0.1%~2.0%
Tensio-active agent 6%~8%
Distilled water surplus.
2. according to ginseng seed treatment agent claimed in claim 1, it is characterized in that: described Wax is one or more in vegetable wax, animal wax, oxidized petroleum wax.
3. according to ginseng seed treatment agent claimed in claim 2, it is characterized in that: described vegetable wax is one or more in carnauba wax, gama wax, rice bran wax, sugar-cane wax, laurel wax, Semen Ricini wax, lacquer tree fat, George Simond haze tallow, ouricury wax, Pseudotsuga menziesii (Mirbel) Franco wax, described animal wax is one or more in beeswax, wool wax, insect wax, spermaceti, and described oxidized petroleum wax is 60~No. 70 oxidized petroleum waxs.
4. according to ginseng seed treatment agent claimed in claim 1, it is characterized in that: described lipid acid is chain saturated fatty acids, specifically stearic acid and/or Palmiticacid.
5. according to ginseng seed treatment agent claimed in claim 1, it is characterized in that: described wetting Agent for Printing Inks is one or both in dibasic alcohol and polyvalent alcohol.
6. according to ginseng seed treatment agent claimed in claim 1, it is characterized in that: described tensio-active agent is anion surfactant and/or nonionic surface active agent.
7. according to ginseng seed treatment agent claimed in claim 6, it is characterized in that: described anion surfactant is one or more in morpholine, Sodium dodecylbenzene sulfonate, sodium lauryl sulphate, described nonionic surface active agent is one or more in fatty alcohol-polyoxyethylene ether, polyoxyethylene carboxylate, alkylphenol polyoxyethylene.
8. according to ginseng seed treatment agent claimed in claim 1, it is characterized in that: described sterilant is metconazole or cyazofamid.
9. the preparation method of arbitrary described ginseng seed treatment agent in claim 1~8, comprises the steps:
(1) take wetting Agent for Printing Inks according to proportioning and lipid acid joins in container, be heated to 115~145 ℃, reaction 205~245min, obtains A material;
(2) take Wax according to proportioning and join in reactor, be heated to 115~145 ℃, then the A material obtaining in step (1) is joined in reactor, at 115~145 ℃, stirring reaction 20~50min, obtains oil phase substance;
(3) according to proportioning, tensio-active agent is joined in distilled water, be heated to 80~96 ℃, obtain aqueous phase substance;
(4) gained oil phase substance in step (2) is joined under high-speed stirring condition to mixing and emulsifying in the aqueous phase substance of gained in step (3), after completing, emulsification stirs constant 30~50min at 93~97 ℃, add sterilant to stir 8~22min according to proportioning again, cool to 38~52 ℃ through homogenizer, be final treatment agent product.
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CN201210433551.8A CN103788874B (en) | 2012-11-05 | 2012-11-05 | A kind of ginseng seed's inorganic agent and preparation method thereof |
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CN201210433551.8A CN103788874B (en) | 2012-11-05 | 2012-11-05 | A kind of ginseng seed's inorganic agent and preparation method thereof |
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CN103788874A true CN103788874A (en) | 2014-05-14 |
CN103788874B CN103788874B (en) | 2016-08-03 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112823630A (en) * | 2019-11-21 | 2021-05-21 | 沈阳中化农药化工研发有限公司 | Seed treatment agent for sterilization |
CN114213969A (en) * | 2022-01-04 | 2022-03-22 | 东莞理工学院 | Corm plant wax pattern material based on wax plating process, preparation method and application thereof |
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CN1069626A (en) * | 1991-08-29 | 1993-03-10 | 中国石油化工总公司抚顺石油化工研究院 | A kind of fruit trees water retaining and antifreezing agent and production and preparation method thereof |
CN1288654A (en) * | 1999-09-17 | 2001-03-28 | 中国石油化工集团公司 | Water retaining and antifreezing treatment of overwintering grapevine |
CN1288930A (en) * | 1999-09-17 | 2001-03-28 | 中国石油化工集团公司 | Grape vine water-retaining antifreezer and its preparation |
CN1288661A (en) * | 1999-09-17 | 2001-03-28 | 中国石油化工集团公司 | Wax emulsion for treating seeds and its preparation and usage |
CN101278613A (en) * | 2008-05-30 | 2008-10-08 | 中国热带农业科学院橡胶研究所 | Method for storing seeds of rubber tree |
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2012
- 2012-11-05 CN CN201210433551.8A patent/CN103788874B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1069626A (en) * | 1991-08-29 | 1993-03-10 | 中国石油化工总公司抚顺石油化工研究院 | A kind of fruit trees water retaining and antifreezing agent and production and preparation method thereof |
CN1288654A (en) * | 1999-09-17 | 2001-03-28 | 中国石油化工集团公司 | Water retaining and antifreezing treatment of overwintering grapevine |
CN1288930A (en) * | 1999-09-17 | 2001-03-28 | 中国石油化工集团公司 | Grape vine water-retaining antifreezer and its preparation |
CN1288661A (en) * | 1999-09-17 | 2001-03-28 | 中国石油化工集团公司 | Wax emulsion for treating seeds and its preparation and usage |
CN101278613A (en) * | 2008-05-30 | 2008-10-08 | 中国热带农业科学院橡胶研究所 | Method for storing seeds of rubber tree |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112823630A (en) * | 2019-11-21 | 2021-05-21 | 沈阳中化农药化工研发有限公司 | Seed treatment agent for sterilization |
CN112823630B (en) * | 2019-11-21 | 2021-11-23 | 沈阳中化农药化工研发有限公司 | Seed treatment agent for sterilization |
CN114213969A (en) * | 2022-01-04 | 2022-03-22 | 东莞理工学院 | Corm plant wax pattern material based on wax plating process, preparation method and application thereof |
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