CN103755421B - Humic acid type spring rape is compound fertilizer dedicated - Google Patents

Humic acid type spring rape is compound fertilizer dedicated Download PDF

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CN103755421B
CN103755421B CN201410030231.7A CN201410030231A CN103755421B CN 103755421 B CN103755421 B CN 103755421B CN 201410030231 A CN201410030231 A CN 201410030231A CN 103755421 B CN103755421 B CN 103755421B
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fermentation
particle
fertilizer
urea
temperature
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CN103755421A (en
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王平生
韩宏
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GANSU TIANYE ORGANIC ECOLOGY FERTILIZER TECHNOLOGY DEVELOPMENT Co Ltd
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GANSU TIANYE ORGANIC ECOLOGY FERTILIZER TECHNOLOGY DEVELOPMENT Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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Abstract

The present invention relates to a kind of humic acid type spring rape compound fertilizer dedicated, this composite fertilizer is made up of the raw material of following weight per-cent: biological carbon organic fertilizer matrix 60 ~ 80%, urea 6 ~ 20%, monoammonium phosphate 8 ~ 17%, potassium sulfate 3.5 ~ 5.5%, trace element 0.005 ~ 0.015%.The present invention both can be the nutritive element needed for spring rape time of infertility, can be again the soil ulmin that soil provides sufficient, improved Soil structure.

Description

Humic acid type spring rape is compound fertilizer dedicated
Technical field
The present invention relates to agricultural technology field, particularly relate to humic acid type spring rape compound fertilizer dedicated.
Background technology
At present, during Gansu Province's spring rape is produced, generally adopt the habits fertilization method that organic and inorganic combines, fertilizer is directly manured into soil as base manure, inorganic fertilizer (comprising nitrogen, phosphorus, potash fertilizer) is manured into soil as seed manure is disposable at seeding time, and by test for many years and Demonstration And Extension, summed up the nitrogen of spring rape the best, phosphorus, potash fertilizer usage quantity, for larger contribution has been made in the increase of spring rape output.But the ight soil of fertilizer used mainly ox, sheep, pig, chicken and people in producing, these fertilizers are directly manured into soil without becoming thoroughly decomposed, wherein heavy metal content exceeds standard, mix the objectionable impuritiess such as weed seed, germ, insect simultaneously, cause soil pollution, and propagate disease pest and weed, affect spring rape and produce.In addition, after inorganic fertilizer is directly used, the elements such as N, P, K of wherein containing are along with losses such as rains, and Absorption of Rape utilization ratio declines, and fertilising benefit reduces.
Summary of the invention
Technical problem to be solved by this invention be to provide a kind of for soil sufficient soil ulmin is provided, to improve the humic acid type spring rape of Soil structure compound fertilizer dedicated.
For solving the problem, humic acid type spring rape of the present invention is compound fertilizer dedicated, it is characterized in that: this composite fertilizer is made up of the raw material of following weight per-cent: biological carbon organic fertilizer matrix 60 ~ 80%, urea 6 ~ 20%, monoammonium phosphate 8 ~ 17%, potassium sulfate 3.5 ~ 5.5%, trace element 0.005 ~ 0.015%.
Biological carbon organic fertilizer matrix refers to and obtains in the steps below:
(1) remove impurity in ox, sheep ight soil respectively, pulverize after making its dust content≤4%, cross 100 mesh sieves, obtain cow dung particle and the sheep excrement particle of water content≤50% respectively;
(2) Semen Brassicae campestris obtains pie material after refining oil according to a conventional method, is crushed to 100 orders, obtains oil cake powder after this pie material cooks;
(3) will be ground into length at below 0.5cm by fresh high-quality wheat stalk then, obtain wheat straw powder;
(4) wheat straw powder pre fermentation: add the urea of its quality 0.05%, the table sugar of 0.01% in described wheat straw powder, after mixing, is the wheat straw powder namely obtaining fermentation after becoming thoroughly decomposed 25 ~ 35 days under the condition of 20 ~ 40 DEG C in temperature;
(5) prepare mixed fermenting agent: in 1kg fermenting agent, add the described oil cake powder that 30kg fineness is 100 object corn flours, 20kg successively, after mixing, namely obtain mixed fermenting agent;
(6) fermentation materials amounts to the proportioning of dry matter weight gauge gained by natural moisture content: described cow dung particle 10 ~ 30%, described sheep excrement particle 60 ~ 80%, wheat straw powder 3 ~ 7%, the 100 order calcium superphosphate 1 ~ 3% of described fermentation, urea 0.5 ~ 1.5%, surplus are described mixed fermenting agent;
(7) fill pond:
1. in fermentation vat, first by described step (6) in the total consumption of each fermentation materials 1/4th, the end of by, the upper order by " the wheat straw powder-mixed culture fermentation agent-cow dung particle of sheep excrement particle-calcium superphosphate+urea-fermentation " piles one deck mixture, fill the second layer in this order again, by that analogy, pile to 4 layers, make described fermentation vat charging maximum height≤1.2 meter, every pond charging 85 ~ 95 tons, every layer of described mixture moisture content is 50 ~ 60%;
2. close the ventilation opening of described fermentation vat, make described mixture nature fermentation at elevated temperatures;
3. temperature of charge, moisture determination: 9 points, 15 points, 21 points of second day behind dress pond, measure temperature and the moisture of the described mixture of each layer; When described mixture temperature is more than more than 65 DEG C, then turn over throwing in time; When warm indoor air temperature more than 60 DEG C or atmospheric moisture more than 80% time, then timely aeration-cooling wet down; When described mixture water content lower than 50% time spray water in time;
4. material turning: turned over throwing 1 time every 3 ~ 5 days, throws 3 ~ 5 centimetres, bottom for standard to turn at every turn, once saturating, carries out secondary and turns over throwing, to turn over to bottom 3 ~ 5 centimetres for standard; Turn over throwing continuously 3 ~ 6 times later;
5. aerobic fermentation: after described mixture temperature continues more than 10 days at 55 ~ 60 DEG C, covered with plastic film when described mixture reaches 50 ~ 60%, and continue to carry out aerobic fermentation in 5 ~ 7 days at spring, summer, Qiu Sanji, or continue winter to carry out aerobic fermentation in 15 ~ 25 days;
6. anaerobically fermenting: after aerobic fermentation terminates, described mixture surface sprinkling, and by plastic covered, continue to carry out anaerobically fermenting in 4 ~ 5 days;
7. check the degree of becoming thoroughly decomposed of described mixture: when the original shape of described mixture change, cellulosic toughness disappears, color and luster blackening then becomes thoroughly decomposed completely, biological carbon organic substrate;
8. matrix goes out pond: first open fermentation vat for a moment, turn over throwing every day 1 time, moisture content is down to 30% and described biological carbon organic substrate can be made to go out pond;
(8) cross 100 mesh sieves after being pulverized by described biological carbon organic substrate, and carry out natural drying, make its natural moisture content be 10 ~ 12%, then chemically examine according to a conventional method, pack according to a conventional method after qualified.
The nitrogen content of described urea is 46%.
In described monoammonium phosphate nitrogenous 12%, containing Vanadium Pentoxide in FLAKES 46%.
Containing potassium oxide 51% in described potassium sulfate.
Described trace element refers to that zinc sulfate or borax mix by 0.5g:0.5g.
The preparation method that humic acid type spring rape as above is compound fertilizer dedicated, is characterized in that: first weigh by proportioning, carries out granulation according to a conventional method, obtain composite fertilizer particle after then being mixed by each raw material; Finally, after described composite fertilizer particle is dried to constant weight at 350 DEG C of temperature, be cooled to room temperature, cross 4 ~ 6mm sieve, to obtain final product.
The present invention compared with prior art has the following advantages:
1, the present invention is on the basis analyzing spring rape nutrient requirement characteristics, according to Soil In Gansu Province nutritional status and conventional fertilizer application method, pass through experimental study, summary proposes spring rape organic and inorganic special compound fertilizer material formula, the spring rape organic and inorganic special compound fertilizer material produced by this formula is through production test, humus content 32%, nitrogen (N) 9.1%, phosphorus (P 2o 5) 6.3%, potassium (K 2o) 3.2%, the more existing fertilizer practice of its stimulation ratio (habits fertilization method---the i.e. fertilizing method that combines of organic and inorganic) is high by 14.4%, per mu yield value increases by 102.54 yuan, and (special fertilizer is by 2.0 yuan/kg, in habits fertilization method, urea is by 2.0 yuan/kg, calcium superphosphate by 0.75 yuan/kg, and Semen Brassicae campestris calculates by 6.0 yuan/kg).
2, the invention belongs to slow control fertilizer, fertilizer nutrient release supply and Absorption of Rape can be reached in time, spatially synchronous, saving of labor during joint, thus improve utilization rate of fertilizer, to reach increasing both production and income and eco-friendly target.
3, the matrix that the present invention selects is the material such as excrement of animals, crop material, adopt totally-enclosed high temperature quick bio fermentation technique, the problem of insect, germ, weed seed is carried in fertilizer in thorough solution conventional fertilizer application technology, simultaneously organic containing abundant biological carbon type.
4, the present invention both can be the nutritive element needed for spring rape time of infertility, can be again the soil ulmin that soil provides sufficient, improved Soil structure.
Embodiment
embodiment 1humic acid type spring rape is compound fertilizer dedicated, and this composite fertilizer is made up of the raw material of following weight per-cent: biological carbon organic fertilizer matrix 60%, urea 19.495%, monoammonium phosphate 17%, potassium sulfate 3.5%, trace element 0.005%.
Compound fertilizer dedicated preparation method refers to this humic acid type spring rape: first weigh by proportioning, carry out granulation according to a conventional method, obtain composite fertilizer particle after then being mixed by each raw material; Finally, composite fertilizer particle is cooled to room temperature be dried to constant weight at 350 DEG C of temperature after, crosses 4 ~ 6mm sieve, to obtain final product.
embodiment 2humic acid type spring rape is compound fertilizer dedicated, and this composite fertilizer is made up of the raw material of following weight per-cent: biological carbon organic fertilizer matrix 80%, urea 6.485%, monoammonium phosphate 8%, potassium sulfate 5.5%, trace element 0.015%.
The compound fertilizer dedicated preparation method of this humic acid type spring rape with embodiment 1.
embodiment 3humic acid type spring rape is compound fertilizer dedicated, and this composite fertilizer is made up of the raw material of following weight per-cent: biological carbon organic fertilizer matrix 70%, urea 17%, monoammonium phosphate 8.49%, potassium sulfate 4.5%, trace element 0.010%.
The compound fertilizer dedicated preparation method of this humic acid type spring rape with embodiment 1.
embodiment 4humic acid type spring rape is compound fertilizer dedicated, and this composite fertilizer is made up of the raw material of following weight per-cent: biological carbon organic fertilizer matrix 76.992%, urea 6%, monoammonium phosphate 14%, potassium sulfate 3%, trace element 0.008%.
The compound fertilizer dedicated preparation method of this humic acid type spring rape with embodiment 1.
embodiment 5humic acid type spring rape is compound fertilizer dedicated, and this composite fertilizer is made up of the raw material of following weight per-cent: biological carbon organic fertilizer matrix 65.988%, urea 20%, monoammonium phosphate 10%, potassium sulfate 4%, trace element 0.012%.
The compound fertilizer dedicated preparation method of this humic acid type spring rape with embodiment 1.
Above-mentioned embodiment 1 ~ 5in, the nitrogen content of urea is 46%.In monoammonium phosphate nitrogenous 12%, containing Vanadium Pentoxide in FLAKES 46%.Containing potassium oxide 51% in potassium sulfate.Trace element refers to that zinc sulfate or borax mix by 0.5g:0.5g.
Biological carbon organic fertilizer matrix refers to and obtains in the steps below:
(1) remove impurity in ox, sheep ight soil respectively, pulverize after making its dust content≤4%, cross 100 mesh sieves, obtain cow dung particle and the sheep excrement particle of water content≤50% respectively.
(2) Semen Brassicae campestris obtains pie material after refining oil according to a conventional method, is crushed to 100 orders, obtains oil cake powder after this pie material cooks.
(3) will be ground into length at below 0.5cm by fresh high-quality wheat stalk then, obtain wheat straw powder.
(4) wheat straw powder pre fermentation: add the urea of its quality 0.05%, the table sugar of 0.01% in wheat straw powder, after mixing, is the wheat straw powder namely obtaining fermentation after becoming thoroughly decomposed 25 ~ 35 days under the condition of 20 ~ 40 DEG C in temperature.
(5) prepare mixed fermenting agent: in 1kg fermenting agent, add the oil cake powder that 30kg fineness is 100 object corn flours, 20kg successively, after mixing, namely obtain mixed fermenting agent.
Wherein: fermenting agent is that RW enzyme agent, the RW that effluent south Hebi Ren Yuan bio-fertilizer Technology R & D Center produces urgees rotten agent (250g dress).
(6) fermentation materials amounts to the proportioning of dry matter weight gauge gained by natural moisture content: cow dung particle 10 ~ 30%, sheep excrement particle 60 ~ 80%, wheat straw powder 3 ~ 7%, the 100 order calcium superphosphate 1 ~ 3% of fermentation, urea 0.5 ~ 1.5%, surplus are mixed fermenting agent.
Wherein: calcium superphosphate produces refined board normal superphosphate by Baiyin phosphate fertilizer plant, and 40kg fills, containing Vanadium Pentoxide in FLAKES 12%.Urea is by Liu Hua limited liability company production the Yellow River, Gansu board urea, and 40kg fills, and nitrogen content is 46%.
(7) fill pond:
1. in fermentation vat, first by step (6) in the total consumption of each fermentation materials 1/4th, the end of by, the upper order by " the wheat straw powder-mixed culture fermentation agent-cow dung particle of sheep excrement particle-calcium superphosphate+urea-fermentation " piles one deck mixture, fill the second layer in this order again, by that analogy, pile to 4 layers, make fermentation vat charging maximum height≤1.2 meter, every pond charging 85 ~ 95 tons, every layer of described mixture moisture content is 50 ~ 60%;
2. close the ventilation opening of fermentation vat, make mixture nature fermentation at elevated temperatures;
3. temperature of charge, moisture determination: 9 points, 15 points, 21 points of second day behind dress pond, measure temperature and the moisture of each layer mixture; When mixture temperature is more than more than 65 DEG C, then turn over throwing in time; When warm indoor air temperature more than 60 DEG C or atmospheric moisture more than 80% time, then timely aeration-cooling wet down; When mixture water content lower than 50% time spray water in time;
4. material turning: turned over throwing 1 time every 3 ~ 5 days, throws 3 ~ 5 centimetres, bottom for standard to turn at every turn, once saturating, carries out secondary and turns over throwing, to turn over to bottom 3 ~ 5 centimetres for standard; Turn over throwing continuously 3 ~ 6 times later;
5. aerobic fermentation: when mixture temperature continues after more than 10 days at 55 ~ 60 DEG C, covered with plastic film when mixture reaches 50 ~ 60%, and continue to carry out aerobic fermentation in 5 ~ 7 days at spring, summer, Qiu Sanji, or lastingly within 15 ~ 25 days, carry out aerobic fermentation winter;
6. anaerobically fermenting: after aerobic fermentation terminates, mixture surface sprinkling, and by plastic covered, continue to carry out anaerobically fermenting in 4 ~ 5 days;
7. check the degree of becoming thoroughly decomposed of mixture: when the original shape of mixture change, cellulosic toughness disappears, color and luster blackening is then become thoroughly decomposed completely, biological carbon organic substrate;
8. matrix goes out pond: first open fermentation vat for a moment, turn over throwing every day 1 time, moisture content is down to 30% and biological carbon organic substrate can be made to go out pond;
(8) cross 100 mesh sieves after being pulverized by biological carbon organic substrate, and carry out natural drying, make its natural moisture content be 10 ~ 12%, then chemically examine according to a conventional method, pack according to a conventional method after qualified.
Above-mentioned quality or weight metering unit are kg.

Claims (2)

1. humic acid type spring rape is compound fertilizer dedicated, it is characterized in that: this composite fertilizer is made up of the raw material of following weight per-cent: biological carbon organic fertilizer matrix 60 ~ 80%, urea 6 ~ 20%, monoammonium phosphate 8 ~ 17%, potassium sulfate 3.5 ~ 5.5%, trace element 0.005 ~ 0.015%;
Described biological carbon organic fertilizer matrix refers to and obtains in the steps below:
(1) remove impurity in ox, sheep ight soil respectively, pulverize after making its dust content≤4%, cross 100 mesh sieves, obtain cow dung particle and the sheep excrement particle of water content≤50% respectively;
(2) Semen Brassicae campestris obtains pie material after refining oil according to a conventional method, is crushed to 100 orders, obtains oil cake powder after this pie material cooks;
(3) will be ground into length at below 0.5cm by fresh high-quality wheat stalk then, obtain wheat straw powder;
(4) wheat straw powder pre fermentation: add the urea of its quality 0.05%, the table sugar of 0.01% in described wheat straw powder, after mixing, is the wheat straw powder namely obtaining fermentation after becoming thoroughly decomposed 25 ~ 35 days under the condition of 20 ~ 40 DEG C in temperature;
(5) prepare mixed fermenting agent: in 1kg fermenting agent, add the described oil cake powder that 30kg fineness is 100 object corn flours, 20kg successively, after mixing, namely obtain mixed fermenting agent;
(6) fermentation materials amounts to the proportioning of dry matter weight gauge gained by natural moisture content: described cow dung particle 10 ~ 30%, described sheep excrement particle 60 ~ 80%, wheat straw powder 3 ~ 7%, the 100 order calcium superphosphate 1 ~ 3% of described fermentation, urea 0.5 ~ 1.5%, surplus are described mixed fermenting agent;
(7) fill pond:
1. in fermentation vat, first by described step (6) in the total consumption of each fermentation materials 1/4th, the end of by, the upper order by " the wheat straw powder-mixed culture fermentation agent-cow dung particle of sheep excrement particle-calcium superphosphate+urea-fermentation " piles one deck mixture, fill the second layer in this order again, by that analogy, pile to 4 layers, make described fermentation vat charging maximum height≤1.2 meter, every pond charging 85 ~ 95 tons, every layer of described mixture moisture content is 50 ~ 60%;
2. close the ventilation opening of described fermentation vat, make described mixture nature fermentation at elevated temperatures;
3. temperature of charge, moisture determination: 9 points, 15 points, 21 points of second day behind dress pond, measure temperature and the moisture of the described mixture of each layer; When described mixture temperature is more than more than 65 DEG C, then turn over throwing in time; When warm indoor air temperature more than 60 DEG C or atmospheric moisture more than 80% time, then timely aeration-cooling wet down; When described mixture water content lower than 50% time spray water in time;
4. material turning: turned over throwing 1 time every 3 ~ 5 days, throws 3 ~ 5 centimetres, bottom for standard to turn at every turn, once saturating, carries out secondary and turns over throwing, to turn over to bottom 3 ~ 5 centimetres for standard; Turn over throwing continuously 3 ~ 6 times later;
5. aerobic fermentation: after described mixture temperature continues more than 10 days at 55 ~ 60 DEG C, covered with plastic film when described mixture reaches 50 ~ 60%, and continue to carry out aerobic fermentation in 5 ~ 7 days at spring, summer, Qiu Sanji, or continue winter to carry out aerobic fermentation in 15 ~ 25 days;
6. anaerobically fermenting: after aerobic fermentation terminates, described mixture surface sprinkling, and by plastic covered, continue to carry out anaerobically fermenting in 4 ~ 5 days;
7. check the degree of becoming thoroughly decomposed of described mixture: when the original shape of described mixture change, cellulosic toughness disappears, color and luster blackening then becomes thoroughly decomposed completely, biological carbon organic substrate;
8. matrix goes out pond: first open fermentation vat for a moment, turn over throwing every day 1 time, moisture content is down to 30% and described biological carbon organic substrate can be made to go out pond;
(8) cross 100 mesh sieves after being pulverized by described biological carbon organic substrate, and carry out natural drying, make its natural moisture content be 10 ~ 12%, then chemically examine according to a conventional method, pack according to a conventional method after qualified;
The nitrogen content of described urea is 46%; In described monoammonium phosphate nitrogenous 12%, containing Vanadium Pentoxide in FLAKES 46%; Containing potassium oxide 51% in described potassium sulfate; Described trace element refers to that zinc sulfate or borax mix by 0.5g:0.5g.
2. the preparation method that humic acid type spring rape as claimed in claim 1 is compound fertilizer dedicated, is characterized in that: first weigh by proportioning, carries out granulation according to a conventional method, obtain composite fertilizer particle after then being mixed by each raw material; Finally, after described composite fertilizer particle is dried to constant weight at 350 DEG C of temperature, be cooled to room temperature, cross 4 ~ 6mm sieve, to obtain final product.
CN201410030231.7A 2014-01-23 2014-01-23 Humic acid type spring rape is compound fertilizer dedicated Expired - Fee Related CN103755421B (en)

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104150990B (en) * 2014-08-20 2016-08-17 湖南湘植园林科技有限公司 A kind of preparation method of plant substrates
CN105646035A (en) * 2015-12-22 2016-06-08 成都新柯力化工科技有限公司 Method for preparing water-soluble ecological organic carbon fertilizer by using plant stalks
CN106631493A (en) * 2016-12-30 2017-05-10 汤广顺 Additive added with azadirachtin-cow dung charcoal suspension liquid for paste leaf fertilizer special for pear trees
CN107382502A (en) * 2017-08-15 2017-11-24 临夏回族自治州农业科学院 Skin tire fruit water-retaining type is compound fertilizer dedicated

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1669992A (en) * 2005-02-14 2005-09-21 曹凯 Colza cake ferment biological organic fertilizer and its production process
DE102006051010A1 (en) * 2006-10-26 2008-05-08 Wehling Anlagen Und Maschinenbau Gmbh Process for the production of structural bodies from organic and mineral fertilizer components and structural bodies
CN101935236A (en) * 2010-09-27 2011-01-05 上海创博生态工程有限公司 Method for preparing acid organic fertilizer by orientation fermentation of organic waste
CN102491802A (en) * 2011-12-13 2012-06-13 黄山市徽山食用油业有限公司 Tea seed cake biological organic fertilizer and production method thereof
CN102992837A (en) * 2012-10-10 2013-03-27 肥西县农业技术推广中心 Special organic/inorganic composite fertilizer for rape
CN103420697A (en) * 2012-10-01 2013-12-04 华中农业大学 Direct-seeding rape special-purpose formulated fertilizer

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1669992A (en) * 2005-02-14 2005-09-21 曹凯 Colza cake ferment biological organic fertilizer and its production process
DE102006051010A1 (en) * 2006-10-26 2008-05-08 Wehling Anlagen Und Maschinenbau Gmbh Process for the production of structural bodies from organic and mineral fertilizer components and structural bodies
CN101935236A (en) * 2010-09-27 2011-01-05 上海创博生态工程有限公司 Method for preparing acid organic fertilizer by orientation fermentation of organic waste
CN102491802A (en) * 2011-12-13 2012-06-13 黄山市徽山食用油业有限公司 Tea seed cake biological organic fertilizer and production method thereof
CN103420697A (en) * 2012-10-01 2013-12-04 华中农业大学 Direct-seeding rape special-purpose formulated fertilizer
CN102992837A (en) * 2012-10-10 2013-03-27 肥西县农业技术推广中心 Special organic/inorganic composite fertilizer for rape

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