CN103636944A - Toffee-flavored flavoring agent and preparation method thereof - Google Patents
Toffee-flavored flavoring agent and preparation method thereof Download PDFInfo
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- CN103636944A CN103636944A CN201310643076.1A CN201310643076A CN103636944A CN 103636944 A CN103636944 A CN 103636944A CN 201310643076 A CN201310643076 A CN 201310643076A CN 103636944 A CN103636944 A CN 103636944A
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Abstract
The invention relates to a toffee-flavored flavoring agent and a preparation method thereof. The flavoring agent consists of the following components in parts by weight, totaling 100 parts: 0.05-3 parts of butyric acid, 0.2-0.8 part of butyryl butyl lactate, 0.1-0.5 part of ethyl lactate, 0.05-0.5 part of ethyl butyrate, 0.5-3 parts of ethyl laurate, 0.8-2 parts of gamma-nonalactone, 0.1-1 part of gamma-decalactone, 0.2-3 parts of delta-decalactone, 0.5-5 parts of ethyl vanillin, 0.5-5 parts of lauric acid, 0.05-5 parts of linalool, 20-30 parts of an adsorbent, namely, silicon dioxide and 60-70 parts of a carrier. In comparison with the prior art, the flavoring agent is unique and unadulterated in toffee flavor, high and comfortable in aroma recognition degree, the food calling effect can be improved, the compatibility with feeds is good, the original bitterness of the feeds can be covered up, and the palatability of feeds is improved so as to promote ingestion of animals.
Description
Technical field
The present invention relates to a kind of toffee local flavor flavouring agent and preparation method thereof, and the application of this flavouring agent in feed or pet food.
Background technology
In animal farming industry, raiser's economic benefit and the growth conditions of animal close ties, the growth conditions of animal is mainly subject to the impact of nutrition condition.Therefore raiser mainly guarantees the healthy growth of animal by the feed of the comprehensive nutrition of feeding.And conventional feed comprises soybean, dregs of beans, corn, fish meal, the assorted dregs of rice, amino acid etc. raw material, these raw materials contain different breaths separately, add to and can produce together heavy bad breath, the palatability of animal is exerted an influence with searching for food, and then affect the healthy growth of animal, finally cause raiser's economic benefit to decline, therefore need to cover bad smell with flavouring agent and improve palatability.
Flavouring agent is physiological characteristic and the dietary habit at different growth phases according to different animals, for improving palatability, the attractant of feed, increase feed intake, improve feed and veterinary drug quality and add a kind of odor additive wherein to, generally by perfume base, adsorbent and carrier three parts, formed.
On market, there are a lot of flavouring agent products now, but some problem of ubiquity: the impure attraction of fragrance not animal; The excessive stimulating animal sense of smell of aroma strength causes detests sense; Fragrance is stable not, easily spoiled, poor with feed compatibility; Cannot really play the effect that improves animal feed intake.
At present, the flavouring agent that needs a kind of new feed or pet food.
Summary of the invention
The problem existing for prior art, the object of the invention is to solve fragrance pure and possess functional diversities, good with feed compatibility, improve the effects such as feed intake.
For achieving the above object, the invention provides a kind of flavouring agent, this flavouring agent is comprised of following weight portion formula, the gross weight of flavouring agent of take is 100 parts, 0.05～3 part of butyric acid, 0.2～0.8 part of butyl butyryl lactate, 0.1～0.5 part of ethyl lactate, 0.05～0.5 part of ethyl butyrate, 0.5～3 part of ethyl laurate, 0.8～2 part of nonyl lactone, 0.1～1 part of γ-decalactone, 0.2～3 part of δ-decalactone, 0.5～5 part of Ethyl vanillin, 0.5～5 part of dodecoic acid, 0.05～5 part of linalool, 20～30 parts of adsorbent silica, 60～70 parts, carrier.
Described carrier is any one in anhydrous saccharin sodium, powdered whiting and anhydrous sodium sulfate.
The present invention also provide above-mentioned flavouring agent preparation method be that this preparation method comprises the step that next coming in order carry out:
0.05～3 part of butyric acid, 0.2～0.8 part of butyl butyryl lactate, 0.1～0.5 part of ethyl lactate, 0.05～0.5 part of ethyl butyrate, 0.5～3 part of ethyl laurate, 0.8～2 part of nonyl lactone, 0.1～1 part of γ-decalactone, 0.2～3 part of δ-decalactone, 0.5～5 part of Ethyl vanillin, 0.5～5 part of dodecoic acid, 0.05～5 part of linalool are dropped in liquid aging tank successively, be uniformly mixed, stir 1～2 hour, obtain essence mixture;
Start mixer, 20～30 parts of adsorbent silica are dropped into mixer, more above-mentioned essence mixture is fed intake, both mix 4～5 minutes; Finally 60～70 parts of carriers are dropped into mixer and mix in the lump, make described flavouring agent, above umber is all weight portion.。
The present invention also provides a kind of feed or pet food, the flavouring agent that it adopts above-mentioned flavouring agent or said method to make.
Than prior art, flavouring agent of the present invention has the following advantages:
(1) flavouring agent of the present invention, toffee unique flavor, fragrance identification is high, and feature is distinct, is difficult to personation, copies;
(2) toffee local flavor is pure, and fragrance is joyful comfortable, and stimulating animal sense of smell, belongs to Favourite of animal, can improve food calling effect;
(3) good with the compatibility of feed, can make up lack in feed natural flavour mountaineous, and fragrance is stable, sustained taste;
(4) the selected carrier of the present invention can be covered the bitter taste that feedstuff contains, and improves the palatability of feed, promotes searching for food of animal.
The specific embodiment
With embodiment, further illustrate the present invention below, but the present invention is not limited.The experimental technique of unreceipted actual conditions in embodiment below, conventionally according to normal condition, or the condition of advising according to manufacturer.Wherein, described percentage unless otherwise noted, is all weight percentage; Described umber, is parts by weight.
Embodiment 1
(1) first by 1 kilogram of butyric acid, 3 kilograms of butyl butyryl lactates, 2 kilograms of ethyl lactates, 1 kilogram of ethyl butyrate, 15 kilograms of ethyl laurates, 10 kilograms of nonyl lactones, 3 kilograms of γ-decalactones, 5 kilograms of δ-decalactones, 10 kilograms of Ethyl vanillins, 10 kilograms of dodecoic acids, 1 kilogram of linalool drops in liquid aging tank successively, be uniformly mixed, stir 1 hour; After to be mixed completing, be that ageing completes, by production department, can be put into production after the assay was approved;
(2) start mixer, 200 kilograms of the silica weighing up are fed intake, through screen cloth, enter mixer, the essence preparing is fed intake, after having fed intake, mix 5 minutes;
(3) after remaining 700 kilograms, carrier (anhydrous saccharin sodium) and dropping into again mixer and mix, shut down weighing and bagging after sieving.
Embodiment 2
(1) first by 2 kilograms of butyric acid, 4 kilograms of butyl butyryl lactates, 3 kilograms of ethyl lactates, 2 kilograms of ethyl butyrates, 18 kilograms of ethyl laurates, 12 kilograms of nonyl lactones, 5 kilograms of γ-decalactones, 8 kilograms of δ-decalactones, 15 kilograms of Ethyl vanillins, 15 kilograms of dodecoic acids, in 3 kilograms of input liquid aging tanks of linalool, be uniformly mixed, stir 2 hours; After to be mixed completing, be that ageing completes, by production department, can be put into production after the assay was approved;
(2) start mixer, 250 kilograms of the silica weighing up are fed intake, through screen cloth, enter mixer, the essence preparing is fed intake, after having fed intake, mix 4 minutes;
(3) after remaining 700 kilograms, carrier (powdered whiting) and dropping into again mixer and mix, shut down; Weighing and bagging after sieving.
Embodiment 3
(1) first by 2 kilograms of butyric acid, 5 kilograms of butyl butyryl lactates, 4 kilograms of ethyl lactates, 1 kilogram of ethyl butyrate, 25 kilograms of ethyl laurates, 15 kilograms of nonyl lactones, 8 kilograms of γ-decalactones, 10 kilograms of δ-decalactones, 10 kilograms of Ethyl vanillins, 25 kilograms of dodecoic acids, in 5 kilograms of input liquid aging tanks of linalool, be uniformly mixed, stir 1.5 hours; After to be mixed completing, be that ageing completes, by production department, can be put into production after the assay was approved;
(2) start mixer, 300 kilograms of the silica weighing up are fed intake, through screen cloth, enter mixer, the essence preparing is fed intake, after having fed intake, mix 5 minutes;
(3) after remaining 600 kilograms, carrier (anhydrous sodium sulfate) and dropping into again mixer and mix, shut down; Weighing and bagging after sieving.
Below by effect embodiment, further illustrate beneficial effect of the present invention.
Effect embodiment 1
Flavouring agent fragrance and applicating evaluating: embodiment 2 obtain for sample 1, with commercially available feedstuff flavouring agent A(sample 2) carry out fragrance comparative evaluation.Participating in assessment number is 10 people.
Table 1 finished product fragrance and applicating evaluating proof list
Table 2 flavouring agent sample aroma strength and Comfort Evaluation
Table 3 flavouring agent application verification is evaluated
In sum, no matter sample 1 is all being better than sample 2 aspect aroma strength and comfort level.Perfuming intensity, comfort level and the fragrance remaining time of sample 1 are all better than sample 2.
Effect embodiment 2
Zoopery effect assessment: by embodiment 1(experimental group) add to respectively in powdery perfect compound feed with feedstuff flavouring agent A (control group), addition is 500g/t.Select the healthy DLY piglet of 25 age in days wean to carry out zoopery, be one week experimental period, investigates daily ingestion amount, daily gain and material anharmonic ratio situation, and as shown in Table 4, experimental group can obviously improve the daily ingestion amount of piglet and improve the utilization rate of feed result.
The impact of table 4. flavouring agent on Production Performance of Weaning Pigs
| 25-32 age in days piglet | Control group (feedstuff flavouring agent A) | Experimental group |
| Daily ingestion amount/kg | 0.45±0.021 | 0.67±0.018 |
| Daily gain/kg | 0.32±0.041 | 0.36±0.010 |
| Material anharmonic ratio | 2.14±0.05 | 1.86±0.01 |
From above effect, the index of the daily ingestion amount of experimental group, daily gain and material anharmonic ratio is better than control group.And at aspects such as aroma strength, fragrance comfort level and perfuming feed fragrance remaining time, all there is obvious advantage, be applied in feed and can effectively improve Production Performance of Weaning Pigs.
The flavouring agent that those skilled in the art can prepare above-described embodiment is directly as feed or pet food additives, or the flavouring agent that can adopt conventional method that above-described embodiment is prepared is mixed with feed or pet food additives.Same, those skilled in the art, in the manufacture process of feed or pet food, add these additives in product in a conventional manner.
Claims (5)
1. a flavouring agent, it is characterized in that, this flavouring agent is comprised of following weight portion formula, the gross weight of flavouring agent of take is 100 parts, 0.05～3 part of butyric acid, 0.2～0.8 part of butyl butyryl lactate, 0.1～0.5 part of ethyl lactate, 0.05～0.5 part of ethyl butyrate, 0.5～3 part of ethyl laurate, 0.8～2 part of nonyl lactone, 0.1～1 part of γ-decalactone, 0.2～3 part of δ-decalactone, 0.5～5 part of Ethyl vanillin, 0.5～5 part of dodecoic acid, 0.05～5 part of linalool, 20～30 parts of adsorbent silica, 60～70 parts, carrier.
2. a kind of flavouring agent as claimed in claim 1, is characterized in that, described carrier is selected from any one in anhydrous saccharin sodium, powdered whiting and anhydrous sodium sulfate.
3. a preparation method for flavouring agent, is characterized in that, this preparation method comprises the step that next coming in order carry out:
0.05～3 part of butyric acid, 0.2～0.8 part of butyl butyryl lactate, 0.1～0.5 part of ethyl lactate, 0.05～0.5 part of ethyl butyrate, 0.5～3 part of ethyl laurate, 0.8～2 part of nonyl lactone, 0.1～1 part of γ-decalactone, 0.2～3 part of δ-decalactone, 0.5～5 part of Ethyl vanillin, 0.5～5 part of dodecoic acid, 0.05～5 part of linalool are dropped in liquid aging tank successively, be uniformly mixed, stir 1～2 hour, obtain essence mixture;
Start mixer, 20～30 parts of adsorbent silica are dropped into mixer, more above-mentioned essence mixture is fed intake, both mix 4～5 minutes; Finally 60～70 parts of carriers are dropped into mixer and mix in the lump, make described flavouring agent, above umber is all weight portion.
4. preparation method as claimed in claim 3, is characterized in that, described carrier is selected from any one in anhydrous saccharin sodium, powdered whiting and anhydrous sodium sulfate.
5. feed or a pet food, is characterized in that: in this feed or pet food, added flavouring agent as claimed in claim 1 or 2, or added the flavouring agent that adopts the preparation method of claim 3 or 4 to make.
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| CN103636944B CN103636944B (en) | 2016-03-23 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105595027A (en) * | 2016-01-27 | 2016-05-25 | 上海美农生物科技股份有限公司 | Preparing method for cream smell pig feed attractant |
| CN106561997A (en) * | 2016-11-15 | 2017-04-19 | 常熟市凯力达蜂窝包装材料有限公司 | Fragrance type feed additive |
| CN106578410A (en) * | 2016-11-15 | 2017-04-26 | 常熟市凯力达蜂窝包装材料有限公司 | Preparation method of flavor-type feed additive |
| CN113057254A (en) * | 2021-04-28 | 2021-07-02 | 味氏（广东）生物科技股份有限公司 | Preparation method and application of water-soluble sweet milk essence suitable for drinking water, porridge material and liquid feed of mammals |
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| US20020119233A1 (en) * | 2000-12-15 | 2002-08-29 | Huang An Shun | Cookies with improved shelf life and process for preparing them |
| CN101336699A (en) * | 2008-08-08 | 2009-01-07 | 四川省畜科饲料有限公司 | Super glucin formulation and use thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105595027A (en) * | 2016-01-27 | 2016-05-25 | 上海美农生物科技股份有限公司 | Preparing method for cream smell pig feed attractant |
| CN106561997A (en) * | 2016-11-15 | 2017-04-19 | 常熟市凯力达蜂窝包装材料有限公司 | Fragrance type feed additive |
| CN106578410A (en) * | 2016-11-15 | 2017-04-26 | 常熟市凯力达蜂窝包装材料有限公司 | Preparation method of flavor-type feed additive |
| CN113057254A (en) * | 2021-04-28 | 2021-07-02 | 味氏（广东）生物科技股份有限公司 | Preparation method and application of water-soluble sweet milk essence suitable for drinking water, porridge material and liquid feed of mammals |
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| CN103636944B (en) | 2016-03-23 |
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Inventor after: Hu Zhuodong Inventor after: Tang Zhongyi Inventor after: Wei Wei Inventor before: Zong Jiajia Inventor before: Hu Zhuodong Inventor before: Tang Zhongyi |
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Application publication date: 20140319 Assignee: Chengdu Mei Yide Bioisystech Co., Ltd Assignor: Shanghai Menon Animal Nutrition Technology Co., Ltd. Contract record no.: 2017510000046 Denomination of invention: Toffee-flavored flavoring agent and preparation method thereof Granted publication date: 20160323 License type: Common License Record date: 20171208 |
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