CN111096394A - Fruit milk fragrance type feed flavoring agent and preparation method thereof - Google Patents
Fruit milk fragrance type feed flavoring agent and preparation method thereof Download PDFInfo
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- CN111096394A CN111096394A CN201911420781.9A CN201911420781A CN111096394A CN 111096394 A CN111096394 A CN 111096394A CN 201911420781 A CN201911420781 A CN 201911420781A CN 111096394 A CN111096394 A CN 111096394A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
- A23K10/37—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/105—Aliphatic or alicyclic compounds
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/111—Aromatic compounds
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/163—Sugars; Polysaccharides
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
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Abstract
The invention discloses a fruit milk fragrance type feed flavoring agent and a preparation method thereof, wherein the fruit milk fragrance type feed flavoring agent comprises the following components in parts by weight: 5-15 parts of ethyl butyrate; 8-20 parts of butyric acid; 1-15 parts of ethyl lactate; 0.5-3 parts of acetic acid; 3-17 parts of isoamyl acetate; 10-30 parts of isoamyl butyrate; 5-16 parts of benzyl alcohol; 1-18 parts of ethyl maltol; 1-18 parts of capric acid; 10-30 parts of coconut aldehyde; 3-15 parts of ethyl decanoate; 3-15 parts of peach aldehyde; 1-5 parts of ethyl dodecanoate; 10-30 parts of butter lactone; 3-50 parts of a non-toxic solvent; 100-1000 parts of a carrier. The fruit milk flavor type feed flavoring agent accords with the olfactory and gustatory preferences of animals, has high fragrance joyful degree and good stability, can effectively attract the animals to eat, can obviously improve and coordinate the flavor of the feed when added into the feed, improves the palatability of the feed, attracts the animals to eat, and obviously increases the food consumption.
Description
Technical Field
The invention relates to the technical field of feed additives, in particular to a fruit milk flavor type feed flavoring agent and a preparation method thereof
Background
In animal production, with the improvement of productivity, not only the nutrient substances in daily ration but also the feed has good palatability and sufficient feed intake to meet the overall demand of the livestock on nutrients, so people usually add feed flavoring agents into the feed to improve the palatability and the pleasure of the feed, thereby improving the feed intake of the livestock. In terms of the scents, studies have found that there is a great difference in the food calling effect of various scents on animals, and some people do not necessarily like the animals who smell the preferred scent. The flavoring agent mainly plays a role through the induction of the smell of animals, but the research of the smell physiology discovers that the acuteness of the smell is determined by the area of the olfactory mucosa epithelium and the number of olfactory cells in the epithelium, so that the flavoring agent cannot be selected for the animals only according to the sensory recognition of human beings, and the flavoring agent can be really selected from the perspective of the sensory physiology of the animals only according to the physiological characteristics of the smell and the taste of the animals. The development and selection of the fragrance of the feed flavoring agents must be in line with the animal's habits to satisfy the animal's preference for certain specific fragrances at various stages of growth. The existing feed flavoring agent generally only can promote ingestion to a certain extent, is difficult to satisfy the problem of favorable flavor of animals, has unstable flavor, has poor uniformity when being mixed into the feed, and further influences the ingestion amount of the animals. Therefore, a feed flavoring agent which has the fragrance and taste which are preferred by animals, can improve the palatability of the feed and attract the animals to eat is needed.
Disclosure of Invention
The fruit milk fragrance type feed flavoring agent provided by the invention is in accordance with the olfactory and gustatory preferences of animals, has high fragrance delight degree and good stability, can effectively attract the animals to eat, can be added into the feed, can obviously improve and coordinate the feed flavor, improves the feed palatability, induces the animals to eat, obviously increases the feed intake and increases the weight gain.
The invention also aims to provide a preparation method of the fruit milk flavor type feed flavoring agent.
The technical scheme adopted by the invention is as follows:
a fruit milk fragrance type feed flavoring agent comprises the following components in parts by weight: 5-15 parts of ethyl butyrate; 8-20 parts of butyric acid; 1-15 parts of ethyl lactate; 0.5-3 parts of acetic acid; 3-17 parts of isoamyl acetate; 10-30 parts of isoamyl butyrate; 5-16 parts of benzyl alcohol; 1-18 parts of ethyl maltol; 1-18 parts of capric acid; 10-30 parts of coconut aldehyde; 3-15 parts of ethyl decanoate; 3-15 parts of peach aldehyde; 1-5 parts of ethyl dodecanoate; 10-30 parts of butter lactone; 3-50 parts of a non-toxic solvent; 100-1000 parts of a carrier.
The invention prepares the fruit milk flavor type feed flavoring agent which accords with the olfactory and gustatory preferences of animals according to the physiological characteristics of the animals, the preference of the fruit milk flavor type, the physiological threshold of the fruit milk flavor and other factors and comprehensively considers the flavor type, the head flavor and the fragrance-remaining period of the product. The cream lactone is used for establishing the milk flavor of the fruit milk flavor type feed flavoring agent; isoamyl acetate and isoamyl butyrate have fruity odor; the ethyl lactate has soft fruit fragrance, wine fragrance and cream fragrance; the ethyl maltol has obvious aroma enhancement effect on the fragrance; the capric acid has fruit flavor, and also increases the flavor of fruit milk flavor type feed flavoring agent; peach aldehyde has strong peach aroma, is a lactone spice and is also an edible essence; ethyl butyrate has a strong sweet fruity note of qingling, a slight fruity or floral note of ethyl dodecanoate; the ethyl decanoate has fruity fragrance and wine fragrance; the benzyl alcohol has aromatic smell, and can be used as perfume fixative for lasting fragrance. The fruit milk flavor type feed flavoring agent which accords with the preference of animals is obtained by selecting the components which accord with the smelling and gustatory flavors of the animals and adjusting and preparing the dosage of the components for a plurality of times, and the fruit milk flavor type feed flavoring agent can improve and coordinate the flavor of the feed, improve the palatability of the feed, lure the animals to eat, increase the feed intake and increase the weight by adding the fruit milk flavor type feed flavoring agent into the feed.
Preferably, the fruit milk fragrance type feed flavoring agent comprises the following components in parts by weight: 10-15 parts of ethyl butyrate; 10-15 parts of butyric acid; 5-10 parts of ethyl lactate; 1-3 parts of acetic acid; 10-17 parts of isoamyl acetate; 10-15 parts of isoamyl butyrate; 2-5 parts of ethyl maltol; 3-10 parts of capric acid; 10-20 parts of coconut aldehyde; 10-15 parts of ethyl decanoate; 3-8 parts of peach aldehyde; 3-5 parts of ethyl dodecanoate; 20-30 parts of butter lactone; 10-20 parts of a non-toxic solvent; 700-900 parts of a carrier.
Preferably, the carrier is one or more of silica, glucose, stone powder and rice bran. The variety of the carrier has great influence on the aroma retention period of the flavoring agent and the mixing uniformity in the feed, and the flavoring agent obtained by the invention has longer aroma retention period and can be uniformly mixed in the feed by adopting one or more of silicon dioxide, glucose, stone powder and rice bran as the carrier, so that the palatability of the feed is uniformly improved. Based on the product formula of the fruit milk flavor type feed flavoring agent, the proportion of raw materials with good stability is increased on the premise of not influencing the flavor and the cost performance of the product, so that the prepared flavoring agent has better stability.
Preferably, the nontoxic solvent is one or more of propylene glycol, glycerol triacetate and ethanol.
Preferably, the cream lactone is prepared by the following process: and (3) carrying out esterification reaction on 1-5 per mill of lipase and the balance of butter at 50-70 ℃ for 6-8 h to obtain the cream lactone. The esterification reaction is carried out for 6-8 h at 50-70 ℃, which is beneficial to promoting the esterification reaction between lipase and butter, promoting the release of fragrance, reducing the using amount of cream lactone, improving the feed intake, saving the cost and promoting the absorption of animals to nutrient substances.
The preparation method of the fruit milk flavor type feed flavoring agent comprises the following steps:
s1, stirring and mixing the cream lactone and other raw materials except a carrier at constant temperature, and then sealing, standing and aging for more than 10 hours; preferably, the stirring and mixing time is 1-3 h.
S2, firstly, mixing and adsorbing the aged mixture obtained in the step S1 for 2-10 min by using 10-70% of carriers, and then, secondarily mixing the rest carriers for 5-10 min.
In order to mix uniformly, the stirring time in step S1 should not be too short; however, the stirring time is too long, on one hand, the production period is prolonged and the production cost is increased, on the other hand, a period of time is needed for aging after the raw materials are mixed, and the stirring is not beneficial to aging. After the mixing is finished, a period of aging is needed to remove the impurities occluded in the precipitate, the removal of the impurities is not facilitated due to too short time, and the raw materials interact with each other in the aging process, so that the fragrance becomes harmonious, mellow and soft when the end point is reached.
In order to uniformly mix the aged liquid mixture with the carrier, the mixing process is carried out by two times, so that the mixing is more uniform, and the coefficient of variation is reduced.
Preferably, the flavoring agent is obtained by vibratory sieving after the mixing is completed. After the mixing is finished, the obtained feed flavoring agent is in a bead shape, has good fluidity and is not agglomerated, so that the mixing uniformity of the feed flavoring agent and the feed can be improved, and the feed intake of animals is increased.
Preferably, the raw materials except the carrier in step S1 are fed in a solid-first and liquid-second order. The feeding mode can dissolve the solid for enough time to fully and uniformly mix the components.
Compared with the prior art, the invention has the beneficial effects that: the invention comprehensively considers the physiological specificity of smell and taste of animals, prepares a fruit milk flavor type feed flavoring agent which accords with the preference of smell and taste of animals, wherein cream lactone extract lays the milk flavor of the fruit milk flavor type feed flavoring agent, and is matched with esters such as ethyl lactate with fruit flavor acetic acid isoamyl ester and butyrate isoamyl ester, fruit milk flavor with soft fruit flavor, wine flavor and cream flavor, delta decalactone with cream flavor and fruit milk flavor and the like, the obtained fruit milk flavor type feed flavoring agent accords with the preference of smell and taste of animals, has high fragrance joyful degree and good stability, and can effectively attract animals to eat; when the additive is added into the feed, the flavor of the feed can be improved and coordinated, the palatability of the feed is improved, animals are induced to eat the feed, the feed intake is obviously increased, the weight gain is improved, and the diarrhea rate can be reduced.
Detailed Description
The examples of the present invention are provided for illustrative purposes only and are not to be construed as limiting the invention.
The cream lactone described in the following examples was prepared by the following method: esterifying 2 per mill lipase with the rest butter at 60 deg.C for 7 hr to obtain butter lactone.
Example 1
A fruit milk fragrance type feed flavoring agent comprises the following components in parts by weight:
10 parts of ethyl butyrate;
butyric acid 15 parts
5 parts of ethyl lactate;
3 parts of acetic acid;
10 parts of isoamyl acetate;
10 parts of isoamyl butyrate;
16 parts of benzyl alcohol;
3 parts of ethyl maltol;
5 parts of capric acid;
20 parts of coconut aldehyde;
15 parts of ethyl decanoate;
5 parts of peach aldehyde;
5 parts of ethyl dodecanoate;
30 parts of butter lactone;
10 parts of glycerol triacetate;
838 parts of rice bran.
The preparation method of the fruit milk flavor type feed flavoring agent is characterized by comprising the following steps:
s1, preparing raw materials according to the proportion, putting cream lactone and other raw materials except a carrier into a reaction kettle in a sequence of firstly solid and then liquid, stirring and mixing for 2 hours at constant temperature, and after uniform mixing is finished, sealing and placing the mixture for aging for 12 hours;
s2, firstly, carrying out mixing adsorption on the aged mixture obtained in the step S1 for 6min by using 40% carrier rice bran, then carrying out secondary mixing for 7.5min by using the rest carrier, discharging materials after the mixing is finished, and sieving the materials by using a vibrating screen to obtain the flavoring agent.
Example 2
A fruit milk fragrance type feed flavoring agent comprises the following components in parts by weight:
15 parts of ethyl butyrate;
10 parts of butyric acid;
10 parts of ethyl lactate;
1 part of acetic acid;
17 parts of isoamyl acetate;
15 parts of isoamyl butyrate;
10 parts of benzyl alcohol;
5 parts of ethyl maltol;
10 parts of capric acid;
10 parts of coconut aldehyde;
10 parts of ethyl decanoate;
8 parts of peach aldehyde;
3 parts of ethyl dodecanoate;
20 parts of butter lactone;
20 parts of glycerol triacetate;
836 portions of rice bran.
The preparation method of the fruit milk flavor type feed flavoring agent is basically the same as that of the embodiment 1, and the description is omitted.
Example 3
A fruit milk fragrance type feed flavoring agent comprises the following components in parts by weight:
5 parts of ethyl butyrate;
20 parts of butyric acid;
15 parts of ethyl lactate;
0.5 part of acetic acid;
3 parts of isoamyl acetate;
30 parts of isoamyl butyrate;
5 parts of benzyl alcohol;
18 parts of ethyl maltol;
16.5 parts of capric acid;
30 parts of coconut aldehyde;
3 parts of ethyl decanoate;
peach aldehyde 15 parts;
1 part of ethyl dodecanoate;
10 parts of butter lactone;
48 parts of glycerol triacetate;
780 parts of rice bran.
The preparation method of the fruit milk flavor type feed flavoring agent is basically the same as that of the embodiment 1, and the description is omitted.
The fruit milk flavored feed flavourings described in examples 1 to 3 were subjected to a product performance test according to the following protocol:
first, qualitative test
Setting daily ration: the fruit milk flavored feed rations according to examples 1 to 3 were added to the basal ration at an addition of 500g/t, and designated as groups a1, a2, A3, respectively, and the basal ration without fruit milk flavored feed rations was set as a blank control group a 0.
Selecting a pigsty: selecting 2 piggeries, wherein 6 weaned piglets in each piggery have the same variety and similar weight, and each piggery is provided with 4 labeled troughs. (the trough is placed in the DV video camera)
The specific experimental scheme includes that according to the fairness principle, control daily ration and test daily ration are respectively contained in troughs of each fence to be fed by animals, feeding trough positions are randomly changed once a day, animal feeding behaviors are observed and recorded, the experimental scheme is divided into a ① sea selection stage, wherein 4 troughs are placed at four corners of a pigsty, control daily ration A0 and test daily ration A1, A2 and A3 are respectively contained in the four troughs of the pigsty to be fed by the animals, feeding trough positions must be randomly changed every day, 2 best-effect fragrance types are selected by comparison, a ② club decision stage is that 2 troughs are placed in each pigsty, ① is referred to in the experimental process, and the favorite fragrance types of piglets are selected by comparison.
Through experimental observation, the number of piglets eating the experimental diets A0, A1, A2 and A3 is arranged as follows: a1 > A2 > A3 > A0. Therefore, the fruit milk flavor type feed flavoring agent provided by the invention accords with the olfactory and gustatory preferences of animals, and can effectively attract the animals to eat.
Second, quantitative test
According to the results of qualitative experiments, the dietary test ration A1 was selected as the experimental group and the basal dietary A0 was selected as the blank control group. Selecting 2 piglets, wherein the weaning age is 24-26 days, 8 piglets in each piglet, respectively containing an experimental group edible test diet A1 and a blank control group basic diet A0 for feeding the piglets, and recording the average feed intake of 1-9 days. The results are shown in Table 1.
TABLE 1
The overall average growth index of piglets is shown in table 2.
TABLE 2
| Test items | A1 | A0 |
| Initial weight (kg/head) of test | 7.93 | 7.92 |
| Weight balance at end of test (kg/head) | 9.79 | 9.65 |
| Average daily food intake (g/d/head) in the first 3 days | 121.25 | 113.44 |
| Average daily food intake (g/d/head) | 199.31 | 178.37 |
| Average daily gain (g/d/head) | 186.50 | 173.06 |
| Average feed conversion ratio | 1.15 | 1.14 |
| Average diarrhea percentage (%) | 0.83 | 1.88 |
From the experimental results in table 2, it can be seen that the average food consumption of the first three days of the experimental group is increased by 6.89% compared with that of the blank control group, the average food consumption of the experimental group for 9 days of the whole experimental period is increased by 11.74% compared with that of the blank control group, and the average daily gain of the experimental group is increased by 7.77% compared with that of the blank control group. Therefore, the fruit milk flavor type feed flavoring agent can improve and coordinate the feed flavor, improve the feed palatability, lure animals to eat, increase the feed intake, increase the weight gain and reduce the diarrhea rate.
It should be understood that the above-mentioned embodiments of the present invention are only examples for clearly illustrating the technical solutions of the present invention, and are not intended to limit the specific embodiments of the present invention. Any modification, equivalent replacement, and improvement made within the spirit and principle of the present invention claims should be included in the protection scope of the present invention claims.
Claims (8)
1. A fruit milk fragrance type feed flavoring agent is characterized by comprising the following components in parts by weight: 5-15 parts of ethyl butyrate; 8-20 parts of butyric acid; 1-15 parts of ethyl lactate; 0.5-3 parts of acetic acid; 3-17 parts of isoamyl acetate; 10-30 parts of isoamyl butyrate; 5-16 parts of benzyl alcohol; 1-18 parts of ethyl maltol; 1-18 parts of capric acid; 10-30 parts of coconut aldehyde; 3-15 parts of ethyl decanoate; 3-15 parts of peach aldehyde; 1-5 parts of ethyl dodecanoate; 10-30 parts of butter lactone; 3-50 parts of a non-toxic solvent; 100-1000 parts of a carrier.
2. The fruit milk flavored feed flavoring according to claim 1, wherein said fruit milk flavored feed flavoring comprises the following components in parts by weight: 10-15 parts of ethyl butyrate; 10-15 parts of butyric acid; 5-10 parts of ethyl lactate; 1-3 parts of acetic acid; 10-17 parts of isoamyl acetate; 10-15 parts of isoamyl butyrate; 2-5 parts of ethyl maltol; 3-10 parts of capric acid; 10-20 parts of coconut aldehyde; 10-15 parts of ethyl decanoate; 3-8 parts of peach aldehyde; 3-5 parts of ethyl dodecanoate; 20-30 parts of butter lactone; 10-20 parts of a non-toxic solvent; 700-900 parts of a carrier.
3. The fruit milk flavored feed flavoring according to claim 1, wherein said carrier is one or more of silica, dextrose, stone powder, rice bran.
4. The fruit milk flavor feed flavoring according to claim 1, wherein the non-toxic solvent is one or more of propylene glycol, triacetin, and ethanol.
5. The fruit milk flavored feed flavoring according to claim 1, wherein said creamy lactone is obtained by esterification of a lipase with butter.
6. The fruit milk flavored feed flavoring according to claim 5, wherein said cream lactone is prepared by the following process: and (3) carrying out esterification reaction on 1-5 per mill of lipase and the balance of butter at 50-70 ℃ for 6-8 h to obtain the cream lactone.
7. The method of producing a fruit milk flavored feed stuff according to any of claims 1 to 6, characterized in that it comprises the following steps:
s1, stirring and mixing the cream lactone and other raw materials except a carrier at constant temperature, and then sealing, standing and aging for more than 10 hours;
s2, firstly, mixing and adsorbing the aged mixture obtained in the step S1 for 2-10 min by using 10-70% of carriers, and then, secondarily mixing the rest carriers for 5-10 min.
8. The flavor with fruit milk flavor according to claim 1, wherein the ingredients other than the carrier in step S1 are added in order of solid first and liquid second.
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| CN112868928A (en) * | 2021-02-09 | 2021-06-01 | 中国农业大学 | Application of flavoring agent in regulating intestinal microorganisms of sow and improving reproductive performance |
| CN112998134A (en) * | 2021-04-08 | 2021-06-22 | 成都朴瑞威饲料科技有限公司 | Feed flavoring agent with function of inhibiting intestinal harmful bacteria and preparation method thereof |
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| CN111821296A (en) * | 2020-07-24 | 2020-10-27 | 河南思迈尔健康科技有限公司 | Substance for regulating and controlling hunger sensation hormone of organism and application thereof |
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