CN106954737A - A kind of milk flavoured type feedstuff flavouring agent and preparation method thereof - Google Patents
A kind of milk flavoured type feedstuff flavouring agent and preparation method thereof Download PDFInfo
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- CN106954737A CN106954737A CN201710189162.8A CN201710189162A CN106954737A CN 106954737 A CN106954737 A CN 106954737A CN 201710189162 A CN201710189162 A CN 201710189162A CN 106954737 A CN106954737 A CN 106954737A
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Abstract
The invention discloses a kind of milk flavoured type feedstuff flavouring agent, include each raw material components of following weight parts composition:1 ~ 15 part of ethyl acetate, 10 ~ 60 parts of Ethyl vanillin, 1 ~ 15 part of ethyl lactate, 1 ~ 18 part of octanoic acid, 3 ~ 17 parts of butyric acid, 0.5 ~ 10 part of furanone, 1 ~ 15 part of ethyl oleate, 3 ~ 15 parts of delta-decalactone, 1 ~ 18 part of capric acid, 1 ~ 18 part of the dodecalactone in fourth position, 10 ~ 60 parts of cream lactone, 3 ~ 50 parts of solvent, 200 ~ 1000 parts of carrier;The solvent includes the one or more in propane diols, triacetyl glycerine, ethanol;The carrier includes the one or more in silica, glucose, stone flour, rice bran.The present invention relates to field of fodder, the milk fragrance of milk flavoured type feedstuff flavouring agent has been established by component cream lactone, it is equipped with the esters such as ethyl acetate, ethyl lactate, ethyl oleate, delta-decalactone and fourth position dodecalactone, and prepared according to aforementioned proportion, obtained milk flavoured type feedstuff flavouring agent meet animal smell, sense of taste preference, fragrance pleasure degree is high, good stability, lures feed intake, improves weightening.
Description
Technical field
The present invention relates to field of fodder, more particularly to a kind of milk flavoured type feedstuff flavouring agent and preparation method thereof.
Background technology
Feedstuff flavouring agent is physiological property according to different animals in different growth phases, dietary habit, to improve feed
Attractant and palatability and be added to the fragrant non-nutritional feed additive in feed.Feed nutrition, feed intake
It is to ensure livestock birds health growth and three key elements efficiently produced with digesting and assimilating.But feed industry personage it is of interest mainly
Nutrient content in feed how to meet the nutritional requirements of livestock and poultry and usually ignore be implied between the two one it is crucial because
Element --- feed intake.Numerous studies show:Feed efficiency, growth of animal potential play, Reproduction performance all with feeding
Amount is closely related, and the palatability of feed affects feed intake, and actually any formula is all using certain feed intake as base
Plinth design, feed palatability is bad, and feed intake declines, and certainly will influence the total amount of nutrients intake, undoubtedly also influence whether feed
Effect.In husbandry sector, with the raising of productivity, the nutriment ensured in daily ration is not required nothing more than, feed is also required
There are good palatability and enough feed intakes, just can guarantee that aggregate demand of the livestock and poultry to nutrient, therefore, people are generally in feed
Feedstuff flavouring agent is added to improve the palatability of feed, so as to improve the feed intake of livestock and poultry.
In terms of flavouring agent, research finds that various flavouring agents have huge difference to the phagostimulating effect of animal, and some hear
The odor type animal for hobby of getting up not necessarily is liked.Flavouring agent is mainly induced and played a role by the smell of animal, but smell is given birth to
The quantity of olfactory cell determines the acuity of smell in the area and epithelium of reason research discovery smell mucous epithelium, therefore, no
It can to select flavouring agent for animal according only to the sense organ identification of people, it is necessary to, could be real according to the smelling of animal, sense of taste physilogical characteristics
Flavouring agent is selected from animal sense organ physiological angle.The exploitation of feedstuff flavouring agent fragrance has to comply with the habit of animal with selection, full
Hobby of the sufficient animal in different growth phases to some special aromas.And existing feedstuff flavouring agent still has and is unsatisfactory for animal
The problem of itself preference local flavor, feeding can only be promoted to a certain extent, fragrance is unstable, uniformity coefficient during incorporation feed
Difference, and the uniformity coefficient of its incorporation will influence feed intake.Therefore, it is necessary to be improved to prior art.
The content of the invention
There is provided a kind of milk of the pure powder local flavor of simulation to overcome at least one deficiency described in above-mentioned prior art by the present invention
Type feedstuff flavouring agent, improves and coordinates feed local flavor, improves feed palatability.It is another object of the present invention to provide described
The preparation method of milk flavoured type feedstuff flavouring agent.
In order to solve the above-mentioned technical problem, the present invention is achieved by the following technical programs:
A kind of milk flavoured type feedstuff flavouring agent, includes each raw material components of following weight parts composition:1 ~ 15 part of ethyl acetate, ethyl is fragrant
Blue 10 ~ 60 parts of element, 1 ~ 15 part of ethyl lactate, 1 ~ 18 part of octanoic acid, 3 ~ 17 parts of butyric acid, 0.5 ~ 10 part of furanone, ethyl oleate 1 ~ 15
Part, 3 ~ 15 parts of delta-decalactone, 1 ~ 18 part of capric acid, 1 ~ 18 part of the dodecalactone in fourth position, 10 ~ 60 parts of cream lactone cream lactone is molten
3 ~ 50 parts of agent, 200 ~ 1000 parts of carrier;
The cream lactone includes 1 ~ 5 ‰ lipase and the butter of surplus is made by esterification;
The solvent includes the one or more in propane diols, triacetyl glycerine, ethanol;
The carrier includes the one or more in silica, glucose, stone flour, rice bran.
The present invention is according to the smelling of animal, sense of taste physilogical characteristics, the preference to milk odor type, the physiological threshold to milk fragrance etc.
Combined factors consider that the odor type of product, head be fragrant and fragrance keeping period, obtain cream lactone using butter and esterification by lipase reaction reaction and will
It goes out above-mentioned milk flavoured type feedstuff flavouring agent formula with other components mixing preparation, and milk has been established by component cream lactone cream lactone
The milk fragrance of odor type feedstuff flavouring agent, is equipped with the ethyl acetate with fruity and aroma, with soft fruity, aroma, creamy
The ethyl lactate of gas, the ethyl oleate with the fragrance of a flower and the delta-decalactone with cream fragrance fruity fragrance and fourth position 12
The esters such as lactone, and prepared according to aforementioned proportion, obtain meeting the milk flavoured type feedstuff flavouring agent of animal preference, be added into feed
In, improve and coordinate feed local flavor, improve feed palatability, lure feed intake, increase feed intake, improve weightening.Carrier
Species on the fragrance keeping period of flavouring agent, in feed mixing uniformity influence it is larger, the present invention using silica, glucose,
One or more in stone flour, rice bran are as carrier, and obtained flavouring agent has longer fragrance keeping period, and can be mixed in feed
Uniformly, it is uniform to improve feed palatability.The present invention is in product formula structure, before the local flavor and cost performance of product is not influenceed
Put, increase the ratio of the raw material of good stability so that obtained flavouring agent has good stability.
Preferably, the milk flavoured type feedstuff flavouring agent includes each raw material components that following weight parts are constituted:Ethyl acetate 3 ~
10 parts, 15 ~ 50 parts of Ethyl vanillin, 3 ~ 10 parts of ethyl lactate, 3 ~ 13 parts of octanoic acid, 5 ~ 12 parts of butyric acid, 1 ~ 8 part of furanone, oleic acid
3 ~ 10 parts of ethyl ester, 5 ~ 10 parts of delta-decalactone, 3 ~ 13 parts of capric acid, 3 ~ 13 parts of the dodecalactone in fourth position, cream lactone cream lactone 15 ~
50 parts, 5 ~ 40 parts of solvent, 0 ~ 900 part of carrier 30 as one kind.
A kind of method for preparing the milk flavoured type feedstuff flavouring agent, comprises the following steps:
S1. cream lactone is made in the butter esterification of 1 ~ 5 ‰ lipase and surplus;
S2. closed place is aged after cream lactone made from step S1 is mixed with other raw material constant temperature stirring in addition to carrier
More than 10h;
S3. the mixture after being aged with carrier to step S2 carries out mixing and absorption, obtains flavouring agent.
Further, in step S1, esterification reacts 6 ~ 8h at 50 ~ 70 DEG C, may advantageously facilitate lipase and butter
Between esterification, promote fragrance release, reduce cream lactone consumption, not only improved feed intake but also be conducive to saving into
This, while also helping the absorption for promoting animal to nutriment.
In step S2, the raw material in addition to carrier is fed intake according to the order of liquid after first solid, enough to solid dissolving
Time makes each component be sufficiently mixed uniformly.
In step S2,1 ~ 3h of constant temperature stirring mixing.Each raw material mixes more uniform in raw material stirring mixed process, in order to
Well mixed, mixing time is unsuitable too short;The long one side of mixing time extends manufacture cycle raising production cost, on the other hand
A period of time is needed to be aged after the completion of raw material mixing, stirring is unfavorable for the progress of ageing.
It is closed to place ageing more than 12h in step S2.Mixing needs ageing for some time after finishing, remove precipitation
In the impurity that contains, the time too short removal for being unfavorable for impurity, each raw material interaction, fragrance when reaching terminal in ageing process
Become harmonious, mellow and full, soft.
In step S3, the mixture after being first aged with 10 ~ 70wt% carrier to step S1 carries out mixing and absorption, then with remaining
Under carrier carry out secondary mixing, obtain flavouring agent.
In step S3, the mixture after the ageing first obtained with 10 ~ 70wt% carrier to step S1 carry out mixing and absorption 2 ~
10min, then carry out with remaining carrier 5 ~ 10min of secondary mixing.In order that the liquid mixture after ageing is uniformly mixed with carrier
Close, mixed process is carried out in two times so that mixing is more uniformly distributed, reduce the coefficient of variation.
In step S3, complete vibration screening after mixing and obtain flavouring agent.Mixture mixed with carrier after vibration screening, it is to avoid just
Bonded between the flavouring agent particle just produced, so as to improve its uniformity coefficient mixed with feed, and then increase dynamic
Thing feed intake, improves weightening, improves efficiency of feed utilization, reduces feed cost to plant, increases the benefit.
Compared with prior art, the present invention has the advantages that:
The present invention takes thing to establish the milk fragrance of milk flavoured type feedstuff flavouring agent by cream lactone, is equipped with the second with fruity and aroma
Acetoacetic ester, with soft fruity, aroma, butter aroma ethyl lactate, ethyl oleate with the fragrance of a flower and with creamy
The esters such as delta-decalactone and fourth the position dodecalactone of taste fruity fragrance, and prepared according to aforementioned proportion, obtained milk flavoured type is raised
Material flavouring agent meets the smell of animal, sense of taste preference, and fragrance pleasure degree is high, good stability, can effectively attract feed intake, add
Add in feed, improve and coordinate feed local flavor, improve feed palatability, lure feed intake, hence it is evident that increase feed intake, improve
Weightening.Mixing is sieved after completing through vibratory sieve, and obtained feedstuff flavouring agent is in microballon shape, good fluidity, do not lumpd, so as to improve
Its uniformity coefficient mixed with feed, and then increase animal feed intake.
Embodiment
In order to allow those skilled in the art to more fully understand technical scheme, with reference to the present invention is made into
One step is illustrated, but embodiment is not limited in any form to the present invention.
Embodiment 1
A kind of milk flavoured type feedstuff flavouring agent described in the present embodiment includes each component of following parts by weight:6.5 parts of ethyl acetate,
32.5 parts of Ethyl vanillin, 6.5 parts of ethyl lactate, 8 parts of octanoic acid, 8.5 parts of butyric acid, 4.5 parts of furanone, 6.5 parts of ethyl oleate, fourth
7.5 parts of the decalactone in position, 8 parts of capric acid, 8 parts of the dodecalactone in fourth position, 32.5 parts of cream lactone, 22.5 parts of solvent, 600 parts of carrier.
The cream lactone includes 3 ‰ lipase and the butter of surplus is made by esterification;
The solvent includes propane diols, triacetyl glycerine, ethanol;
The carrier includes silica, glucose, stone flour, rice bran.
The preparation method of described milk flavoured type feedstuff flavouring agent comprises the following steps:
S1. by 3 ‰ lipase and the butter of surplus, cream lactone is made in esterification 7h at 60 DEG C;
S2. raw material is got ready by the proportioning, by cream lactone made from step S1 and other raw materials in addition to carrier according to first solid
After body in the order input reactor of liquid, closed place of mixture is aged by constant temperature stirring mixing 2h, uniform mixing after finishing
12h;
S3. the mixture after the ageing first obtained with 40% carrier to step S2 carries out mixing and absorption 6min, then is carried with remaining
Body carries out secondary mixing 7.5min, completes after mixing blowing and is sieved to obtain flavouring agent through vibratory sieve.
Embodiment 2
The present embodiment is in addition to the parts by weight composition of each raw material components is different, other be the same as Examples 1.
The milk flavoured type feedstuff flavouring agent includes each component of following parts by weight:3 parts of ethyl acetate, Ethyl vanillin 15
Part, 3 parts of ethyl lactate, 3 parts of octanoic acid, 5 parts of butyric acid, 1 part of furanone, 3 parts of ethyl oleate, 5 parts of delta-decalactone, 3 parts of capric acid, fourth
3 parts of the dodecalactone in position, 15 parts of cream lactone, 5 parts of solvent, 0 part of carrier 30 as one kind.
Embodiment 3
The present embodiment is in addition to the parts by weight composition of each raw material components is different, other be the same as Examples 1.
The milk flavoured type feedstuff flavouring agent includes each component of following parts by weight:10 parts of ethyl acetate, Ethyl vanillin
50 parts, 10 parts of ethyl lactate, 13 parts of octanoic acid, 12 parts of butyric acid, 8 parts of furanone, 10 parts of ethyl oleate, 10 parts of delta-decalactone, the last of the ten Heavenly stems
13 parts of acid, 13 parts of the dodecalactone in fourth position, 50 parts of cream lactone, 40 parts of solvent, 900 parts of carrier.
Embodiment 4
The present embodiment is in addition to the parts by weight composition of each raw material components is different, other be the same as Examples 1.
The milk flavoured type feedstuff flavouring agent includes each component of following parts by weight:1 part of ethyl acetate, Ethyl vanillin 10
Part, 1 part of ethyl lactate, 1 part of octanoic acid, 3 parts of butyric acid, 0.5 part of furanone, 1 part of ethyl oleate, 3 parts of delta-decalactone, 1 part of capric acid,
1 part of the dodecalactone in fourth position, 10 parts of cream lactone, 3 parts of solvent, 200 parts of carrier.
Embodiment 5
The present embodiment is in addition to the parts by weight composition of each raw material components is different, other be the same as Examples 1.
The milk flavoured type feedstuff flavouring agent includes each component of following parts by weight:15 parts of ethyl acetate, Ethyl vanillin
60 parts, 15 parts of ethyl lactate, 18 parts of octanoic acid, 17 parts of butyric acid, 10 parts of furanone, 15 parts of ethyl oleate, 15 parts of delta-decalactone, the last of the ten Heavenly stems
18 parts of acid, 18 parts of the dodecalactone in fourth position, 60 parts of cream lactone, 50 parts of solvent, 1000 parts of carrier.
Embodiment 6
The present embodiment is in addition to the composition of cream lactone, solvent and carrier is different, other be the same as Examples 1.
The cream lactone includes 1 ‰ lipase and the butter of surplus is made by esterification;
The solvent includes propane diols, triacetyl glycerine, ethanol;
The carrier includes silica, glucose, stone flour.
Embodiment 7
The present embodiment is in addition to the composition of cream lactone, solvent and carrier is different, other be the same as Examples 1.
The cream lactone includes 5 ‰ lipase and the butter of surplus is made by esterification;
The solvent includes triacetyl glycerine, ethanol;
The carrier includes glucose, stone flour, rice bran.
Embodiment 8
The present embodiment is in addition to solvent is different with the composition of carrier, other be the same as Examples 1.
The solvent includes propane diols;
The carrier includes silica.
Embodiment 9
The present embodiment is in addition to the preparation process of flavouring agent is different, other be the same as Examples 1.
S1. by 3 ‰ lipase and the butter of surplus, cream lactone is made in esterification 6h at 50 DEG C;
S2. raw material is got ready by the proportioning, by cream lactone made from step S1 and other raw materials in addition to carrier according to first solid
After body in the order input reactor of liquid, closed place of mixture is aged by constant temperature stirring mixing 1h, uniform mixing after finishing
More than 10h;
S3. the mixture after the ageing first obtained with 10% carrier to step S2 carries out mixing and absorption 2min, then is carried with remaining
Body carries out secondary mixing 10min, completes after mixing blowing and is sieved to obtain flavouring agent through vibratory sieve.
Embodiment 10
The present embodiment is in addition to the preparation process of flavouring agent is different, other be the same as Examples 1.
S1. by 3 ‰ lipase and the butter of surplus, cream lactone is made in esterification 8h at 70 DEG C;
S2. raw material is got ready by the proportioning, by cream lactone made from step S1 and other raw materials in addition to carrier according to first solid
After body in the order input reactor of liquid, closed place of mixture is aged by constant temperature stirring mixing 3h, uniform mixing after finishing
15h;
S3. the mixture after the ageing first obtained with 70% carrier to step S2 carries out mixing and absorption 10min, then with remaining
Carrier carries out secondary mixing 5min, completes after mixing blowing and is sieved to obtain flavouring agent through vibratory sieve.
Test method
1st, method:Select that kind is identical, body weight is close, the outer ternary piglet 88 of health in 28 day age, be randomly divided into 11 groups, bag
10 test groups and 1 blank control group are included, every group of 8 pigs add the flavouring agent of embodiment 1 in the feed of test group 1,
The flavouring agent of embodiment 2 is added in the feed of test group 2, by that analogy, embodiment 3 ~ 10 is added respectively in test group 3 ~ 10
Flavouring agent, blank control group is without flavouring agent.The addition of flavouring agent is 500g/ tons, and experiment is carried out 3 weeks.
2. result of the test
Starting weight/kg | Whole weight/kg | Average weight increasing a day/g | Average daily feed intake/g | Feedstuff-meat ratio(F/G) | |
Test group 1 | 6.44 | 14.52 | 288.44 | 451.44 | 1.57 |
Test group 2 | 6.45 | 14.54 | 289.06 | 477.50 | 1.65 |
Test group 3 | 6.54 | 14.55 | 286.26 | 463.89 | 1.62 |
Test group 4 | 6.45 | 14.19 | 276.46 | 435.14 | 1.57 |
Test group 5 | 6.50 | 14.07 | 270.30 | 429.19 | 1.59 |
Test group 6 | 6.53 | 13.89 | 262.84 | 419.21 | 1.59 |
Test group 7 | 6.52 | 14.14 | 272.07 | 424.17 | 1.56 |
Test group 8 | 6.49 | 14.21 | 275.71 | 434.49 | 1.58 |
Test group 9 | 6.48 | 14.07 | 271.05 | 451.17 | 1.66 |
Test group 10 | 6.49 | 14.11 | 272.23 | 458.43 | 1.68 |
Control group | 6.50 | 13.21 | 239.64 | 421.80 | 1.76 |
Raising of the flavouring agent of embodiment 1 ~ 10 to piglet feed intake has obvious in the present invention it can be seen from data above
Contribution, the average daily feed intake that with the addition of the piglet of the test group of the flavouring agent of embodiment 1 ~ 10 is substantially better than control group, Average weight increasing a day
Also had a clear superiority with feedstuff-meat ratio, the digestibility and utilization of feed is also promoted while piglet feeding is promoted, cultivation effect is improved
Benefit.
Claims (10)
1. a kind of milk flavoured type feedstuff flavouring agent, it is characterised in that each raw material components constituted including following weight parts:Ethyl acetate
1 ~ 15 part, 10 ~ 60 parts of Ethyl vanillin, 1 ~ 15 part of ethyl lactate, 1 ~ 18 part of octanoic acid, 3 ~ 17 parts of butyric acid, 0.5 ~ 10 part of furanone,
In 1 ~ 15 part of ethyl oleate, 3 ~ 15 parts of delta-decalactone, 1 ~ 18 part of capric acid, 1 ~ 18 part of the dodecalactone in fourth position, cream lactone cream
10 ~ 60 parts of ester, 3 ~ 50 parts of solvent, 200 ~ 1000 parts of carrier;
The cream lactone includes 1 ~ 5 ‰ lipase and the butter of surplus is made by esterification;
The solvent includes the one or more in propane diols, triacetyl glycerine, ethanol;
The carrier includes the one or more in silica, glucose, stone flour, rice bran.
2. milk flavoured type feedstuff flavouring agent according to claim 1, it is characterised in that each original constituted including following weight parts
Expect component:3 ~ 10 parts of ethyl acetate, 15 ~ 50 parts of Ethyl vanillin, 3 ~ 10 parts of ethyl lactate, 3 ~ 13 parts of octanoic acid, 5 ~ 12 parts of butyric acid,
1 ~ 8 part of furanone, 3 ~ 10 parts of ethyl oleate, 5 ~ 10 parts of delta-decalactone, 3 ~ 13 parts of capric acid, 3 ~ 13 parts of the dodecalactone in fourth position, milk
Oily 15 ~ 50 parts of lactone cream lactone, 5 ~ 40 parts of solvent, 0 ~ 900 part of carrier 30 as one kind.
3. the method that one kind prepares the milk flavoured type feedstuff flavouring agent described in any one of claim 1 ~ 2, it is characterised in that including such as
Lower step:
S1. cream lactone is made in the butter esterification of 1 ~ 5 ‰ lipase and surplus;
S2. closed place is aged after cream lactone made from step S1 is mixed with other raw material constant temperature stirring in addition to carrier;
S3. the mixture after being aged with carrier to step S2 carries out mixing and absorption, obtains flavouring agent.
4. the preparation method of milk flavoured type feedstuff flavouring agent according to claim 3, it is characterised in that in step S1, esterification
6 ~ 8h is reacted in reaction at 50 ~ 70 DEG C.
5. the preparation method of milk flavoured type feedstuff flavouring agent according to claim 3, it is characterised in that in step S2, will be removed
Raw material outside carrier feeds intake mixing according to the order of liquid after first solid.
6. the preparation method of milk flavoured type feedstuff flavouring agent according to claim 3, it is characterised in that in step S2, constant temperature
1 ~ 3h of stirring mixing.
7. the preparation method of milk flavoured type feedstuff flavouring agent according to claim 3, it is characterised in that closed in step S2
Place ageing more than 12h.
8. the preparation method of milk flavoured type feedstuff flavouring agent according to claim 3, it is characterised in that in step S3, first use
Mixture after 10 ~ 70wt% carrier is aged to step S1 carries out mixing and absorption, then carries out with remaining carrier secondary mixing,
Obtain flavouring agent.
9. the preparation method of milk flavoured type feedstuff flavouring agent according to claim 7, it is characterised in that in step S3, first use
Mixture after the ageing that 10 ~ 70wt% carrier is obtained to step S1 carries out 2 ~ 10min of mixing and absorption, then uses remaining carrier
Carry out 5 ~ 10min of secondary mixing.
10. the preparation method of milk flavoured type feedstuff flavouring agent according to claim 7, it is characterised in that in step S3, is completed
Vibration screening obtains flavouring agent after mixing.
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CN108740348A (en) * | 2018-05-15 | 2018-11-06 | 成都大帝汉克生物科技有限公司 | A kind of sweet citrus type house ox feedstuff flavouring agent and preparation method thereof |
CN109864203A (en) * | 2019-03-14 | 2019-06-11 | 仲恺农业工程学院 | Food calling milk-flavor base material for promoting pet to eat and preparation and use processes |
CN111096394A (en) * | 2019-12-31 | 2020-05-05 | 广东瑞生科技集团有限公司 | Fruit milk fragrance type feed flavoring agent and preparation method thereof |
CN111821296A (en) * | 2020-07-24 | 2020-10-27 | 河南思迈尔健康科技有限公司 | Substance for regulating and controlling hunger sensation hormone of organism and application thereof |
CN113057254A (en) * | 2021-04-28 | 2021-07-02 | 味氏(广东)生物科技股份有限公司 | Preparation method and application of water-soluble sweet milk essence suitable for drinking water, porridge material and liquid feed of mammals |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108740348A (en) * | 2018-05-15 | 2018-11-06 | 成都大帝汉克生物科技有限公司 | A kind of sweet citrus type house ox feedstuff flavouring agent and preparation method thereof |
CN109864203A (en) * | 2019-03-14 | 2019-06-11 | 仲恺农业工程学院 | Food calling milk-flavor base material for promoting pet to eat and preparation and use processes |
CN111096394A (en) * | 2019-12-31 | 2020-05-05 | 广东瑞生科技集团有限公司 | Fruit milk fragrance type feed flavoring agent and preparation method thereof |
CN111821296A (en) * | 2020-07-24 | 2020-10-27 | 河南思迈尔健康科技有限公司 | Substance for regulating and controlling hunger sensation hormone of organism and application thereof |
CN113057254A (en) * | 2021-04-28 | 2021-07-02 | 味氏(广东)生物科技股份有限公司 | Preparation method and application of water-soluble sweet milk essence suitable for drinking water, porridge material and liquid feed of mammals |
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