CN103636944B - Flavouring agent of a kind of toffee local flavor and preparation method thereof - Google Patents
Flavouring agent of a kind of toffee local flavor and preparation method thereof Download PDFInfo
- Publication number
- CN103636944B CN103636944B CN201310643076.1A CN201310643076A CN103636944B CN 103636944 B CN103636944 B CN 103636944B CN 201310643076 A CN201310643076 A CN 201310643076A CN 103636944 B CN103636944 B CN 103636944B
- Authority
- CN
- China
- Prior art keywords
- flavouring agent
- ethyl
- parts
- decalactone
- feed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Fodder In General (AREA)
Abstract
The present invention relates to flavouring agent of a kind of toffee local flavor and preparation method thereof, this flavouring agent is made up of following weight portion formula, it is 100 parts in the gross weight of flavouring agent, butyric acid 0.05 ~ 3 part, butyl butyryl lactate 0.2 ~ 0.8 part, ethyl lactate 0.1 ~ 0.5 part, ethyl butyrate 0.05 ~ 0.5 part, ethyl laurate 0.5 ~ 3 part, nonyl lactone 0.8 ~ 2 part, γ-decalactone 0.1 ~ 1 part, δ-decalactone 0.2 ~ 3 part, Ethyl vanillin 0.5 ~ 5 part, dodecoic acid 0.5 ~ 5 part, linalool 0.05 ~ 5 part, adsorbent silica 20 ~ 30 parts, 60 ~ 70 parts, carrier.Compared with prior art, flavouring agent of the present invention, toffee unique flavor, fragrance identification is high, toffee pure flavor, fragrance is joyful comfortable, can improve phagostimulating effect, good with the compatibility of feed, the bitter taste that feedstuff contains can be covered, improve the palatability of feed, promote searching for food of animal.
Description
Technical field
The present invention relates to a kind of toffee local flavor flavouring agent and preparation method thereof, and the application of this flavouring agent in feed or pet food.
Background technology
In animal farming industry, the economic benefit of raiser and the growth conditions of animal are maintained close ties with, and the growth conditions of animal is mainly subject to the impact of nutrition condition.Therefore raiser mainly through the feed of comprehensive nutrition of feeding to ensure the healthy growth of animal.And the feed of routine comprises soybean, dregs of beans, corn, fish meal, the assorted dregs of rice, amino acid etc. raw material, these raw materials are separately containing different breaths, add to and can produce heavy bad breath together, the palatability of animal is had an impact with searching for food, and then affect the healthy growth of animal, finally cause the economic benefit of raiser to decline, therefore need to use flavouring agent to improve palatability to cover bad smell.
Flavouring agent is at the physiological characteristic of Different growth phases and dietary habit according to different animals, for improving palatability, the attractant of feed, increase feed intake, improve feed and veterinary drug quality and a kind of odor additive of adding to wherein, generally by perfume base, adsorbent and carrier three part form.
Now commercially there is a lot of flavouring agent product, but some problem of ubiquity: the impure attraction of fragrance not animal; The excessive stimulating animal sense of smell of aroma strength causes detests sense; Fragrance is stable not, easily spoiled, poor with feed compatibility; Really cannot play the effect improving animal feed intake.
At present, the flavouring agent of a kind of new feed or pet food is needed.
Summary of the invention
For prior art Problems existing, the object of the invention is to solve fragrance pure and possess functional diversities, with feed compatibility good, improve the effects such as feed intake.
For achieving the above object, the invention provides a kind of flavouring agent, this flavouring agent is made up of following weight portion formula, it is 100 parts in the gross weight of flavouring agent, butyric acid 0.05 ~ 3 part, butyl butyryl lactate 0.2 ~ 0.8 part, ethyl lactate 0.1 ~ 0.5 part, ethyl butyrate 0.05 ~ 0.5 part, ethyl laurate 0.5 ~ 3 part, nonyl lactone 0.8 ~ 2 part, γ-decalactone 0.1 ~ 1 part, δ-decalactone 0.2 ~ 3 part, Ethyl vanillin 0.5 ~ 5 part, dodecoic acid 0.5 ~ 5 part, linalool 0.05 ~ 5 part, adsorbent silica 20 ~ 30 parts, 60 ~ 70 parts, carrier.
Described carrier is any one in anhydrous saccharin sodium, powdered whiting and anhydrous sodium sulfate.
Present invention also offers above-mentioned flavouring agent preparation method be that this preparation method comprises the step that next coming in order carry out:
0.05 ~ 3 part of butyric acid, 0.2 ~ 0.8 part of butyl butyryl lactate, 0.1 ~ 0.5 part of ethyl lactate, 0.05 ~ 0.5 part of ethyl butyrate, 0.5 ~ 3 part of ethyl laurate, 0.8 ~ 2 part of nonyl lactone, 0.1 ~ 1 part of γ-decalactone, 0.2 ~ 3 part of δ-decalactone, 0.5 ~ 5 part of Ethyl vanillin, 0.5 ~ 5 part of dodecoic acid, 0.05 ~ 5 part of linalool are dropped in liquid aging tank successively, be uniformly mixed, stir 1 ~ 2 hour, obtain perfume mixture;
Start mixer, 20 ~ 30 parts of adsorbent silica are dropped into mixer, then is fed intake by above-mentioned perfume mixture, both mix 4 ~ 5 minutes; Finally 60 ~ 70 parts of carriers are dropped into mixer to mix in the lump, obtained described flavouring agent, above number is all weight portion.。
Present invention also offers a kind of feed or pet food, its flavouring agent adopting above-mentioned flavouring agent or said method to obtain.
Compared to prior art, flavouring agent of the present invention has the following advantages:
(1) flavouring agent of the present invention, toffee unique flavor, fragrance identification is high, signature, is difficult to personation, copies;
(2) toffee pure flavor, fragrance is joyful comfortable, and stimulating animal sense of smell, belongs to Favourite of animal, can improve phagostimulating effect;
(3) good with the compatibility of feed, lack in feed natural flavour mountaineous can be made up, and fragrance is stablized, sustained taste;
(4) carrier selected by the present invention can cover the bitter taste that feedstuff contains, and improves the palatability of feed, promotes searching for food of animal.
Detailed description of the invention
Further illustrate the present invention by embodiment below, but the present invention is not limited.The experimental technique of unreceipted actual conditions in embodiment below, usually conveniently condition, or according to the condition that manufacturer advises.Wherein, described percentage unless otherwise noted, is all weight percentage; Described number, is parts by weight.
Embodiment 1
(1) first by butyric acid 1 kilogram, butyl butyryl lactate 3 kilograms, ethyl lactate 2 kilograms, ethyl butyrate 1 kilogram, ethyl laurate 15 kilograms, nonyl lactone 10 kilograms, γ-decalactone 3 kilograms, δ-decalactone 5 kilograms, Ethyl vanillin 10 kilograms, dodecoic acid 10 kilograms, linalool 1 kilogram drops in liquid aging tank successively, be uniformly mixed, stir 1 hour; To be mixed complete after namely ageing complete, can be put into production after the assay was approved by production department;
(2) start mixer, the silica 200 kilograms weighed up is fed intake, enters mixer through screen cloth, the essence prepared is fed intake, after having fed intake, mix 5 minutes;
(3) 700 kilograms, carrier (anhydrous saccharin sodium) will be remained drop into mixer again and after mixing, shut down, weighing and bagging after sieving.
Embodiment 2
(1) first by butyric acid 2 kilograms, butyl butyryl lactate 4 kilograms, ethyl lactate 3 kilograms, ethyl butyrate 2 kilograms, ethyl laurate 18 kilograms, nonyl lactone 12 kilograms, γ-decalactone 5 kilograms, δ-decalactone 8 kilograms, Ethyl vanillin 15 kilograms, dodecoic acid 15 kilograms, linalool 3 kilograms drops in liquid aging tank, be uniformly mixed, stir 2 hours; To be mixed complete after namely ageing complete, can be put into production after the assay was approved by production department;
(2) start mixer, the silica 250 kilograms weighed up is fed intake, enters mixer through screen cloth, the essence prepared is fed intake, after having fed intake, mix 4 minutes;
(3) 700 kilograms, carrier (powdered whiting) will be remained drop into mixer again and after mixing, shut down; Weighing and bagging after sieving.
Embodiment 3
(1) first by butyric acid 2 kilograms, butyl butyryl lactate 5 kilograms, ethyl lactate 4 kilograms, ethyl butyrate 1 kilogram, ethyl laurate 25 kilograms, nonyl lactone 15 kilograms, γ-decalactone 8 kilograms, δ-decalactone 10 kilograms, Ethyl vanillin 10 kilograms, dodecoic acid 25 kilograms, linalool 5 kilograms drops in liquid aging tank, be uniformly mixed, stir 1.5 hours; To be mixed complete after namely ageing complete, can be put into production after the assay was approved by production department;
(2) start mixer, the silica 300 kilograms weighed up is fed intake, enters mixer through screen cloth, the essence prepared is fed intake, after having fed intake, mix 5 minutes;
(3) 600 kilograms, carrier (anhydrous sodium sulfate) will be remained drop into mixer again and after mixing, shut down; Weighing and bagging after sieving.
Beneficial effect of the present invention is further illustrated below by effect example.
Effect example 1
Flavouring agent fragrance and applicating evaluating: what embodiment 2 obtained is sample 1, with commercial diet flavouring agent A(sample 2) carry out fragrance comparative evaluation.Participating in assessment number is 10 people.
Table 1 finished product fragrance and applicating evaluating proof list
Table 2 flavouring agent sample aroma strength and Comfort Evaluation
Table 3 flavouring agent application verification is evaluated
In sum, no matter sample 1 is all better than sample 2 in aroma strength and comfort level.The perfuming intensity of sample 1, comfort level and fragrance remaining time are all better than sample 2.
Effect example 2
Zoopery effect assessment: by embodiment 1(experimental group) add in powdery perfect compound feed respectively with feedstuff flavouring agent A (control group), addition is 500g/t.Select the healthy DLY piglet of 25 age in days wean to carry out zoopery, experimental period is one week, investigates daily ingestion amount, daily gain and feed-weight ratio situation, and as shown in Table 4, experimental group can significantly improve the daily ingestion amount of piglet and improve the utilization rate of feed result.
Table 4. flavouring agent is on the impact of Production Performance of Weaning Pigs
| 25-32 age in days piglet | Control group (feedstuff flavouring agent A) | Experimental group |
| Daily ingestion amount/kg | 0.45±0.021 | 0.67±0.018 |
| Daily gain/kg | 0.32±0.041 | 0.36±0.010 |
| Feed-weight ratio | 2.14±0.05 | 1.86±0.01 |
From above effect, the index of the daily ingestion amount of experimental group, daily gain and feed-weight ratio is better than control group.And in aroma strength, fragrance comfort level and perfuming feed fragrance remaining time etc., all there is obvious advantage, be applied in feed and effectively can improve Production Performance of Weaning Pigs.
The flavouring agent that above-described embodiment can prepare by those skilled in the art is directly as feed or pet food additives, or the flavouring agent that conventional method can be adopted to be prepared by above-described embodiment is mixed with feed or pet food additives.Same, these additives, in the manufacture process of feed or pet food, add in product by those skilled in the art in a conventional manner.
Claims (4)
1. a flavouring agent, it is characterized in that, this flavouring agent is made up of following weight portion formula, it is 100 parts in the gross weight of flavouring agent, butyric acid 0.05 ~ 3 part, butyl butyryl lactate 0.2 ~ 0.8 part, ethyl lactate 0.1 ~ 0.5 part, ethyl butyrate 0.05 ~ 0.5 part, ethyl laurate 0.5 ~ 3 part, nonyl lactone 0.8 ~ 2 part, γ-decalactone 0.1 ~ 1 part, δ-decalactone 0.2 ~ 3 part, Ethyl vanillin 0.5 ~ 5 part, dodecoic acid 0.5 ~ 5 part, linalool 0.05 ~ 5 part, adsorbent silica 20 ~ 30 parts, 60 ~ 70 parts, carrier;
Described carrier be selected from anhydrous saccharin sodium, powdered whiting and anhydrous sodium sulfate any one.
2. a preparation method for flavouring agent, is characterized in that, this preparation method comprises the step that next coming in order carry out:
0.05 ~ 3 part of butyric acid, 0.2 ~ 0.8 part of butyl butyryl lactate, 0.1 ~ 0.5 part of ethyl lactate, 0.05 ~ 0.5 part of ethyl butyrate, 0.5 ~ 3 part of ethyl laurate, 0.8 ~ 2 part of nonyl lactone, 0.1 ~ 1 part of γ-decalactone, 0.2 ~ 3 part of δ-decalactone, 0.5 ~ 5 part of Ethyl vanillin, 0.5 ~ 5 part of dodecoic acid, 0.05 ~ 5 part of linalool are dropped in liquid aging tank successively, be uniformly mixed, stir 1 ~ 2 hour, obtain perfume mixture;
Start mixer, 20 ~ 30 parts of adsorbent silica are dropped into mixer, then is fed intake by above-mentioned perfume mixture, both mix 4 ~ 5 minutes; Finally 60 ~ 70 parts of carriers are dropped into mixer to mix in the lump, obtained described flavouring agent, above number is all weight portion.
3. preparation method as claimed in claim 2, is characterized in that, described carrier be selected from anhydrous saccharin sodium, powdered whiting and anhydrous sodium sulfate any one.
4. feed or a pet food, is characterized in that: with the addition of flavouring agent as claimed in claim 1 in this feed or pet food, or with the addition of the flavouring agent adopting the preparation method of Claims 2 or 3 to obtain.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310643076.1A CN103636944B (en) | 2013-12-03 | 2013-12-03 | Flavouring agent of a kind of toffee local flavor and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310643076.1A CN103636944B (en) | 2013-12-03 | 2013-12-03 | Flavouring agent of a kind of toffee local flavor and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103636944A CN103636944A (en) | 2014-03-19 |
| CN103636944B true CN103636944B (en) | 2016-03-23 |
Family
ID=50242352
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310643076.1A Active CN103636944B (en) | 2013-12-03 | 2013-12-03 | Flavouring agent of a kind of toffee local flavor and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103636944B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105595027A (en) * | 2016-01-27 | 2016-05-25 | 上海美农生物科技股份有限公司 | Preparing method for cream smell pig feed attractant |
| CN106561997A (en) * | 2016-11-15 | 2017-04-19 | 常熟市凯力达蜂窝包装材料有限公司 | Fragrance type feed additive |
| CN106578410A (en) * | 2016-11-15 | 2017-04-26 | 常熟市凯力达蜂窝包装材料有限公司 | Preparation method of flavor-type feed additive |
| CN113057254A (en) * | 2021-04-28 | 2021-07-02 | 味氏（广东）生物科技股份有限公司 | Preparation method and application of water-soluble sweet milk essence suitable for drinking water, porridge material and liquid feed of mammals |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101336699A (en) * | 2008-08-08 | 2009-01-07 | 四川省畜科饲料有限公司 | Super glucin formulation and use thereof |
| CN101411459A (en) * | 2008-11-17 | 2009-04-22 | 广州市名花香料有限公司 | Milk fat element |
| CN102987080A (en) * | 2011-09-15 | 2013-03-27 | 上海美农生物科技股份有限公司 | Feed fragrance agent having cream biscuit fragrance, and preparation method thereof |
| CN102987081A (en) * | 2011-09-15 | 2013-03-27 | 上海美农生物科技股份有限公司 | Feed fragrance agent with feeding attraction function, and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20020119233A1 (en) * | 2000-12-15 | 2002-08-29 | Huang An Shun | Cookies with improved shelf life and process for preparing them |
-
2013
- 2013-12-03 CN CN201310643076.1A patent/CN103636944B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101336699A (en) * | 2008-08-08 | 2009-01-07 | 四川省畜科饲料有限公司 | Super glucin formulation and use thereof |
| CN101411459A (en) * | 2008-11-17 | 2009-04-22 | 广州市名花香料有限公司 | Milk fat element |
| CN102987080A (en) * | 2011-09-15 | 2013-03-27 | 上海美农生物科技股份有限公司 | Feed fragrance agent having cream biscuit fragrance, and preparation method thereof |
| CN102987081A (en) * | 2011-09-15 | 2013-03-27 | 上海美农生物科技股份有限公司 | Feed fragrance agent with feeding attraction function, and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103636944A (en) | 2014-03-19 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101606545B (en) | Nutritional biscuit with high bone calcium and making method thereof | |
| CN103636944B (en) | Flavouring agent of a kind of toffee local flavor and preparation method thereof | |
| CN102132782A (en) | Micropterus salmoides compound feed and preparation method thereof | |
| CN106942464A (en) | A kind of phagostimulant and preparation method thereof | |
| EP2932857A1 (en) | Pet food | |
| CN104366144A (en) | Feed special for meat geese | |
| CN106954737A (en) | A kind of milk flavoured type feedstuff flavouring agent and preparation method thereof | |
| CN109907183A (en) | A kind of Ba Shayu juvenile fish anino acid feed and preparation method thereof | |
| CN101912065B (en) | Shoat feed and preparation method | |
| CN102987081B (en) | Feed fragrance agent with feeding attraction function, and preparation method thereof | |
| CN107647158A (en) | A kind of egg feedstuff for reducing Egg cholesterol amount and preparation method thereof | |
| CN105532578B (en) | A kind of beef ox fattening method and beef acid discharge method | |
| CN104543581A (en) | Formula of high-quality chicken feed for forest grazing | |
| CN106615947A (en) | Laying hen fodder containing carrots and preparation method thereof | |
| CN101756052A (en) | Nutrition feed of laying duck | |
| CN102630847A (en) | Piglet feed and preparation method and application thereof | |
| CN102987080B (en) | Feed fragrance agent having cream biscuit fragrance, and preparation method thereof | |
| CN104543488A (en) | Piglet feed and preparation method thereof | |
| CN110214864A (en) | A kind of Fruity type cattle feed flavouring agent and preparation method thereof | |
| CN101874558A (en) | Raw pig feed made of natural raw materials readily available in rural areas | |
| CN105285384A (en) | Milk flavored calf feed condiment containing sweetening agent as well as preparation method and application thereof | |
| CN105192328A (en) | Deep fermentation bioprotein feed for mutton sheep fattening | |
| CN105341391A (en) | Grass-scent lactating cow feed flavoring agent containing sweetening agent and preparation method and application thereof | |
| CN105475649A (en) | Sweetening agent-containing pig fattening feed flavoring agent with caramel fragrance, and preparation method and applications thereof | |
| CN109247446A (en) | A kind of feed for goat |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C53 | Correction of patent for invention or patent application | ||
| CB03 | Change of inventor or designer information |
Inventor after: Hu Zhuodong Inventor after: Tang Zhongyi Inventor after: Wei Wei Inventor before: Zong Jiajia Inventor before: Hu Zhuodong Inventor before: Tang Zhongyi |
|
| COR | Change of bibliographic data |
Free format text: CORRECT: INVENTOR; FROM: ZONG JIAJIA HU ZHUODONG TANG ZHONGYI TO: HU ZHUODONG TANG ZHONGYI WEI WEI |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20140319 Assignee: Chengdu Mei Yide Bioisystech Co., Ltd Assignor: Shanghai Menon Animal Nutrition Technology Co., Ltd. Contract record no.: 2017510000046 Denomination of invention: Toffee-flavored flavoring agent and preparation method thereof Granted publication date: 20160323 License type: Common License Record date: 20171208 |
|
| EE01 | Entry into force of recordation of patent licensing contract |