CN101336699A - Super glucin formulation and use thereof - Google Patents

Super glucin formulation and use thereof Download PDF

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Publication number
CN101336699A
CN101336699A CNA2008100457596A CN200810045759A CN101336699A CN 101336699 A CN101336699 A CN 101336699A CN A2008100457596 A CNA2008100457596 A CN A2008100457596A CN 200810045759 A CN200810045759 A CN 200810045759A CN 101336699 A CN101336699 A CN 101336699A
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Prior art keywords
glucin
ethyl
super glucin
super
acid
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CNA2008100457596A
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Chinese (zh)
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邝声耀
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SICHUAN ANIMTECH FEED CO Ltd
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SICHUAN ANIMTECH FEED CO Ltd
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Priority to CNA2008100457596A priority Critical patent/CN101336699A/en
Publication of CN101336699A publication Critical patent/CN101336699A/en
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Abstract

The invention discloses an ultra-sweet essence formulation, which comprises the following components, in mass percentages, edible level saccharin sodium 50-70%, starch 18-28%, ultra-sweet essence fragrant base 2-8% and white carbon black 10-15%. The ultra-sweet essence fragrant base comprises the following raw materials: vanillic aldehyde, ethyl vanillin, ethyl maltol, tonka bean camphor, coconut aldehyde, peach aldehyde, methyl cyclopentenolone, pineapple-ketone, butanedione, dodecanoic acid, butanoic acid, acetic acid, canoic acid, ethyl lactate, butyl butyryllactate, delta-decalactone, butyric ether, propylene glycol, cream flavour intensifier, musk xylene and silicon dioxide. The invention also discloses a use of ultra-sweet essence as animal feed flavoring. The ultra-sweet essence according to the invention contains multiple sweetening agents, flavoring agents and potentiating agents, and can eliminate bitterness and metallic taste of saccharin sodium when solely used and other bad side-effects, and is ultra-concentrated and ultra-sweet. And the product can be used as the animal feed flavoring capable of obviously improving feed intake of animal, thereby increasing growth rate of animal.

Description

Super glucin formulation and uses thereof
Technical field
The present invention relates to a kind of sweetener of high concentration, relate in particular to super glucin formulation of a kind of hyperconcetration that is used for flavor enhancement and uses thereof, belong to the production field of seasoning formulation sweetener.
Background technology
Sweetener (or claiming glucin) is widely used in the production of various food or medicine, as the production of products such as ice cream, carbonated drink, cola, soya-bean milk, preserved fruit, Western medicine dressing, its objective is sweet taste and the fragrance of strengthening food, makes it fragrant and sweet more good to eat, liked by the people.Common sweetener is mainly formed by the allotment of sweet taste concentrates such as sucrose, asccharin, honey element, alitame, Aspartame on the market now, its sweet taste can reach 50 of sucrose---and 60 times, but concentration is high not enough, during in particular for the flavor enhancement of the great animal feed of consumption, effect is not ideal enough.
At present, the flavor enhancement that is used for animal feed (especially piglet feed that is used for) more, it mainly is the monomer sweetener, as sucrose, Sucralose, asccharin, stevia, honey element, alitame, Aspartame etc., its sweet taste and fragrance all can not satisfy the sense of taste demand of animal (especially newborn animal) fully, so a lot of animals (especially newborn animal) are still arranged at present because of feed intake influences its speed of growth inadequately, serious meeting causes it to fall ill or death, has hindered the development of aquaculture virtually.
Summary of the invention
Purpose of the present invention is exactly super glucin formulation that provides in order to address the above problem a kind of hyperconcetration that is used for flavor enhancement and uses thereof.
The present invention is achieved through the following technical solutions above-mentioned purpose:
The raw material of the super glucin formulation among the present invention is: food grade saccharin sodium, starch, super glucin perfume base, white carbon black.
Saccharin sodium claims soluble saccharin again, is the sodium salt of asccharin, colourless crystallization or albescent slightly crystalline powder, and odorless or little fragrance arranged, the dense sweet band of distinguishing the flavor of is bitter, and sugariness is 500 times of sucrose.A little less than the heat-resisting and alkali resistance, acid condition heating sweet taste down dies down, and solution is greater than 0.026% bitter.The food grade saccharin sodium is widely used in products such as food, feed.
Starch is the high polymer of glucose, hydrolysis to the disaccharides stage be maltose, obtain glucose after the complete hydrolysis.Starch has amylose and amylopectin two classes.Amylose contains a hundreds of glucose unit, and amylopectin contains several thousand glucose units.In native starch straight chain account for 22%~26%, it is a solubility, remaining then is an amylopectin.
White carbon is well behaved reinforcing agent, filler, lubricant, has very high porous, water imbibition, good reinforcement is arranged and increase glutinous effect, good dispersiveness, suspension and thixotropy characteristic.
Above-mentioned raw materials is added the extremely dense super glucin perfume base of fragrant degree, gets product after evenly mixing.
As the optimization formula of super glucin among the present invention, the mass percent of above-mentioned each raw material is: food grade saccharin sodium 50---70%, starch 18---28%, super glucin perfume base 2---8%, white carbon black 10---15%; Its best in quality percentage is: food grade saccharin sodium 60%, starch 22.5%, super glucin perfume base 5%, white carbon black 12.5%.For guaranteeing the high concentration of product, the purity of described food grade saccharin sodium is not less than 99%.
As the super glucin perfume base of one of the raw material of super glucin formulation among the present invention, it is made up of following raw material: vanillic aldehyde, Ethyl vanillin, ethyl maltol, cumarin, arbricolin, peach aldehyde, methyl cyclopentenyl ketone, pineapple ketone, diacetyl, dodecoic acid, butyric acid, acetate, certain herbaceous plants with big flowers acid, ethyl lactate, two butyl ester, fourth position certain herbaceous plants with big flowers lactone, ethyl butyrate, propane diols, cream fumet, musk xylene, silica.
Above-mentioned each raw material has been gathered various fragrance, makes the super glucin perfume base that finally makes have various fragrance, can adapt to the sense of taste demand of different animals.
The preferred mass percentage of each raw material of above-mentioned super glucin perfume base is: vanillic aldehyde 12---18%, Ethyl vanillin 12---18%, ethyl maltol 2---4%, cumarin 3---5%, arbricolin 5---7%, peach aldehyde 1---3%, methyl cyclopentenyl ketone 0.2---0.8%, pineapple ketone 1---2%, diacetyl 5---8%, dodecoic acid 2---3%, butyric acid 3---6%, acetate 0.8---1.2%, certain herbaceous plants with big flowers acid 0.8---1.2%, ethyl lactate 5---9%, two butyl esters 3---5%, fourth position certain herbaceous plants with big flowers lactone 0.8---1.2%, ethyl butyrate 3---5%, propane diols 10---18%, cream fumet 1---3%, musk xylene 0.2---0.8%, silica 4---6%; Its best in quality percentage is: vanillic aldehyde 15%, Ethyl vanillin 15%, ethyl maltol 3%, cumarin 4%, arbricolin 6%, peach aldehyde 2%, methyl cyclopentenyl ketone 0.5%, pineapple ketone 1.5%, diacetyl 6.5%, dodecoic acid 2.5%, butyric acid 4.5%, acetate 1%, certain herbaceous plants with big flowers acid 1%, ethyl lactate 7%, two butyl ester 4%, fourth position certain herbaceous plants with big flowers lactone 1%, ethyl butyrate 4%, propane diols 14%, cream fumet 2%, musk xylene 0.5%, silica 5%.
The purposes of super glucin among the present invention, it is used for the animal feed flavor enhancement.Its optimum amount is: one ton of animal feed adds super glucin 80 grams.
Beneficial effect of the present invention is:
Super glucin with the super glucin formulation production among the present invention has concentrated multiple sweetener, flavouring agent and synergist, adverse side effects such as the bitter taste of independent use saccharin sodium and metallic taste have been eliminated, super dense, super sweet, be used for the animal feed flavor enhancement and can obviously improve the feed intake of animal, thereby improved the speed of growth of animal; Especially at newborn animal, guaranteed their feed intake effectively with the super glucin of the super glucin formulation production among the present invention, even under sick situation, also can allow animal take food as much as possible, promoted the fast development of aquaculture, accelerated the circulation rate of meat product, helped whole human beings'health demand indirectly, thus promote entire society better, development quickly.
The specific embodiment
Below in conjunction with specific embodiment the present invention is further described in detail:
Embodiment 1:
(1) at first takes by weighing following raw material: vanillic aldehyde 15 grams, Ethyl vanillin 15 grams, ethyl maltol 3 grams, cumarin 4 grams, arbricolin 6 grams, peach aldehyde 2 grams, methyl cyclopentenyl ketone 0.5 gram, pineapple ketone 1.5 grams, diacetyl 6.5 grams, dodecoic acid 2.5 grams, butyric acid 4.5 grams, acetate 1 gram, certain herbaceous plants with big flowers acid 1 gram, ethyl lactate 7 grams, two butyl ester 4 grams, fourth position certain herbaceous plants with big flowers lactone 1 gram, ethyl butyrate 4 grams, propane diols 14 grams, cream fumet 2 grams, musk xylene 0.5 gram, silica 5 grams.
(2) then above-mentioned each raw material is added in the agitator, mix, make super glucin perfume base and amount to 100 grams.
(3) take by weighing following raw material again: purity is not less than 99% food grade saccharin sodium 60 grams, starch 22.5 grams, white carbon black 12.5 grams.
(4) then each raw material in above-mentioned (3) step is added in the agitator, add super glucin perfume base 5 grams that make in above-mentioned (2) step again, mix, make super glucin and amount to 100 grams.
(5) at last 80 grams in the super glucin that makes in above-mentioned (4) step are added in 1 ton of feed, mix, obtain amounting to 1000.08 kilograms seasoning feed.
The seasoning feed that makes in above-mentioned (5) step is used for a month big sucking pig feeds, its appetite reaches 1 kilogram/meal soon, and constantly increase, at last to 8 kilograms/meal, fed 1000.08 kilograms seasoning feed, shared 95 days of front and back, sucking pig becomes 110 kilograms from 12 kilograms, and its speed of growth is about 1.5 times of former forage feed, and the speed of delivering for sale is obviously accelerated, whole cost does not increase, and raiser's synergy income is obvious.
Embodiment 2:
(1) at first takes by weighing following raw material: vanillic aldehyde 12 grams, Ethyl vanillin 12 grams, ethyl maltol 2 grams, cumarin 3 grams, arbricolin 7 grams, peach aldehyde 3 grams, methyl cyclopentenyl ketone 0.8 gram, pineapple ketone 2 grams, diacetyl 8 grams, dodecoic acid 3 grams, butyric acid 6 grams, acetate 1.2 grams, certain herbaceous plants with big flowers acid 1.2 grams, ethyl lactate 9 grams, two butyl ester 5 grams, fourth position certain herbaceous plants with big flowers lactone 1.2 grams, ethyl butyrate 5 grams, propane diols 11 grams, cream fumet 1 gram, musk xylene 0.6 gram, silica 6 grams.
(2) then above-mentioned each raw material is added in the agitator, mix, make super glucin perfume base and amount to 100 grams.
(3) take by weighing following raw material again: purity is not less than 99% food grade saccharin sodium 70 grams, starch 18 grams, white carbon black 10 grams.
(4) then each raw material in above-mentioned (3) step is added in the agitator, add super glucin perfume base 2 grams that make in above-mentioned (2) step again, mix, make super glucin and amount to 100 grams.
(5) at last 80 grams in the super glucin that makes in above-mentioned (4) step are added in 1 ton of feed, mix, obtain amounting to 1000.08 kilograms seasoning feed.
The seasoning feed that makes in above-mentioned (5) step is used for three months big healthy growth pigs feeds, because super glucin perfume base reduces, fragrance slightly descends, but its cost also decreases, and compares embodiment 1, and the food-intake of growth pig slightly descends but be not obvious, its speed of growth is not add about 1.4 times of super glucin forage feed, the speed of delivering for sale is compared that embodiment 1 slightly descends but still is very fast, and whole cost descends to some extent, and raiser's synergy income is obvious.
Embodiment 3:
(1) at first takes by weighing following raw material: vanillic aldehyde 18 grams, Ethyl vanillin 18 grams, ethyl maltol 4 grams, cumarin 5 grams, arbricolin 5 grams, peach aldehyde 1 gram, methyl cyclopentenyl ketone 0.2 gram, pineapple ketone 1 gram, diacetyl 5 grams, dodecoic acid 2 grams, butyric acid 3 grams, acetate 0.8 gram, certain herbaceous plants with big flowers acid 0.8 gram, ethyl lactate 5 grams, two butyl ester 3 grams, fourth position certain herbaceous plants with big flowers lactone 0.8 gram, ethyl butyrate 3 grams, propane diols 16 grams, cream fumet 3 grams, musk xylene 0.8 gram, silica 4.6 grams.
(2) then above-mentioned each raw material is added in the agitator, mix, make super glucin perfume base and amount to 100 grams.
(3) take by weighing following raw material again: purity is not less than 99% food grade saccharin sodium 50 grams, starch 28 grams, white carbon black 14 grams.
(4) then each raw material in above-mentioned (3) step is added in the agitator, add super glucin perfume base 8 grams that make in above-mentioned (2) step again, mix, make super glucin and amount to 100 grams.
(5) at last 80 grams in the super glucin that makes in above-mentioned (4) step are added in 1 ton of feed, mix, obtain amounting to 1000.08 kilograms seasoning feed.
The seasoning feed that makes in above-mentioned (5) step is used for two months big dispirited type growth pigs feeds, because super glucin perfume base increases, fragrance is denseer, but embodiment 1 is compared in the also rising to some extent of its cost, the food-intake of growth pig further improves, its speed of growth is not add about 1.6 times of super glucin forage feed, and the speed of delivering for sale is further accelerated, though whole cost rises to some extent, but the cycle of delivering for sale shortens, and raiser's synergy income is obvious.

Claims (9)

1, a kind of super glucin formulation is characterized in that: its formula material is: food grade saccharin sodium, starch, super glucin perfume base, white carbon black.
2, super glucin formulation according to claim 1 is characterized in that: the mass percent of each raw material is: food grade saccharin sodium 50---70%, starch 18---28%, super glucin perfume base 2---8%, white carbon black 10---15%.
3, super glucin formulation according to claim 2 is characterized in that: the mass percent of each raw material is: food grade saccharin sodium 60%, starch 22.5%, super glucin perfume base 5%, white carbon black 12.5%.
4, according to claim 1 or 2 or 3 described super glucin formulations, it is characterized in that: the purity of described food grade saccharin sodium is not less than 99%.
5, according to claim 1 or 2 or 3 described super glucin formulations, it is characterized in that: described super glucin perfume base is made up of following raw material: vanillic aldehyde, Ethyl vanillin, ethyl maltol, cumarin, arbricolin, peach aldehyde, methyl cyclopentenyl ketone, pineapple ketone, diacetyl, dodecoic acid, butyric acid, acetate, certain herbaceous plants with big flowers acid, ethyl lactate, two butyl ester, fourth position certain herbaceous plants with big flowers lactone, ethyl butyrate, propane diols, cream fumet, musk xylene, silica.
6, super glucin formulation according to claim 5 is characterized in that: the mass percent of each raw material of described super glucin perfume base is: vanillic aldehyde 12---18%, Ethyl vanillin 12---18%, ethyl maltol 2---4%, cumarin 3---5%, arbricolin 5---7%, peach aldehyde 1---3%, methyl cyclopentenyl ketone 0.2---0.8%, pineapple ketone 1---2%, diacetyl 5---8%, dodecoic acid 2---3%, butyric acid 3---6%, acetate 0.8---1.2%, certain herbaceous plants with big flowers acid 0.8---1.2%, ethyl lactate 5---9%, two butyl esters 3---5%, fourth position certain herbaceous plants with big flowers lactone 0.8---1.2%, ethyl butyrate 3---5%, propane diols 10---18%, cream fumet 1---3%, musk xylene 0.2---0.8%, silica 4---6%.
7, super glucin formulation according to claim 6 is characterized in that: the mass percent of each raw material of described super glucin perfume base is: vanillic aldehyde 15%, Ethyl vanillin 15%, ethyl maltol 3%, cumarin 4%, arbricolin 6%, peach aldehyde 2%, methyl cyclopentenyl ketone 0.5%, pineapple ketone 1.5%, diacetyl 6.5%, dodecoic acid 2.5%, butyric acid 4.5%, acetate 1%, certain herbaceous plants with big flowers acid 1%, ethyl lactate 7%, two butyl esters 4%, fourth position certain herbaceous plants with big flowers lactone 1%, ethyl butyrate 4%, propane diols 14%, cream fumet 2%, musk xylene 0.5%, silica 5%.
8, a kind of purposes of super glucin as claimed in claim 1 is characterized in that: it is used for the animal feed flavor enhancement.
9, the purposes of super glucin according to claim 8 is characterized in that: its its be used for the animal feed flavor enhancement consumption be: one ton of animal feed adds super glucin 80 and restrains.
CNA2008100457596A 2008-08-08 2008-08-08 Super glucin formulation and use thereof Pending CN101336699A (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102669623A (en) * 2012-05-02 2012-09-19 郑书旺 Bitter screening agent and debitterizing stevia sugar
CN102987083A (en) * 2011-09-15 2013-03-27 上海美农生物科技股份有限公司 Feed fragrance agent having pig breast milk flavor, and preparation method thereof
CN102987080A (en) * 2011-09-15 2013-03-27 上海美农生物科技股份有限公司 Feed fragrance agent having cream biscuit fragrance, and preparation method thereof
CN102987084A (en) * 2011-09-15 2013-03-27 上海美农生物科技股份有限公司 Feed fragrance agent used in premix, and preparation method thereof
CN102987081A (en) * 2011-09-15 2013-03-27 上海美农生物科技股份有限公司 Feed fragrance agent with feeding attraction function, and preparation method thereof
CN103636944A (en) * 2013-12-03 2014-03-19 上海美农生物科技股份有限公司 Toffee-flavored flavoring agent and preparation method thereof
CN105309912A (en) * 2014-12-31 2016-02-10 许静 Preparation method of cane sugar powder essence special for betel nuts and cane sugar base special for cane sugar powder essence

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
A.MAEKAWA等: "LONG-TERM TOXICITY/CARCINOGENICITY OF MUSK XYLOL IN B6C3F1 MICE", 《FOOD AND CHEMICAL TOXICOLOGY》 *

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102987083A (en) * 2011-09-15 2013-03-27 上海美农生物科技股份有限公司 Feed fragrance agent having pig breast milk flavor, and preparation method thereof
CN102987080A (en) * 2011-09-15 2013-03-27 上海美农生物科技股份有限公司 Feed fragrance agent having cream biscuit fragrance, and preparation method thereof
CN102987084A (en) * 2011-09-15 2013-03-27 上海美农生物科技股份有限公司 Feed fragrance agent used in premix, and preparation method thereof
CN102987081A (en) * 2011-09-15 2013-03-27 上海美农生物科技股份有限公司 Feed fragrance agent with feeding attraction function, and preparation method thereof
CN102987083B (en) * 2011-09-15 2014-10-29 上海美农生物科技股份有限公司 Feed fragrance agent having pig breast milk flavor, and preparation method thereof
CN102987081B (en) * 2011-09-15 2014-11-19 上海美农生物科技股份有限公司 Feed fragrance agent with feeding attraction function, and preparation method thereof
CN102669623A (en) * 2012-05-02 2012-09-19 郑书旺 Bitter screening agent and debitterizing stevia sugar
CN103636944A (en) * 2013-12-03 2014-03-19 上海美农生物科技股份有限公司 Toffee-flavored flavoring agent and preparation method thereof
CN103636944B (en) * 2013-12-03 2016-03-23 上海美农生物科技股份有限公司 Flavouring agent of a kind of toffee local flavor and preparation method thereof
CN105309912A (en) * 2014-12-31 2016-02-10 许静 Preparation method of cane sugar powder essence special for betel nuts and cane sugar base special for cane sugar powder essence
CN105309912B (en) * 2014-12-31 2017-11-24 许静 A kind of preparation method of special sucrose powdered flavor of betel nut and its special sucrose perfume base

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Application publication date: 20090107