CN102987084A - Feed fragrance agent used in premix, and preparation method thereof - Google Patents
Feed fragrance agent used in premix, and preparation method thereof Download PDFInfo
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- CN102987084A CN102987084A CN2011102740011A CN201110274001A CN102987084A CN 102987084 A CN102987084 A CN 102987084A CN 2011102740011 A CN2011102740011 A CN 2011102740011A CN 201110274001 A CN201110274001 A CN 201110274001A CN 102987084 A CN102987084 A CN 102987084A
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Abstract
The present invention relates to a feed fragrance agent used in a premix, and a preparation method thereof. The feed fragrance agent comprises the following components, by weight, 4-20 parts of gamma-nonanolactone, 3-25 parts of ethyl vanillin, 0.3-2 parts of pentadecanolide, 1-8 parts of ethyl maltol, 1-10 parts of dihydrocoumarin, 4-20 parts of benzyl alcohol, 4-20 parts of ethyl lactate, and 5-20 parts of ethyl butyrate. The preparation method comprises: sequentially pouring perfumes to a liquid aging tank according to a solid-liquid sequence, carrying out stirring mixing to prepare a flavor, carrying out sealed placing aging, absorbing the flavor by using partial carrier, mixing in a mixer, pouring the remaining carrier to the mixer to mix, discharging the material after completing the mixing, and screening through a vibration sieve to obtain the product. Compared with the feed fragrance agent in the prior art, the feed fragrance agent of the present invention has advantages of pure fragrance, strong concentration, long fragrance lasting time, strong fragrance penetration, and the like.
Description
Technical field
The present invention relates to feed additive field, especially relate to a kind of feedstuff flavouring agent for premix and preparation method thereof.
Background technology
At present owing to the primary raw material that uses in the premix is: constant mineral matter and trace quantity mineral substance element, vitamin, single amino acid, medicine, antioxidant and mould inhibitor etc., because the interpolation of above raw material, cause premix to have bad smell and mouthfeel, therefore premix need to be covered bad smell with flavouring agent, improve the feed intake of pig, also satisfy buyer's needs.Also need cover bad mouthfeel simultaneously, thereby decrease premix is on the impact of complete feed palatability.There are the following problems but after present conventional flavouring agent uses in premix:
1, fragrance is pure not, or even pungent peculiar smell;
2, fragrance remaining time is not long, one month less than time premix smell covered the smell of flavouring agent, or even the part material in the flavouring agent and premix stock yard produce chemical reaction, causes the change of smell, affects the result of use of premix;
3, too emphasize the fragrance concentration of flavouring agent, ignored the essence of fragrance as phagostimulant, cause flavouring agent to become feed perfume fully, feed food calling poor effect;
4, conventional frankincense type product since penetration power a little less than, need higher addition just can satisfy the demand, use cost increases;
5, conventional fruital product because shelf-life and the service time of premix are longer, affects the anaphase effect of premix because volatility is stronger.
In view of above problem, need a kind of flavouring agent product of specialized designs for premix, it must possess stronger masking ability, longer fragrance remaining time, purer fragrance just can be met the need of market.
The present invention is directed to the characteristics of premix, by constantly groping, design to be fit to the special-purpose milk flavouring agent prescription that premix is used, the above drawback that in premix, exists to solve the conventional feed flavouring agent.
Summary of the invention
Purpose of the present invention be exactly provide in order to overcome the defective that above-mentioned prior art exists a kind of natural, fragrance is pure, the feedstuff flavouring agent that is used for premix of high concentration and preparation method thereof.
Purpose of the present invention can be achieved through the following technical solutions:
A kind of feedstuff flavouring agent for premix is characterized in that: this feedstuff flavouring agent comprises following component and weight portion content:
Nonyl lactone 4～20, Ethyl vanillin 3～25, omega-pentadecanolide 0.3～2, ethyl maltol 1～8, dihydrocoumarin 1～10, phenmethylol 4～20, ethyl lactate 4～20, ethyl butyrate 5～20, carrier 100～800;
The preferred following component of described feedstuff flavouring agent and weight portion content:
Nonyl lactone 5～19, Ethyl vanillin 5～24, omega-pentadecanolide 0.5～3, ethyl maltol 1～6, dihydrocoumarin 1～10, phenmethylol 4～20, ethyl lactate 4～20, ethyl butyrate 5～15, carrier 100～800;
Described carrier is selected from one or more in silica, stone flour or the rice bran.
A kind of preparation method of the feedstuff flavouring agent for premix is characterized in that, the method may further comprise the steps:
(1) get the raw materials ready according to following component and weight portion content:
Nonyl lactone 4～20, Ethyl vanillin 3～25, omega-pentadecanolide 0.3～2, ethyl maltol 1～8, dihydrocoumarin 1～10, phenmethylol 4～20, ethyl lactate 4～20, ethyl butyrate 5～20, carrier 100～800;
(2) by the prescription requirement, liquid behind the first solid drops into above-mentioned raw material except carrier in the liquid aging tank successively, mixes, and mixing time is controlled at 1.5～2.5 hours;
(3) after to be mixed the finishing, with the airtight placement ageing of the essence that makes more than 12 hours;
(4) by the amount of prescription requirement, with the carrier of 20-30wt% essence is adsorbed, in mixer, mixed 2～6 minutes;
(5) then remaining carrier is dropped into mixer again, mixed 1～5 minute, finish mix after blowing and sieve through vibratory sieve and namely to obtain product.
Compared with prior art, the present invention has the following advantages:
(1) purer fragrance-natural (natural equivalent) raw material possesses purer fragrance;
(2) the flavouring agent concentrate of stronger concentration-high concentration;
(3) the special-purpose flavouring agent that designs for premix specially;
(4) fragrance remaining time is long, and the ability of covering smell is strong, can better act on premix;
(5) this flavouring agent fragrance penetration power is strong, adds cost low, and cost performance is high;
(6) better food calling-natural (natural equivalent) raw material and optimization of C/C composites.
The specific embodiment
The present invention is described in detail below in conjunction with specific embodiment.
Embodiment 1
A kind of preparation method of the feedstuff flavouring agent for premix, the method may further comprise the steps:
(1) gets the raw materials ready according to following component and content: nonyl lactone 8kg, Ethyl vanillin 4kg, omega-pentadecanolide 0.5kg, ethyl maltol 3kg, dihydrocoumarin 2kg, phenmethylol 10kg, ethyl lactate 6kg, ethyl butyrate 8kg;
(2) order according to liquid behind the first solid drops into above-mentioned raw material except carrier in the liquid aging tank, mixes, and stirs 1.6 hours;
(3) after to be mixed the finishing, with the airtight placement ageing of the essence that makes more than 12 hours;
(4) by the prescription requirement, with the silica supports of 40kg essence is adsorbed, mixing is 2 minutes in mixer;
(5) then remaining 120kg silica supports is dropped into mixer, mixed 2 minutes, finish mixing;
(6) blowing and through the vibratory sieve weighing and bagging that sieves namely gets product.
Embodiment 2
A kind of preparation method of the feedstuff flavouring agent for premix, the method may further comprise the steps:
(1) gets the raw materials ready according to following component and content: nonyl lactone 10kg, Ethyl vanillin 5kg, omega-pentadecanolide 0.7kg, ethyl maltol 4kg, dihydrocoumarin 3kg, phenmethylol 10kg, ethyl lactate 7kg, ethyl butyrate 8kg;
(2) order according to liquid behind the first solid drops into above-mentioned raw material except carrier in the liquid aging tank, mixes, and stirs 2 hours;
(3) after to be mixed the finishing, with the airtight placement ageing of the essence that makes more than 12 hours;
(4) by the prescription requirement, with the silica supports of 50kg essence is adsorbed, mixing is 2.5 minutes in mixer;
(5) then remaining 150kg silica supports is dropped into mixer, mixed 2.5 minutes, finish mixing;
(6) blowing and through the vibratory sieve weighing and bagging that sieves namely gets product.
Embodiment 3
A kind of preparation method of the feedstuff flavouring agent for premix, the method may further comprise the steps:
(1) gets the raw materials ready according to following component and content: nonyl lactone 10kg, Ethyl vanillin 7kg, omega-pentadecanolide 2kg, ethyl maltol 8kg, dihydrocoumarin 5kg, phenmethylol 10kg, ethyl lactate 10kg, ethyl butyrate 8kg;
(2) order according to liquid behind the first solid drops into above-mentioned raw material except carrier in the liquid aging tank, mixes, and stirs 2.5 hours;
(3) after to be mixed the finishing, with the airtight placement ageing of the essence that makes more than 12 hours;
(4) by the prescription requirement, with the silica supports of 75kg essence is adsorbed, mixing is 3 minutes in mixer;
(5) then remaining 175kg silica supports is dropped into mixer again, mixed 3 minutes, finish mixing;
(6) blowing and through the vibratory sieve weighing and bagging that sieves namely gets product.
Embodiment 4
A kind of preparation method of the feedstuff flavouring agent for premix, the method may further comprise the steps:
(1) gets the raw materials ready according to following component and content: nonyl lactone 4kg, Ethyl vanillin 3kg, omega-pentadecanolide 0.3kg, ethyl maltol 1kg, dihydrocoumarin 1kg, phenmethylol 4kg, ethyl lactate 4kg, ethyl butyrate 5kg;
(2) order according to liquid behind the first solid drops into above-mentioned raw material except carrier in the liquid aging tank, mixes, and stirs 1.5 hours;
(3) after to be mixed the finishing, with the airtight placement ageing of the essence that makes more than 12 hours;
(4) by the prescription requirement, with the silica supports of 20kg essence is adsorbed, mixing is 2 minutes in mixer;
(5) then remaining 80kg carrier is dropped into mixer again, mixed 2 minutes, finish mixing;
(6) blowing and through the vibratory sieve weighing and bagging that sieves namely gets product.
Embodiment 5
A kind of preparation method of the feedstuff flavouring agent for premix, the method may further comprise the steps:
(1) gets the raw materials ready according to following component and content: nonyl lactone 20kg, Ethyl vanillin 25kg, omega-pentadecanolide 2kg, ethyl maltol 8kg, dihydrocoumarin 10kg, phenmethylol 20kg, ethyl lactate 20kg, ethyl butyrate 20kg;
(2) order according to liquid behind the first solid drops into above-mentioned raw material except carrier in the liquid aging tank, mixes, and stirs 2.5 hours;
(3) after to be mixed the finishing, with the airtight placement ageing of the essence that makes more than 12 hours;
(4) by the prescription requirement, with the silica supports of 200kg essence is adsorbed, mixing is 6 minutes in mixer;
(5) then remaining 600kg carrier is dropped into mixer again, mixed 5 minutes, finish mixing;
(6) blowing and through the vibratory sieve weighing and bagging that sieves namely gets product.
Claims (4)
1. a feedstuff flavouring agent that is used for premix is characterized in that, this feedstuff flavouring agent comprises following component and weight portion content:
Nonyl lactone 4～20, Ethyl vanillin 3～25, omega-pentadecanolide 0.3～2, ethyl maltol 1～8, dihydrocoumarin 1～10, phenmethylol 4～20, ethyl lactate 4～20, ethyl butyrate 5～20, carrier 100～800.
2. a kind of feedstuff flavouring agent for premix according to claim 1 is characterized in that, the preferred following component of described feedstuff flavouring agent and weight portion content:
Nonyl lactone 5～19, Ethyl vanillin 5～24, omega-pentadecanolide 0.5～3, ethyl maltol 1～6, dihydrocoumarin 1～10, phenmethylol 4～20, ethyl lactate 4～20, ethyl butyrate 5～15, carrier 100～800.
3. a kind of feedstuff flavouring agent for premix according to claim 1 and 2 is characterized in that, described carrier is selected from one or more in silica, stone flour or the rice bran.
4. the preparation method of the feedstuff flavouring agent for premix as claimed in claim 1 is characterized in that, the method may further comprise the steps:
(1) get the raw materials ready according to following component and weight portion content:
Nonyl lactone 4～20, Ethyl vanillin 3～25, omega-pentadecanolide 0.3～2, ethyl maltol 1～8, dihydrocoumarin 1～10, phenmethylol 4～20, ethyl lactate 4～20, ethyl butyrate 5～20, carrier 100～800:
(2) by the prescription requirement, liquid behind the first solid drops into above-mentioned raw material except carrier in the liquid aging tank successively, mixes, and mixing time is controlled at 1.5～2.5 hours;
(3) after to be mixed the finishing, with the airtight placement ageing of the mixture that makes more than 12 hours;
(4) by the prescription requirement, with 20～30wt% carrier essence is adsorbed, in mixer, mixed 2～6 minutes;
(5) then remaining carrier is dropped into mixer again, mixed 1～5 minute, finish mix after blowing and sieve through vibratory sieve and namely to obtain product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110274001.1A CN102987084B (en) | 2011-09-15 | 2011-09-15 | Feed fragrance agent used in premix, and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110274001.1A CN102987084B (en) | 2011-09-15 | 2011-09-15 | Feed fragrance agent used in premix, and preparation method thereof |
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| CN102987084A true CN102987084A (en) | 2013-03-27 |
| CN102987084B CN102987084B (en) | 2014-08-20 |
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| CN201110274001.1A Active CN102987084B (en) | 2011-09-15 | 2011-09-15 | Feed fragrance agent used in premix, and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105746905A (en) * | 2016-03-01 | 2016-07-13 | 湖南晶天科技实业有限公司 | Feed additive and preparation method thereof |
| CN108713645A (en) * | 2018-05-15 | 2018-10-30 | 成都大帝汉克生物科技有限公司 | A kind of special fatty acid product improving beef cattle growth performance |
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| CN101336699A (en) * | 2008-08-08 | 2009-01-07 | 四川省畜科饲料有限公司 | Super glucin formulation and use thereof |
| CN101965964A (en) * | 2010-09-25 | 2011-02-09 | 上海美农饲料有限公司 | Method for preparing milk flavor essence, prepared milk flavor essence thereof and related feed flavoring agent |
| WO2011104208A1 (en) * | 2010-02-24 | 2011-09-01 | Rhodia Operations | Method for preparing a composition including a compound containing vanillin and ethylvanillin, composition thus obtained and use thereof |
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2011
- 2011-09-15 CN CN201110274001.1A patent/CN102987084B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101336699A (en) * | 2008-08-08 | 2009-01-07 | 四川省畜科饲料有限公司 | Super glucin formulation and use thereof |
| WO2011104208A1 (en) * | 2010-02-24 | 2011-09-01 | Rhodia Operations | Method for preparing a composition including a compound containing vanillin and ethylvanillin, composition thus obtained and use thereof |
| CN101965964A (en) * | 2010-09-25 | 2011-02-09 | 上海美农饲料有限公司 | Method for preparing milk flavor essence, prepared milk flavor essence thereof and related feed flavoring agent |
Non-Patent Citations (1)
| Title |
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| 汪海峰，等: "饲用奶香和焦糖香味剂主要致香成分的分析", 《饲料研究》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105746905A (en) * | 2016-03-01 | 2016-07-13 | 湖南晶天科技实业有限公司 | Feed additive and preparation method thereof |
| CN108713645A (en) * | 2018-05-15 | 2018-10-30 | 成都大帝汉克生物科技有限公司 | A kind of special fatty acid product improving beef cattle growth performance |
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| Publication number | Publication date |
|---|---|
| CN102987084B (en) | 2014-08-20 |
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Application publication date: 20130327 Assignee: Chengdu Mei Yide Bioisystech Co., Ltd Assignor: Shanghai Menon Animal Nutrition Technology Co., Ltd. Contract record no.: 2017510000046 Denomination of invention: Feed fragrance agent used in premix, and preparation method thereof Granted publication date: 20140820 License type: Common License Record date: 20171208 |