CN102987084B - Feed fragrance agent used in premix, and preparation method thereof - Google Patents
Feed fragrance agent used in premix, and preparation method thereof Download PDFInfo
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- CN102987084B CN102987084B CN201110274001.1A CN201110274001A CN102987084B CN 102987084 B CN102987084 B CN 102987084B CN 201110274001 A CN201110274001 A CN 201110274001A CN 102987084 B CN102987084 B CN 102987084B
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Abstract
The present invention relates to a feed fragrance agent used in a premix, and a preparation method thereof. The feed fragrance agent comprises the following components, by weight, 4-20 parts of gamma-nonanolactone, 3-25 parts of ethyl vanillin, 0.3-2 parts of pentadecanolide, 1-8 parts of ethyl maltol, 1-10 parts of dihydrocoumarin, 4-20 parts of benzyl alcohol, 4-20 parts of ethyl lactate, and 5-20 parts of ethyl butyrate. The preparation method comprises: sequentially pouring perfumes to a liquid aging tank according to a solid-liquid sequence, carrying out stirring mixing to prepare a flavor, carrying out sealed placing aging, absorbing the flavor by using partial carrier, mixing in a mixer, pouring the remaining carrier to the mixer to mix, discharging the material after completing the mixing, and screening through a vibration sieve to obtain the product. Compared with the feed fragrance agent in the prior art, the feed fragrance agent of the present invention has advantages of pure fragrance, strong concentration, long fragrance lasting time, strong fragrance penetration, and the like.
Description
Technical field
The present invention relates to feed additive field, especially relate to a kind of feedstuff flavouring agent for premix and preparation method thereof.
Background technology
At present because the primary raw material using in premix is: constant mineral matter and trace quantity mineral substance element, vitamin, single amino acid, medicine, antioxidant and mould inhibitor etc., due to the interpolation of above raw material, cause premix to have bad smell and mouthfeel, therefore premix need to be covered bad smell with flavouring agent, improve the feed intake of pig, also meet buyer's needs.Also need to cover bad mouthfeel simultaneously, thereby significantly reduce the impact of premix on complete feed palatability.But after current conventional flavouring agent uses in premix, there are the following problems:
1, fragrance is pure not, or even pungent peculiar smell;
2, fragrance remaining time is not long, one month less than time premix smell covered the smell of flavouring agent, or even part material and premix stock yard in flavouring agent produce chemical reaction, causes the change of smell, affects the result of use of premix;
3, too emphasize the fragrance concentration of flavouring agent, ignored the essence of fragrance as phagostimulant, cause flavouring agent to become feed perfume completely, feed food calling poor effect;
4, conventional frankincense type product due to penetration power a little less than, need higher addition just can satisfy the demand, use cost increase;
5, conventional fruital product, because volatility is stronger, because shelf-life and the service time of premix are longer, affects the anaphase effect of premix.
In view of above problem, need a kind of flavouring agent product of specialized designs for premix, it must possess stronger masking ability, longer fragrance remaining time, purer fragrance just can be met the need of market.
The present invention is directed to the feature of premix, by constantly groping, design and be applicable to the special milk flavouring agent formula that premix is used, the above drawback existing to solve conventional feed flavouring agent in premix.
Summary of the invention
Object of the present invention be exactly provide in order to overcome the defect that above-mentioned prior art exists a kind of natural, fragrance is pure, the feedstuff flavouring agent for premix of high concentration and preparation method thereof.
Object of the present invention can be achieved through the following technical solutions:
For a feedstuff flavouring agent for premix, it is characterized in that: this feedstuff flavouring agent comprises following component and weight portion content:
Nonyl lactone 4～20, Ethyl vanillin 3～25, omega-pentadecanolide 0.3～2, ethyl maltol 1～8, dihydrocoumarin 1～10, phenmethylol 4～20, ethyl lactate 4～20, ethyl butyrate 5～20, carrier 100～800;
The preferred following component of described feedstuff flavouring agent and weight portion content:
Nonyl lactone 5～19, Ethyl vanillin 5～24, omega-pentadecanolide 0.5～3, ethyl maltol 1～6, dihydrocoumarin 1～10, phenmethylol 4～20, ethyl lactate 4～20, ethyl butyrate 5～15, carrier 100～800;
Described carrier is selected from one or more in silica, stone flour or rice bran.
For a preparation method for the feedstuff flavouring agent of premix, it is characterized in that, the method comprises the following steps:
(1) get the raw materials ready according to following component and weight portion content:
Nonyl lactone 4～20, Ethyl vanillin 3～25, omega-pentadecanolide 0.3～2, ethyl maltol 1～8, dihydrocoumarin 1～10, phenmethylol 4～20, ethyl lactate 4～20, ethyl butyrate 5～20, carrier 100～800;
(2) by formula requirement, liquid after first solid, drops into the above-mentioned raw material except carrier in liquid aging tank successively, is uniformly mixed, and mixing time is controlled at 1.5～2.5 hours;
(3) after to be mixed completing, by airtight the essence making placement ageing more than 12 hours;
(4) by the amount of formula requirement, essence is adsorbed with the carrier of 20-30wt%, in mixer, mix 2～6 minutes;
(5) then remaining carrier is dropped into mixer again, mix 1～5 minute, complete and mix rear blowing and sieve and obtain product through vibratory sieve.
Compared with prior art, the present invention has the following advantages:
(1) purer fragrance-natural (natural equivalent) raw material, possesses purer fragrance;
(2) the flavouring agent concentrate of stronger concentration-high concentration;
(3) the special flavouring agent designing for premix specially;
(4) fragrance remaining time is long, and the ability of covering smell is strong, can better act on premix;
(5) this flavouring agent fragrance penetration power is strong, adds cost low, and cost performance is high;
(6) better food calling-natural (natural equivalent) raw material and optimization of C/C composites.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in detail.
Embodiment 1
For a preparation method for the feedstuff flavouring agent of premix, the method comprises the following steps:
(1) get the raw materials ready according to following component and content: nonyl lactone 8kg, Ethyl vanillin 4kg, omega-pentadecanolide 0.5kg, ethyl maltol 3kg, dihydrocoumarin 2kg, phenmethylol 10kg, ethyl lactate 6kg, ethyl butyrate 8kg;
(2) according to the order of liquid after first solid, above-mentioned raw material except carrier is dropped in liquid aging tank, be uniformly mixed, stir 1.6 hours;
(3) after to be mixed completing, by airtight the essence making placement ageing more than 12 hours;
(4) by formula requirement, essence is adsorbed with the silica supports of 40kg, in mixer, mix 2 minutes;
(5) then remaining 120kg silica supports is dropped into mixer, mix 2 minutes, complete mixing;
(6) blowing through the vibratory sieve weighing and bagging that sieves, obtains product.
Embodiment 2
For a preparation method for the feedstuff flavouring agent of premix, the method comprises the following steps:
(1) get the raw materials ready according to following component and content: nonyl lactone 10kg, Ethyl vanillin 5kg, omega-pentadecanolide 0.7kg, ethyl maltol 4kg, dihydrocoumarin 3kg, phenmethylol 10kg, ethyl lactate 7kg, ethyl butyrate 8kg;
(2) according to the order of liquid after first solid, above-mentioned raw material except carrier is dropped in liquid aging tank, be uniformly mixed, stir 2 hours;
(3) after to be mixed completing, by airtight the essence making placement ageing more than 12 hours;
(4) by formula requirement, essence is adsorbed with the silica supports of 50kg, in mixer, mix 2.5 minutes;
(5) then remaining 150kg silica supports is dropped into mixer, mix 2.5 minutes, complete mixing;
(6) blowing through the vibratory sieve weighing and bagging that sieves, obtains product.
Embodiment 3
For a preparation method for the feedstuff flavouring agent of premix, the method comprises the following steps:
(1) get the raw materials ready according to following component and content: nonyl lactone 10kg, Ethyl vanillin 7kg, omega-pentadecanolide 2kg, ethyl maltol 8kg, dihydrocoumarin 5kg, phenmethylol 10kg, ethyl lactate 10kg, ethyl butyrate 8kg;
(2) according to the order of liquid after first solid, above-mentioned raw material except carrier is dropped in liquid aging tank, be uniformly mixed, stir 2.5 hours;
(3) after to be mixed completing, by airtight the essence making placement ageing more than 12 hours;
(4) by formula requirement, essence is adsorbed with the silica supports of 75kg, in mixer, mix 3 minutes;
(5) then remaining 175kg silica supports is dropped into mixer again, mix 3 minutes, complete mixing;
(6) blowing through the vibratory sieve weighing and bagging that sieves, obtains product.
Embodiment 4
For a preparation method for the feedstuff flavouring agent of premix, the method comprises the following steps:
(1) get the raw materials ready according to following component and content: nonyl lactone 4kg, Ethyl vanillin 3kg, omega-pentadecanolide 0.3kg, ethyl maltol 1kg, dihydrocoumarin 1kg, phenmethylol 4kg, ethyl lactate 4kg, ethyl butyrate 5kg;
(2) according to the order of liquid after first solid, above-mentioned raw material except carrier is dropped in liquid aging tank, be uniformly mixed, stir 1.5 hours;
(3) after to be mixed completing, by airtight the essence making placement ageing more than 12 hours;
(4) by formula requirement, essence is adsorbed with the silica supports of 20kg, in mixer, mix 2 minutes;
(5) then remaining 80kg carrier is dropped into mixer again, mix 2 minutes, complete mixing;
(6) blowing through the vibratory sieve weighing and bagging that sieves, obtains product.
Embodiment 5
For a preparation method for the feedstuff flavouring agent of premix, the method comprises the following steps:
(1) get the raw materials ready according to following component and content: nonyl lactone 20kg, Ethyl vanillin 25kg, omega-pentadecanolide 2kg, ethyl maltol 8kg, dihydrocoumarin 10kg, phenmethylol 20kg, ethyl lactate 20kg, ethyl butyrate 20kg;
(2) according to the order of liquid after first solid, above-mentioned raw material except carrier is dropped in liquid aging tank, be uniformly mixed, stir 2.5 hours;
(3) after to be mixed completing, by airtight the essence making placement ageing more than 12 hours;
(4) by formula requirement, essence is adsorbed with the silica supports of 200kg, in mixer, mix 6 minutes;
(5) then remaining 600kg carrier is dropped into mixer again, mix 5 minutes, complete mixing;
(6) blowing through the vibratory sieve weighing and bagging that sieves, obtains product.
Claims (3)
1. for a feedstuff flavouring agent for premix, it is characterized in that, this feedstuff flavouring agent adopts following component and weight portion content:
Nonyl lactone 4～20, Ethyl vanillin 3～25, omega-pentadecanolide 0.3～2, ethyl maltol 1～8, dihydrocoumarin 1～10, phenmethylol 4～20, ethyl lactate 4～20, ethyl butyrate 5～20, carrier 100～800.
2. a kind of feedstuff flavouring agent for premix according to claim 1, is characterized in that, described carrier is selected from one or more in silica, stone flour or rice bran.
3. a preparation method for the feedstuff flavouring agent for premix as claimed in claim 1, is characterized in that, the method comprises the following steps:
(1) get the raw materials ready according to following component and weight portion content:
Nonyl lactone 4～20, Ethyl vanillin 3～25, omega-pentadecanolide 0.3～2, ethyl maltol 1～8, dihydrocoumarin 1～10, phenmethylol 4～20, ethyl lactate 4～20, ethyl butyrate 5～20, carrier 100～800:
(2) by formula requirement, liquid after first solid, drops into above-mentioned raw material except carrier in liquid aging tank successively, is uniformly mixed, and mixing time is controlled at 1.5～2.5 hours;
(3) after to be mixed completing, by airtight the mixture making placement ageing more than 12 hours;
(4) by formula requirement, essence is adsorbed with 20～30wt% carrier, in mixer, mix 2～6 minutes;
(5) then remaining carrier is dropped into mixer again, mix 1～5 minute, complete and mix rear blowing and sieve and obtain product through vibratory sieve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201110274001.1A CN102987084B (en) | 2011-09-15 | 2011-09-15 | Feed fragrance agent used in premix, and preparation method thereof |
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| CN201110274001.1A CN102987084B (en) | 2011-09-15 | 2011-09-15 | Feed fragrance agent used in premix, and preparation method thereof |
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| CN102987084A CN102987084A (en) | 2013-03-27 |
| CN102987084B true CN102987084B (en) | 2014-08-20 |
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| CN105746905A (en) * | 2016-03-01 | 2016-07-13 | 湖南晶天科技实业有限公司 | Feed additive and preparation method thereof |
| CN108713645A (en) * | 2018-05-15 | 2018-10-30 | 成都大帝汉克生物科技有限公司 | A kind of special fatty acid product improving beef cattle growth performance |
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| FR2956661B1 (en) * | 2010-02-24 | 2012-02-10 | Rhodia Operations | PROCESS FOR THE PREPARATION OF A COMPOSITION COMPRISING A COMPOUND BASED ON VANILLINE AND ETHYLVANILLIN, COMPOSITION OBTAINED AND APPLICATIONS THEREOF |
| CN101965964A (en) * | 2010-09-25 | 2011-02-09 | 上海美农饲料有限公司 | Method for preparing milk flavor essence, prepared milk flavor essence thereof and related feed flavoring agent |
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Application publication date: 20130327 Assignee: Chengdu Mei Yide Bioisystech Co., Ltd Assignor: Shanghai Menon Animal Nutrition Technology Co., Ltd. Contract record no.: 2017510000046 Denomination of invention: Feed fragrance agent used in premix, and preparation method thereof Granted publication date: 20140820 License type: Common License Record date: 20171208 |
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