CN110122670A - The preparation method of olibanum type feed addictive - Google Patents
The preparation method of olibanum type feed addictive Download PDFInfo
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- CN110122670A CN110122670A CN201910390897.6A CN201910390897A CN110122670A CN 110122670 A CN110122670 A CN 110122670A CN 201910390897 A CN201910390897 A CN 201910390897A CN 110122670 A CN110122670 A CN 110122670A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/10—Animal feeding-stuffs obtained by microbiological or biochemical processes
- A23K10/14—Pretreatment of feeding-stuffs with enzymes
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
- A23K10/37—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/105—Aliphatic or alicyclic compounds
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/111—Aromatic compounds
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/116—Heterocyclic compounds
- A23K20/121—Heterocyclic compounds containing oxygen or sulfur as hetero atom
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/116—Heterocyclic compounds
- A23K20/121—Heterocyclic compounds containing oxygen or sulfur as hetero atom
- A23K20/126—Lactones
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/158—Fatty acids; Fats; Products containing oils or fats
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/28—Silicates, e.g. perlites, zeolites or bentonites
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/60—Feeding-stuffs specially adapted for particular animals for weanlings
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
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Abstract
The present invention discloses a kind of preparation method of olibanum type feed addictive, this method comprises: buffer solution of the secure ph range 6.0 to 7.0, buffer solution is prepared by least one acid solution and a kind of aqueous slkali by preset ratio；Butter emulsion of the mass concentration value range of butter 50% to 70% is made by buffer solution；Lipase is added into butter emulsion, butter zymolyte is made；Ingredient is added into butter zymolyte to obtain imitative olibanum essence, ingredient includes: butter zymolyte, propylene glycol, diacetyl, butyl butyryl lactate, dihydrocoumarin, arbricolin, peach aldehyde, third caprylolactone, gamma decalactone, delta-decalactone, fourth position dodecalactone, ethylmaltol, Ethyl vanillin；Imitative olibanum is adsorbed using absorption carrier and is refined into olibanum type feed addictive powder, wherein the value range 1 to 2 of absorption carrier and the mass ratio of imitative olibanum essence.The invention has the beneficial effects that providing a kind of preparation method for capableing of the more natural olibanum type feed addictive of fragrance.
Description
Technical field
This application involves animal feed preparation fields, in particular to a kind of preparation side of olibanum type feed addictive
Method.
Background technique
Feed ingredient is complicated, and wherein the bad smells weight such as dregs of beans, fish meal, influences feed intake.Especially to rigid wean children
Age mammal, bad feed odor impact feed palatability aggravates stress reaction, therefore milk flavouring agent is dynamic in young age lactation
Using extensive in object feed.Using milk flavouring agent prepared by the relevant technologies mainly by manually being compounded by monomer perfume
At fragrance is strong and is pungent, and certain limitation is brought to animal feed phagostimulating effect.
Summary of the invention
To achieve the goals above, according to the one aspect of the application, a kind of system of olibanum type feed addictive is provided
Preparation Method, preparation method include:
Buffer solution of the secure ph range 6.0 to 7.0, buffer solution is by least one acid solution and a kind of aqueous slkali
It is prepared by preset ratio；
Butter emulsion of the mass concentration value range of butter 50% to 70% is made by buffer solution；
Lipase is added into butter emulsion, butter zymolyte is made；
Ingredient is added into butter zymolyte to obtain imitative olibanum essence, ingredient includes: butter zymolyte, propylene glycol, fourth
Diketone, butyl butyryl lactate, dihydrocoumarin, arbricolin, peach aldehyde, third caprylolactone, gamma decalactone, delta-decalactone, fourth
Position dodecalactone, ethylmaltol, Ethyl vanillin；
Imitative olibanum is adsorbed using absorption carrier and is refined into olibanum type feed addictive powder, wherein absorption carrier and imitative cream
The value range 1 to 2 of the mass ratio of essence.
Further, acid solution is aqueous citric acid solution, and aqueous slkali is disodium hydrogen phosphate.
Further, the value range of the molar concentration of acid solution is 0.15mol/L to 0.2mol/L.
Further, the value range of the molar concentration of aqueous slkali is 0.05mol/L to 0.15mol/L.
Further, buffer solution and butter mixed configuration become butter mixed liquor, then emulsify butter mixed liquor and obtain
Butter emulsion.
Further, it is heated to preset temperature before emulsification butter mixed liquor and carries out pasteurize preset duration.
Further, the value range of preset temperature is 80 DEG C to 90 DEG C.
Further, the value range of the preset duration of pasteurize is 20 minutes to 40 minutes.
Further, ingredient includes according to weight percent: butter zymolyte 40 to 80%, propylene glycol 3 to 5%, fourth two
Ketone 2 to 8%, butyl butyryl lactate 0.5 to 1.5%, dihydrocoumarin 0.5 to 2%, arbricolin 1 to 4%, peach aldehyde 0.5 to 2%,
Third caprylolactone 2 to 8%, gamma decalactone 2 to 8%, delta-decalactone 1 to 4.5%, fourth position dodecalactone 0.5 to 2%, second
Base maltol 3 to 7%, Ethyl vanillin 4 to 8%.
Further, absorption carrier includes: silica, system one or more of chaff and zeolite powder.
The invention has the beneficial effects that providing a kind of system for capableing of the more natural olibanum type feed addictive of fragrance
Preparation Method.
Detailed description of the invention
Fig. 1 is according to a kind of schematic process flow diagram of embodiment of the application；
Fig. 2 is the preparation method butter zymolyte GC map obtained of embodiments herein 1.
Specific embodiment
The preparation method of olibanum type feed addictive as shown in Figure 1 include: secure ph range 6.0 to 7.0 it is slow
Solution is rushed, buffer solution is prepared by least one acid solution and a kind of aqueous slkali by preset ratio；Butter is made by buffer solution
Butter emulsion of the mass concentration value range 50% to 70%；Lipase is added into butter emulsion, butter enzymatic hydrolysis is made
Object；Ingredient is added into butter zymolyte to obtain imitative olibanum essence, ingredient includes: butter zymolyte, propylene glycol, diacetyl,
Butyl butyryl lactate, dihydrocoumarin, arbricolin, peach aldehyde, third caprylolactone, gamma decalactone, delta-decalactone, Ding Weishi bis-
Lactone, ethylmaltol, Ethyl vanillin；Imitative olibanum is adsorbed using absorption carrier and is refined into olibanum type feed addictive powder,
Wherein, the value range 1 to 2 of absorption carrier and the mass ratio of imitative olibanum essence.
Specifically, acid solution is aqueous citric acid solution, aqueous slkali is disodium hydrogen phosphate.
Specifically, the value range of the molar concentration of acid solution is 0.15mol/L to 0.2mol/L.
Specifically, the value range of the molar concentration of aqueous slkali is 0.05mol/L to 0.15mol/L.
Specifically, buffer solution and butter mixed configuration become butter mixed liquor, then emulsifies butter mixed liquor and obtain
Butter emulsion.
Specifically, being heated to preset temperature before emulsification butter mixed liquor and carrying out pasteurize preset duration.
Specifically, the value range of preset temperature is 80 DEG C to 90 DEG C.
Specifically, the value range of the preset duration of pasteurize is 20 minutes to 40 minutes.
Specifically, ingredient includes according to weight percent: butter zymolyte 40 to 80%, propylene glycol 3 to 5%, fourth two
Ketone 2 to 8%, butyl butyryl lactate 0.5 to 1.5%, dihydrocoumarin 0.5 to 2%, arbricolin 1 to 4%, peach aldehyde 0.5 to 2%,
Third caprylolactone 2 to 8%, gamma decalactone 2 to 8%, delta-decalactone 1 to 4.5%, fourth position dodecalactone 0.5 to 2%, second
Base maltol 3 to 7%, Ethyl vanillin 4 to 8%.
Specifically, absorption carrier includes: silica, system one or more of chaff and zeolite powder.
As specific scheme, preparation method of the invention specifically comprises the following steps:
(1) buffer solution is prepared, is pressed using 0.2mol/L disodium hydrogen phosphate and 0.1mol/L aqueous citric acid solution
Ratio is configured to the buffer solution of pH6.0~7.0.
(2) it weighs butter (solid), dissolves by heating, step (1) made buffer solution is added after dissolution and is made into butter quality
Accounting reaches the oil-water mixture of 50~70% concentration, is warming up to 85 DEG C, and pasteurize 20 minutes, cooling down to room temperature,
Matter machine 10000-16000rpm machinery emulsification 1~3 minute, obtain emulsion.
(3) lipase for accounting for substrate (butter) quality 0.5-1.5% is added into butter emulsion made from step (2).
45~50 DEG C of sustained oscillations digest 5-10 hours, 85 DEG C of enzyme deactivation 30min, stand 1h cooling, butter emulsion is due to high temperature
Water-oil phase natural layering extracts upper oil phase, obtains butter zymolyte.
The present invention screens a variety of lipase, selectes two kinds of enzyme LMERJ0451814 (it is wild) and LBK-B4000 (green micro- health)
It is best.
(4) imitative breast milk milk flavor, formulation weight accounting: butter are deployed by basic note of butter zymolyte obtained by step (3)
Zymolyte 40~80%, propylene glycol 3~5%, diacetyl 2~8%, butyl butyryl lactate 0.5~1.5%, dihydrocoumarin 0.5
~2%, arbricolin 1~4%, peach aldehyde 0.5~2%, third caprylolactone 2~8%, gamma decalactone 2~8%, delta-decalactone 1
~4.5%, fourth position dodecalactone 0.5~2%, ethylmaltol 3~7%, Ethyl vanillin 4~8%.After the completion of formula addition
It is sufficiently stirred dissolution, container closure curing is for 24 hours to get to imitative breast milk milk flavor.
(5) imitative breast milk milk flavor obtained by step (4) adsorbed using feed with carrier to (essence is the same as carrier ratio
Example 1:1~2), it is uniformly mixed, obtains the good feed addictive powder of free-running property.
The present invention includes silica, system chaff and zeolite powder etc. using feeding carrier.
The real butter zymolyte that the present invention obtains, short-chain fat acid content reach 35% or more, are re-dubbed imitative breast milk milk
Fragrant feed addictive can assign feed addictive natural smelling of milk-childish flavor, and the milk fragrance with the allotment of market Common Artificial monomer is raised
Feed additives compare, less than flavor strength has, but the purer nature of milk pleasure degree.
The present invention is further elaborated below with reference to embodiment, but institute's protection scope of the present invention is without being limited thereto.
Embodiment 1
(1) buffer solution is prepared, is pressed using 0.2mol/L disodium hydrogen phosphate and 0.1mol/L aqueous citric acid solution
Ratio is configured to the buffer solution of pH7.0.
(2) 200 grams of butter (solid) is weighed, is dissolved by heating, step (1) made buffer solution is added after dissolution and is made into butter
Quality accounting reaches the oil-water mixture of 50% concentration, is warming up to 85 DEG C, and pasteurize 20 minutes, cooling down to room temperature,
Matter machine 16000rpm machinery emulsification 1 minute, obtain emulsion.
(3) 3.0 grams of lipase LMERJ0451814 (it is wild) is added into butter emulsion made from step (2).50℃
Sustained oscillation digests 5 hours, 85 DEG C of enzyme deactivation 30min, stands 1h cooling, and butter emulsion is natural due to high temperature water-oil phase
Layering extracts upper oil phase, obtains 175 grams of butter zymolyte.
(4) imitative breast milk milk flavor, formulation weight accounting: butter are deployed by basic note of butter zymolyte obtained by step (3)
Zymolyte 80%, propylene glycol 3%, diacetyl 2%, butyl butyryl lactate 0.5%, dihydrocoumarin 0.5%, arbricolin 1%, peach
Aldehyde 0.5%, third caprylolactone 2%, gamma decalactone 2%, delta-decalactone 1%, fourth position dodecalactone 0.5%, ethyl malt
Phenol 3%, Ethyl vanillin 4%.Dissolution is sufficiently stirred after the completion of formula addition, and container closure curing is for 24 hours to get to imitating breast milk milk
200 grams of essence.
(5) imitative breast milk milk flavor obtained by step (4) is adsorbed into (essence with carrier silicas using feed
With carrier ratio 1:1, it is uniformly mixed, obtains 400 grams of the good feed addictive powder of free-running property.
The test map of product is made by embodiment 1 as shown in Fig. 2, butter zymolyte is by butter long chain fatty acids fat
For the digestion of enzyme enzyme at short chain aromatic series fatty acid, the smelling of milk-childish is with rich flavor, gas chromatogram fixative quantitative detection, wherein butyric acid content
3.45%, caproic acid content 3.17%, octanoic acid 3.26%, capric acid 5.51%, lauric acid/dodecanoic acid 5.78%, tetradecylic acid 6.0%, hexadecylic acid
10.0%.
Embodiment 2
(1) buffer solution is prepared, is pressed using 0.2mol/L disodium hydrogen phosphate and 0.1mol/L aqueous citric acid solution
Ratio is configured to the buffer solution of pH6.0.
(2) 500 grams of butter (solid) is weighed, is dissolved by heating, step (1) made buffer solution is added after dissolution and is made into butter
Quality accounting reaches the oil-water mixture of 70% concentration, is warming up to 85 DEG C, and pasteurize 20 minutes, cooling down to room temperature,
Matter machine 10000rpm machinery emulsification 3 minutes, obtain emulsion.
(3) 2.5 grams of addition lipase LBK-B4000 (green micro- health) into butter emulsion made from step (2).45 DEG C are held
Continuous concussion enzymatic hydrolysis 10 hours, 85 DEG C of enzyme deactivation 30min, 1h cooling is stood, butter emulsion is natural due to high temperature water-oil phase
Layering extracts upper oil phase, obtains 430 grams of butter zymolyte.
(4) imitative breast milk milk flavor, formulation weight accounting: butter are deployed by basic note of butter zymolyte obtained by step (3)
Zymolyte 40%, propylene glycol 5%, diacetyl 8%, butyl butyryl lactate 1.5%, dihydrocoumarin 2%, arbricolin 4%, peach aldehyde
2%, third caprylolactone 8%, gamma decalactone 8%, delta-decalactone 4.5%, fourth position dodecalactone 2%, ethylmaltol
7%, Ethyl vanillin 8%.Dissolution is sufficiently stirred after the completion of formula addition, and container closure curing is for 24 hours to get to imitating breast milk milk
1000 grams of essence.
(5) imitative breast milk milk flavor obtained by step (4) is adsorbed into (the same load of essence with carrier system chaff using feed
Body ratio 1:2 is uniformly mixed, obtains 3 kilograms of the good feed addictive powder of free-running property.
Embodiment 3
(1) buffer solution is prepared, is pressed using 0.2mol/L disodium hydrogen phosphate and 0.1mol/L aqueous citric acid solution
Ratio is configured to the buffer solution of pH6.0.
(2) 2000 grams of butter (solid) is weighed in 5L reactor tank, is dissolved by heating, and it is made slow that step (1) is added after dissolution
It rushes solution and is made into the oil-water mixture that butter quality accounting reaches 60% concentration, be warming up to 85 DEG C, pasteurize 20 minutes, cool down
It is cooled to room temperature, homogenizer 12000rpm machinery emulsification 2 minutes obtains emulsion.
(3) 20 grams of addition lipase LBK-B4000 (green micro- health) into butter emulsion made from step (2).45 DEG C are held
Continuous concussion enzymatic hydrolysis 7 hours, 85 DEG C of enzyme deactivation 30min, 1h cooling is stood, butter emulsion is divided naturally due to high temperature water-oil phase
Layer extracts upper oil phase, obtains 1700 grams of butter zymolyte.
(4) imitative breast milk milk flavor, formulation weight accounting: butter are deployed by basic note of butter zymolyte obtained by step (3)
Zymolyte 50%, propylene glycol 4%, diacetyl 7%, butyl butyryl lactate 1.5%, dihydrocoumarin 1.5%, arbricolin 3%, peach
Aldehyde 2.5%, third caprylolactone 5%, gamma decalactone 6%, delta-decalactone 5%, fourth position dodecalactone 2.5%, ethyl malt
Phenol 5.5%, Ethyl vanillin 6.5%.Dissolution is sufficiently stirred in formula after the completion of adding, container closure curing is imitative female to get arriving for 24 hours
3000 grams of newborn milk flavor.
(5) imitative breast milk milk flavor obtained by step (4) is inhaled using feed with carrier silicas and mountain flour
Attached (essence: silica: mountain flour=1:1.5:0.5), multifunctional mini-mixer are uniformly mixed, and obtain the good feed addition of free-running property
9 kilograms of agent powder.
The imitative breast milk milk Flavor feed addictive that the present invention obtains is diluted to 1000ppm using mountain flour and carries out fragrance assessment
Comparison.Evaluation criteria is as shown in table 1.
Imitative three embodiment mountain flours of breast milk milk Flavor feed addictive are diluted to 1000ppm, aroma sensory's assessment result
It is shown in Table 2.Three embodiment sensory evaluation scorings of cream milk Flavor feed addictive of the invention are attained by 8.5 or more.
The foregoing is merely preferred embodiment of the present application, are not intended to limit this application, for the skill of this field
For art personnel, various changes and changes are possible in this application.Within the spirit and principles of this application, made any to repair
Change, equivalent replacement, improvement etc., should be included within the scope of protection of this application.
Table 1 is fragrance evaluation criteria
Table 2 is that imitative breast milk milk Flavor feed addictive fragrance assesses table.
Claims (10)
1. a kind of preparation method of olibanum type feed addictive, it is characterised in that:
The preparation method includes:
Buffer solution of the secure ph range 6.0 to 7.0, the buffer solution is by least one acid solution and a kind of aqueous slkali
It is prepared by preset ratio；
Butter emulsion of the mass concentration value range of butter 50% to 70% is made by the buffer solution；
Lipase is added into the butter emulsion, butter zymolyte is made；
Ingredient is added into the butter zymolyte to obtain imitative olibanum essence, the ingredient includes: butter zymolyte, and the third two
Alcohol, diacetyl, butyl butyryl lactate, dihydrocoumarin, arbricolin, peach aldehyde, third caprylolactone, gamma decalactone, in the last of the ten Heavenly stems of fourth position
Ester, fourth position dodecalactone, ethylmaltol, Ethyl vanillin；
The imitative olibanum is adsorbed using absorption carrier and is refined into olibanum type feed addictive powder, wherein absorption carrier with it is described
The value range 1 to 2 of the mass ratio of imitative olibanum essence.
2. the preparation method of olibanum type feed addictive according to claim 1, it is characterised in that:
The acid solution is aqueous citric acid solution, and the aqueous slkali is disodium hydrogen phosphate.
3. the preparation method of olibanum type feed addictive according to claim 2, it is characterised in that:
The value range of the molar concentration of the acid solution is 0.15mol/L to 0.2mol/L.
4. the preparation method of olibanum type feed addictive according to claim 2, it is characterised in that:
The value range of the molar concentration of the aqueous slkali is 0.05mol/L to 0.15mol/L.
5. the preparation method of olibanum type feed addictive according to claim 1, it is characterised in that:
The buffer solution and butter mixed configuration become butter mixed liquor, then emulsify the butter mixed liquor and obtain the Huang
Oil emulsion.
6. the preparation method of olibanum type feed addictive according to claim 5, it is characterised in that:
It is heated to preset temperature before emulsifying the butter mixed liquor and carries out pasteurize preset duration.
7. the preparation method of olibanum type feed addictive according to claim 6, it is characterised in that:
The value range of the preset temperature is 80 DEG C to 90 DEG C.
8. the preparation method of olibanum type feed addictive according to claim 6, it is characterised in that:
The value range of the preset duration of the pasteurize is 20 minutes to 40 minutes.
9. the preparation method of olibanum type feed addictive according to claim 1, it is characterised in that:
The ingredient includes according to weight percent: butter zymolyte 40 to 80%, propylene glycol 3 to 5%, diacetyl 2 to 8%,
Butyl butyryl lactate 0.5 to 1.5%, dihydrocoumarin 0.5 to 2%, arbricolin 1 to 4%, peach aldehyde 0.5 to 2%, third pungent interior
Ester 2 to 8%, gamma decalactone 2 to 8%, delta-decalactone 1 to 4.5%, fourth position dodecalactone 0.5 to 2%, ethylmaltol 3
To 7%, Ethyl vanillin 4 to 8%.
10. the preparation method of olibanum type feed addictive according to claim 1, it is characterised in that:
The absorption carrier includes: silica, system one or more of chaff and zeolite powder.
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| CN113057254A (en) * | 2021-04-28 | 2021-07-02 | 味氏（广东）生物科技股份有限公司 | Preparation method and application of water-soluble sweet milk essence suitable for drinking water, porridge material and liquid feed of mammals |
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