CN103565686A - Permanent plant hair dye and preparation method thereof - Google Patents
Permanent plant hair dye and preparation method thereof Download PDFInfo
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- CN103565686A CN103565686A CN201210276597.3A CN201210276597A CN103565686A CN 103565686 A CN103565686 A CN 103565686A CN 201210276597 A CN201210276597 A CN 201210276597A CN 103565686 A CN103565686 A CN 103565686A
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- extract
- hair dye
- cortex eucommiae
- hair
- armeniacae amarum
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Abstract
The invention provides a permanent plant hair dye and a preparation method thereof. The permanent plant hair dye is composed of a eucommia ulmoides extract, an almond extract and a matrix. The raw materials selected for the plant hair dye have no toxic and side effects; the plant hair dye is capable of dyeing white hair into natural black hair, good in stability for sunshine and daily liquid shampoo and free of irritation; the permanent plant hair dye is also capable of fundamentally improving hair quality, reducing white hair and generating a lasting nourishing effect on the hair if being used for a long time.
Description
Technical field
The invention belongs to a kind of botanical hair dye in cosmetology field.
Background technology
Along with the raising of living standards of the people, hair dye has become a kind of daily cosmetics and has entered huge numbers of families.Hair dye can make up some congenital defects or posteriori sorry, makes color development back to nature.Meanwhile, hair dye can also change single hair color as individual character and fashionable interspersing, to pursue colorful color development.
Yet hair dye directly under the jurisdiction of a municipal government mostly is synthetic, hair dyeing causes that irritated and carcinogenic is the two large serious problems that hair dyeing industry faces.According to U.S. FDA statistics, use chemical hair dye skin allergy rate up to 0.15%.About the possible carcinogenesis of hair dye, relevant report is a lot of in recent years, arouses great concern, and has also increased the worry of people to chemical hair dye safety simultaneously.Along with progressively improving and continuous pursuit to beauty treatment science of consumer health consciousness, on hair dyeing market in the urgent need to safety non-toxic, can not cause the botanical hair dye of serious toxic and side effects.
The Cortex Eucommiae be the Eucommiaceae plant Cortex Eucommiae (
eucommia ulmoidesoliver) dry bark, tool invigorating the liver and kidney, bone and muscle strengthening, blood pressure lowering, many effects such as antiabortive.The Cortex Eucommiae is the traditional famous and precious nourishing " traditional Chinese medicines " of China, famous medical book < < Sheng Nong's herbal classic > > in ancient times, < < Compendium of Materia Medica > >, in the books such as < < Guang Qunfang Pu > > and current authoritative medical book < < Traditional Chinese Medicine voluminous dictionary > >, be all listed in top grade.The traditional Chinese medical science thinks, the main generation marrow of kidney, is the congenital foundation, its Hua Fa.The Cortex Eucommiae can reach the effect of nourishing hair by invigorating the liver and kidney.Modern medicine shows the further research of the Cortex Eucommiae, and it is rich in aucubin, pine refers to the active ingredients such as alcohol diglucoside, vitamin C, has the metabolism of promotion, strengthens immunity, slow down aging, adjusting blood pressure, suppresses the comprehensively effect such as cancer.
Semen Armeniacae Amarum be rosaceous plant Fructus Pruni (
prunus armeniacal.) kernel has sending down the abnormal ascending QI relieving cough and asthma on tcm clinical practice, the effect of loosening bowel to relieve constipation.Modern study proves, fatty oil and other composition contained in Semen Armeniacae Amarum can make keratodermatitis softening, moisturize skin protection, have the effect of neuroprotective peripheral vessel and histoorgan, but and can kill antibacterial.In addition, by the hydrocyanic acid that enzyme hydrolysis generated, can be suppressed the active tryrosinase in body, eliminate pigmentation, freckle, black speck etc., thereby reach the effect of beauty treatment.
In 2010, we declared a Chinese medicament hair dye patent (application number 201010149217.0), had announced a kind of Chinese medicament hair dye that aucubin and beta-glucosidase be main active of take.In actual production, find, this technology production cost is very high, has hindered its application.The present invention is on this basis, and related process has been done to significant improvement, has original two doses to become potion, makes it have that production technology is simple, the advantage of low production cost.
Summary of the invention
Object of the present invention is exactly to provide a kind of permanent botanical hair dye without any side effects and preparation method thereof for above-mentioned background technology.
Permanent botanical hair dye of the present invention, is consisted of Cortex Eucommiae extract, Semen Armeniacae Amarum extract and substrate, wherein: in Cortex Eucommiae extract, except containing active component aucubin, also contain multiple nourishing hair, improve the active component of hair quality; In Semen Armeniacae Amarum extract, except containing active component beta-glucosidase, also contain the multiple active component with cosmetology.The ratio of Cortex Eucommiae extract and Semen Armeniacae Amarum extract is 1:0.1 ~ 1:1.
The preparation method of the permanent botanical hair dye of the present invention, is consisted of following step:
1. the Cortex Eucommiae of take is prepared Cortex Eucommiae extract as raw material;
2. the Semen Armeniacae Amarum of take is prepared Semen Armeniacae Amarum extract as raw material;
3. Cortex Eucommiae extract, Semen Armeniacae Amarum extract are mixed according to weight ratio 1:0.1 ~ 1:1, in addition corresponding substrate is mixed mutually with appropriate excipient and is made corresponding dosage form.
Cortex Eucommiae extract be take the Cortex Eucommiae (comprise the garbage of seed of bark of eucommia, Cortex Eucommiae, Folium Eucommiae, Cortex Eucommiae industry single or its combination) during as raw material, raw material is after appropriateness is pulverized, adopting aquiferous ethanol (or methanol) or dehydrated alcohol (or methanol) is solvent, determining alcohol is from 5-100%, liquid ratio 1:2 ~ 1:20 is advisable, reflux, extract, 1-3 time, each 30-150 minute.Said extracted liquid obtains extractum through concentrating under reduced pressure, and extractum, through solvent extraction and the pure processing of macroporous resin, obtains Cortex Eucommiae extract.
It is raw material that Semen Armeniacae Amarum extract be take fresh or dry Semen Armeniacae Amarum, Semen pruni armeniacae, jordan almond etc., through appropriateness pulverize and defat after, ammonia lixiviate with ethanol (or methanol) precipitation acquisition Semen Armeniacae Amarum extract.
After Cortex Eucommiae extract and Semen Armeniacae Amarum extract are mixed according to weight ratio 1:0.1 ~ 1:1, add the substrate that excipient and medicine and cosmetics are conventional, make corresponding dosage form, as unguentum, Emulsion, water preparation, mousse etc., can obtain permanent botanical hair dye.During use, be applied on pretreatment hair after 30-60 minute, with clear water, rinsed well, hair can be dyed to nature black.Hair after dyeing, can variable color or fade after shampoo repeatedly washs, and can not fade or variable color under sun exposure simultaneously yet, and shampoo and sun exposure are had to good resistance.
Raw material of the present invention is the medicinal and edible Chinese medicine of safety non-toxic, without any side effects, safe and reliable.Hair dye proves through rabbit skin irritation test repeatedly, to skin without any stimulation.
The specific embodiment
Two embodiment are below further introductions made for the present invention.The present invention can prove by following examples, but should not think that these embodiment are the restrictions to technical scope of the present invention.
Embodiment mono-:
With seed of bark of eucommia and Semen Armeniacae Amarum, for selecting raw material, carry out permanent botanical hair dye production.
Prepare Cortex Eucommiae extract:
Get dry seed of bark of eucommia 1.0 Kg, pulverize and cross 10 mesh sieves, be placed in the round-bottomed flask of 10 L, add 5 liter of 95% alcohol reflux 2 times, each 1 hour, filter to get filtrate, merge 2 extracting solution and be evaporated to dryly, then use distilled water suspendible, add isopyknic cyclohexane extraction extraction 2 times, water layer after extraction carries out purification by XDA-8 resin (amount of resin is weight in wet base 2 kg) to it, after the flow velocity loading with 10 mL/min, and standing adsorption 1 hour.With after 2000 mL water elutions, then use 6000 mL 10% ethanol elutions.Reclaim under reduced pressure 10% ethanol elution partly obtains Cortex Eucommiae extract.
Semen Armeniacae Amarum extract:
Get bitter Fructus Pruni powder (crossing 40 mesh sieves) 80 g after ether defatting, add 500 ml 0.06 mol/L ammonia merceration 24 hours, collect filtrate, add glacial acetic acid and neutralize pH=4.0, limit edged stirs, standing rear sucking filtration, filtrate adds 95% ethanol of 4 times of amounts, and collecting precipitation obtains Semen Armeniacae Amarum extract after being dried.
Prepare hair dye:
1) take off row substrate:
Cera alba 5.0 g glyceryl monostearate 3.5 g
Lanoline 1.0 g polyoxyethylene sorbitan monostearate 3.0 g
Paraffin 2.0 g liquid paraffin 20 g
Oleum lini 10.0 g CMC-Na 10.0 g
Gelatin 30 g Tween-80 10 g
2) under the condition of slight fever, mix and constantly stir, making its mix homogeneously, adding 20 grams of Cortex Eucommiae extract, 4 grams of Semen Armeniacae Amarum extracts, then adding distil water to 200 gram, make emulsifiable paste through high-speed emulsifying machine emulsifying, obtains permanent botanical hair dye.
According to externally used paste skin irritation test operational approach, the present embodiment unguentum rabbit of being in of having hair dyed is tested, experimental results show that tested material that above-mentioned substrate is made into is to skin nonirritant.
Embodiment bis-:
Take Cortex Eucommiae and Semen Armeniacae Amarum as raw material, carry out permanent botanical hair dye production.
Prepare Cortex Eucommiae extract:
Get dry Cortex Eucommiae 1.0 Kg, be ground into after coarse powder, be placed in the round-bottomed flask of 10 L, add 7 liters of methanol eddies to extract 2 times, each 1 hour, by 4 layers of filtered through gauze, merge extracting solution 2 times.Extracting solution is evaporated to dry, and the brown extractum obtaining adds after 1000 mL distilled water suspendibles, and centrifuging and taking supernatant carries out purification by XDA-7 resin (amount of resin is weight in wet base 1.5 kg) to it, collects 10% ethanol elution part, after concentrating, obtains Cortex Eucommiae extract.
Prepare Semen Armeniacae Amarum extract:
Semen Armeniacae Amarum method for preparing extractive is with embodiment mono-.
Prepare hair dye:
1) take off row substrate:
Cera alba 5.0 g glyceryl monostearate 3.5 g
Lanoline 1.0 g polyoxyethylene sorbitan monostearate 3.0 g
Paraffin 2.0 g liquid paraffin 20 g
Oleum lini 10.0 g CMC-Na 10.0 g
Gelatin 30 g Tween-80 10 g
2) under the condition of slight fever, mix and constantly stir, making its mix homogeneously, adding 20 grams of Cortex Eucommiae extract, 10 grams of Semen Armeniacae Amarum extracts, then add distilled water to 200 gram, and through high-speed emulsifying machine emulsifying, make emulsifiable paste, obtain permanent botanical hair dye.
According to externally used paste skin irritation test operational approach, the present embodiment unguentum rabbit of being in of having hair dyed is tested, experimental results show that tested material that above-mentioned substrate is made into is to skin nonirritant.
Claims (5)
1. a permanent botanical hair dye, is consisted of Cortex Eucommiae extract, Semen Armeniacae Amarum extract and substrate.
2. Cortex Eucommiae extract according to claim 1, is characterized in that: the selected raw material of extract can be single thing or its mixture of the relevant garbage in seed of bark of eucommia, Cortex Eucommiae, Folium Eucommiae or Cortex Eucommiae industry.
3. Semen Armeniacae Amarum extract according to claim 1, is characterized in that: the selected raw material of extract can be single thing or its mixture of Semen Armeniacae Amarum, Semen pruni armeniacae or jordan almond.
4. a kind of method of preparing botanical hair dye according to claim 1 and 2, is characterized in that: Cortex Eucommiae extract is to take the Cortex Eucommiae as raw material, the extract of preparing after extraction, extraction and resin purification.
5. according to a kind of method of preparing botanical hair dye described in claim 1 or 3, it is characterized in that: Semen Armeniacae Amarum extract is to take Semen Armeniacae Amarum as raw material the extract of preparation after extracting, precipitate, being dried.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210276597.3A CN103565686A (en) | 2012-08-06 | 2012-08-06 | Permanent plant hair dye and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210276597.3A CN103565686A (en) | 2012-08-06 | 2012-08-06 | Permanent plant hair dye and preparation method thereof |
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| CN103565686A true CN103565686A (en) | 2014-02-12 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105456053A (en) * | 2015-04-17 | 2016-04-06 | 武汉海吉亚生物科技有限公司 | Permanent hair dye prepared from dye and enzyme sourced from natural plants |
| CN107811910A (en) * | 2017-11-02 | 2018-03-20 | 杨寿 | One kind discoloration cream rinse |
| CN108653130A (en) * | 2018-06-14 | 2018-10-16 | 广州植境生物科技有限公司 | A kind of draft Haircare composition containing shrubby sophora extract |
| CN111568960A (en) * | 2019-02-15 | 2020-08-25 | 伊德姆有限公司 | Agent for inhibiting and improving gray hair and method for producing same |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101836945A (en) * | 2010-04-13 | 2010-09-22 | 武汉大学 | Chinese medicinal hair dye and preparation method thereof |
-
2012
- 2012-08-06 CN CN201210276597.3A patent/CN103565686A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101836945A (en) * | 2010-04-13 | 2010-09-22 | 武汉大学 | Chinese medicinal hair dye and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105456053A (en) * | 2015-04-17 | 2016-04-06 | 武汉海吉亚生物科技有限公司 | Permanent hair dye prepared from dye and enzyme sourced from natural plants |
| CN105456053B (en) * | 2015-04-17 | 2018-07-27 | 武汉海吉亚生物科技有限公司 | Permanent hairdye prepared by a kind of dyestuff and enzyme by natural botanical source |
| CN107811910A (en) * | 2017-11-02 | 2018-03-20 | 杨寿 | One kind discoloration cream rinse |
| CN108653130A (en) * | 2018-06-14 | 2018-10-16 | 广州植境生物科技有限公司 | A kind of draft Haircare composition containing shrubby sophora extract |
| CN111568960A (en) * | 2019-02-15 | 2020-08-25 | 伊德姆有限公司 | Agent for inhibiting and improving gray hair and method for producing same |
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Application publication date: 20140212 |