CN107744483A - A kind of wormwood flavones nti-freckle gel - Google Patents
A kind of wormwood flavones nti-freckle gel Download PDFInfo
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- CN107744483A CN107744483A CN201711151358.4A CN201711151358A CN107744483A CN 107744483 A CN107744483 A CN 107744483A CN 201711151358 A CN201711151358 A CN 201711151358A CN 107744483 A CN107744483 A CN 107744483A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
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- Cosmetics (AREA)
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Abstract
The invention belongs to caused by cosmetics for special use field, more particularly to a kind of wormwood flavones nti-freckle gel, it is characterised in that be prepared by following weight part ratios：Wormwood extract 23~26%, water-solubleazone 4.5~5.5%, gel 0.8~1.2%, NMF 1~1.5%, surfactant 2~3%, cosurfactant 0.5~1%, purified water polishing to 100%.It is an advantage of the current invention that wormwood extract simple production process, organic solvent consumption is few, and flavones species is enriched in product, uses in ultraviolet spectrophotometry detection wormwood extract flavones content as 21.3~27.5%.Blumea oil has anti-allergic effects, caused allergic reaction probability during use is advantageously reduced when content is relatively low, after adding transdermal agent azone, wormwood flavones is easy to directly act on color spot through skin, accelerate skin cell metabolism, play a part of desalinating color spot and prevent new color spot from generating.
Description
Technical field
The invention belongs to caused by cosmetics for special use field, more particularly to a kind of wormwood flavones nti-freckle gel.
Background technology
Wormwood also known as fragrant Chinese mugwort, argy wormwood, are composite family artemisia herbaceos perennial, are China's traditional Chinese medicines, are used as medicine with leaf, taste
It is pungent, bitter, it is warm-natured, it is slightly poisonous, enter liver, spleen, kidney channel, there are eliminating cold to stop pain, warming channel for arresting bleeding and other effects.Modern study shows that its is main
Chemical composition has volatile oil, eudesmane, triterpenes, flavonoids, also has many trace elements, has anti-bacteria and anti-virus, town of relievining asthma
Cough, eliminating the phlegm, antiallergy, calm immune and other effects.
Flavones is a kind of effective free radical scavenger, has antioxidation, existing using flavones as work(in the market
Imitate the health food of composition, the main health-care effect for publicizing beauty treatment and eliminating spot；The country has developed many Flavonoids extracts,
Pigmentation can be reduced, skin of moistening, such as ginkgo biloba p.e, bamboo extractive, licoflavone, isoflavones,
It is used in cosmetic field, flavones content is up to 5.5% in wormwood, has preferable Development volue.
A kind of Chinese invention patent " folium artemisiae argyi composition with whitening function and its should of Application No. 201610089128.9
With ", crushed after taking folium artemisiae argyi, raspberry, lucid asparagus, white parmelia saxatilis and Ligusticum wallichii cleaning, drying, cross 80~100 mesh sieves, merge coarse powder,
The ethanol that 8~12 times of amount volume fractions of medicinal material coarse powder weight are 60~80% is added, is soaked 6~12 hours, in 45~55 DEG C of temperature
Lower ultrasonic extraction 1~2 time, 45~60 minutes every time, supersonic frequency was 20~30kHz, filtering, merging filtrate, then toward filtrate
It is placed at 4 DEG C of refrigerator after refrigerating 24 hours and takes out after middle addition activated carbon 200g, stirring 10min, takes supernatant liquor to cross 80 mesh sieves,
Chinese medicine extract is obtained, relative density is 1.05~1.10 clear cream when Chinese medicine extract is concentrated under reduced pressure into 60 DEG C, dries, produces
Chinese medical extract.After simple alcohol extracting, the extract of acquisition, not purified, flavones content is low；And composition is complex, easily
The problems such as causing allergy.
The Chinese invention patent " spot-eliminating composition and its external preparation " of Application No. 201710433233.4, the nti-freckle
Composition is made up of P-Cymene, Lavender, Acotus illicioides essential oil and curcuma zedoary essential oil；P-Cymene, Lavender, fennel
The weight of white flag essential oil and curcuma zedoary essential oil ratio is 1：0.6~0.8：0.1~0.5：0.1~0.3.In P-Cymene containing toxicity into
Point, such as absinthol, be not suitable for long-term use.
The content of the invention
It is an object of the invention to provide a kind of a kind of easy to use, non-toxic, wormwood flavones nti-freckle with effect of dispelling spots
Gel.
The present invention takes following technical scheme：
A kind of wormwood flavones nti-freckle gel, it is characterised in that prepared by following weight part ratios：Wormwood extract 23~26%,
Water-solubleazone 4.5~5.5%, gel 0.8~1.2%, NMF 1~1.5%, surfactant 2~3%, help surface-active
Agent 0.5~1%, purified water polishing to 100%.
Described gel is at least one kind of in carbomer, xanthans.
Described NMF is at least one kind of in glycerine, coconut oil, olive oil.
Described surfactant is in Tween 80, polysorbate40, sorbester p18, span 20, polyoxyethylene -35- castor oil
It is at least one kind of.
Described cosurfactant is at least one kind of in absolute ethyl alcohol, 1,2- propane diols, polyethylene glycol 400.
Described wormwood extract is produced according to the following steps：
A) pretreatment of raw material：Fresh wormwood complete stool is gathered, withered blade and root is extractd, is dried after cleaning silt, shredded, used
Colloid mill is ground, and collects homogenate.
B) digest：The cellulose enzyme powder of homogenate weight 1%~3% is added, 50 DEG C of enzymolysis 24h, obtains enzymolysis liquid.
C) distill：By steam distillation heating extraction, flow back 4~5h, and distillate is Blumea oil crude extract, retains distillation
Liquid.
D) filter：Entered using 200 mesh nylon wires and distillate is filtered, retain filter liquor.
E) it is spray-dried for the first time：Filter liquor is spray-dried, obtains raw material meal.
F) alcohol extracting：60% ethanol solution, solid-liquid ratio 1 are added into raw material meal：20~1：25, stir, obtain alcohol
Extract.
G) filter：Alcohol extract is filtered using 45 μm of film, retains smoke filtrate.
H) ultrafiltration：Ultrafiltration removal of impurities is carried out to smoke filtrate using the modified cellulose film that molecular cut off is 30kD, add etc.
The ethanol solution of volume 60%, retain filter liquor, then molecular cut off 5kD modified cellulose film concentrates to filter liquor, adds
Isometric 60% ethanol solution, to stopping concentration during 1/2~2/3 that concentration volume is filtrate volume in step d), retain dense
Contracting liquid.
I) it is spray-dried：It is spray-dried using closed cycle spray drying machine, reclaims ethanol, is obtained wormwood flavones and carry
Take thing dry powder.
J) mix：Blumea oil is mixed with wormwood chromocor extract dry powder, mass ratio 0.03：1~0.05：1, i.e.,
For wormwood extract.
A kind of wormwood flavones nti-freckle gel is produced according to the following steps：
L) it is swelled：Gel is fully swelled with partial purification water.
M) homogeneous：By wormwood extract, water-solubleazone, gel, NMF, surfactant, cosurfactant,
Purified water is transferred in high speed homogenizer, 2500~2800r/min, homogeneous 15~20min, vacuum outgas, and filling is that wormwood is yellow
Ketone nti-freckle gel.
Compared with prior art, it is an advantage of the current invention that wormwood extract simple production process, organic solvent consumption
Few, flavones species is enriched in product, use in ultraviolet spectrophotometry detection wormwood extract flavones content for 21.3~
27.5%.Blumea oil has anti-allergic effects, and caused allergic reaction probability during use is advantageously reduced when content is relatively low,
After adding transdermal agent azone, wormwood flavones is easy to directly act on color spot through skin, accelerates skin cell metabolism, plays
Desalination color spot and the effect for preventing new color spot generation.
Embodiment
Following examples are used to illustrate the present invention, but are not limited to the scope of the present invention.
Embodiment 1
Purchase fresh wormwood herb 100kg, manual removal is withered blade, is cut root, is dried after cleaning silt, shredded, is used
Colloid mill is ground, and collects homogenate 93.5kg.50 DEG C, natural ph, 0.94kg cellulose enzyme powders are added, are stirred, digested
24h, steam distillation heating extraction is pressed to enzymolysis liquid, flow back 4h, and distillate is that Blumea oil slightly guides and support 0.9L.Use 200 mesh
Distillate after nylon net filter distillation, obtains filter liquor 39.67kg, raw material meal 9.41kg is obtained after spray drying, with 60%
Ethanol solution dissolving 188.2kg dissolving raw material meals, are stirred to abundant dissolving, obtain alcohol extract, entered using 45 μm of the film in aperture
Row filters, and retains smoke filtrate.Ultrafiltration removal of impurities is carried out to smoke filtrate using the modified cellulose film that molecular cut off is 30kD, added
60% isometric ethanol solution, retain filter liquor, then with molecular cut off 5kD modified cellulose film filter liquor is carried out dense
Contracting, isometric 60% ethanol solution is added, stop concentrating when to concentration volume be 20L, carried out using closed cycle spray drying machine
Spray drying, ethanol is reclaimed, obtain wormwood chromocor extract dry powder 2.16kg.0.06kg Blumea oils are taken to be carried with 2kg wormwood flavones
Take thing dry powder blend uniform, as wormwood extract 2.06kg.0.08kg Acritamer 940s are fully swelled using 1kg purified waters,
Add 2.06kg wormwood extracts, 0.45kg water-solubleazones, 0.09kg glycerine, 0.13kg Tween 80s, 0.04kg sorbester p18s,
In 0.03kg absolute ethyl alcohols, 0.02kg 1,2-PDs, 4.68kg purified waters input high speed homogenizer, 2500r/min is homogeneous
15min, vacuum outgas is filling, as wormwood flavones nti-freckle gel.
Embodiment 2
Purchase fresh wormwood herb 200kg, manual removal is withered blade, is cut root, is dried after cleaning silt, shredded, is used
Colloid mill is ground, and collects homogenate 189.6kg.50 DEG C, natural ph, 3.5kg cellulose enzyme powders are added, are stirred, digested
24h, steam distillation heating extraction is pressed to enzymolysis liquid, flow back 5h, and distillate is that Blumea oil slightly guides and support 1.61L.Use 200 mesh
Distillate after nylon net filter distillation, obtains filter liquor 83.52kg, and raw material meal 19.15kg is obtained after spray drying, uses
60% ethanol solution dissolving 385kg dissolving raw material meals, are stirred to abundant dissolving, obtain alcohol extract, entered using 45 μm of the film in aperture
Row filters, and retains smoke filtrate.Ultrafiltration removal of impurities is carried out to smoke filtrate using the modified cellulose film that molecular cut off is 30kD, added
60% isometric ethanol solution, retain filter liquor, then with molecular cut off 5kD modified cellulose film filter liquor is carried out dense
Contracting, isometric 60% ethanol solution is added, stop concentrating when to concentration volume be 43L, carried out using closed cycle spray drying machine
Spray drying, ethanol is reclaimed, obtain wormwood chromocor extract dry powder 5.17kg.0.23kg Blumea oils are taken to be carried with 5kg wormwood flavones
Take thing dry powder blend uniform, as wormwood extract 5.23kg.0.13kg xanthans and 0.1kg Acritamer 940s are fully swelled
In 5kg purified waters, add 5.23kg wormwood extracts, 1.09kg water-solubleazones, 0.23kg olive oil, 0.2kg polysorbate40s,
0.27kg span 20s, 0.08kg 1,2- propane diols, 0.06kg polyethylene glycol 400s, 8.13kg purified waters input high speed homogenizer
In, 2500r/min, homogeneous 15min, vacuum outgas is filling, as wormwood flavones nti-freckle gel.
Experimental example
Volunteer's case 216, wherein gently, in, each 72 of severe（Slightly：Color spot is filbert, accounts for face area below 30%；
Moderate：Color spot is yellowish-brown, accounts for face area below 50%, or filbert accounts for face area 30~50%；Severe：Color spot is black
Brown, filbert or yellowish-brown account for face area more than 50%）, 3 groups are equally divided into, control group is without wormwood brass extract
Gel.Application method：Just before going to bed after cleaning face, take the spot-removing ointment of the appropriate present invention to be uniformly applied to face, gently pat
Absorb；At spot print can dosage use, and gently massage 3~5 minutes, allow skin to fully absorb, experimental period 1 month, as a result see
Table 1.
Criterion of therapeutical effect：
（1）It is basic to cure：Naked eyes regard color spot area and disappeared more than 90%, and color disappears substantially, and 1 meter apart from invisible bright
Aobvious spot.
（2）There is positive effect：Naked eyes regard color spot area and disappeared more than 60%, and color is substantially thin out.
（3）Take a turn for the better：Naked eyes regard color spot area and disappeared more than 30%, and color is thin out.
（4）It is invalid：Naked eyes regard color spot area and disappeared less than 30%, color change unobvious.
Table 1
It can be seen that using effect of the present invention is preferable compared to the positive effect of control group, and slight color spot person's effective percentage highest, it is dispelled
Except effect is preferably also；Moderate color spot patient cure rate is relatively slight relatively low, but it is also higher close to half, cure rate to cure number；Weight
Although spending, color spot person's cure rate is minimum, and invalid number is still less.Illustrate, the present invention is preferable for the therapeutic effect of color spot.
Claims (4)
1. a kind of wormwood flavones nti-freckle gel, it is characterised in that prepared by following weight part ratios：
Wormwood extract 23~26%, water-solubleazone 4.5~5.5%, gel 0.8~1.2%, NMF 1~1.5%, surface
Activating agent 2~3%, cosurfactant 0.5~1%, purified water polishing to 100%.
A kind of 2. wormwood flavones nti-freckle gel according to claim 1, it is characterised in that：
Described gel is at least one kind of in carbomer, xanthans；Described NMF is in glycerine, coconut oil, olive oil
It is at least one kind of；Described surfactant is in Tween 80, polysorbate40, sorbester p18, span 20, polyoxyethylene -35- castor oil
It is at least one kind of；Described cosurfactant is at least one kind of in absolute ethyl alcohol, 1,2- propane diols, polyethylene glycol 400.
A kind of 3. wormwood flavones nti-freckle gel according to claim 1, it is characterised in that described wormwood extract press with
Lower step is produced：
A) pretreatment of raw material：Fresh wormwood complete stool is gathered, withered blade and root is extractd, is dried after cleaning silt, shredded, used
Colloid mill is ground, and collects homogenate；
B) digest：The cellulose enzyme powder of homogenate weight 1%~3% is added, 50 DEG C of enzymolysis 24h, obtains enzymolysis liquid；
C) distill：By steam distillation heating extraction, flow back 4~5h, and distillate is Blumea oil crude extract, retains distillate；
D) filter：Entered using 200 mesh nylon wires and distillate is filtered, retain filter liquor；
E) it is spray-dried for the first time：Filter liquor is spray-dried, obtains raw material meal；
F) alcohol extracting：60% ethanol solution, solid-liquid ratio 1 are added into raw material meal：20~1：25, stir, obtain alcohol extracting
Liquid；
G) filter：Alcohol extract is filtered using 45 μm of film, retains smoke filtrate；
H) ultrafiltration：Ultrafiltration removal of impurities is carried out to smoke filtrate using the modified cellulose film that molecular cut off is 30kD, added isometric
60% ethanol solution, retain filter liquor, then molecular cut off 5kD modified cellulose film concentrates to filter liquor, the body such as addition
60% ethanol solution of product, to stopping concentration during 1/2~2/3 that concentration volume is filtrate volume in step d), retain concentrate；
I) it is spray-dried：It is spray-dried using closed cycle spray drying machine, reclaims ethanol, obtains wormwood chromocor extract
Dry powder；
J) mix：Blumea oil is mixed with wormwood chromocor extract dry powder, mass ratio 0.03：1~0.05：1, as end
Careless extract.
4. a kind of wormwood flavones nti-freckle gel according to claim 1, it is characterised in that produced according to the following steps：
L) it is swelled：Gel is fully swelled with partial purification water；
M) homogeneous：By wormwood extract, water-solubleazone, gel, NMF, surfactant, cosurfactant, purifying
Water is transferred in high speed homogenizer, 2500~2800r/min, homogeneous 15~20min, vacuum outgas, and filling is that wormwood flavones is dispelled
Spot gel.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711151358.4A CN107744483A (en) | 2017-11-18 | 2017-11-18 | A kind of wormwood flavones nti-freckle gel |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711151358.4A CN107744483A (en) | 2017-11-18 | 2017-11-18 | A kind of wormwood flavones nti-freckle gel |
Publications (1)
| Publication Number | Publication Date |
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| CN107744483A true CN107744483A (en) | 2018-03-02 |
Family
ID=61252339
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| CN201711151358.4A Withdrawn CN107744483A (en) | 2017-11-18 | 2017-11-18 | A kind of wormwood flavones nti-freckle gel |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109316416A (en) * | 2018-09-06 | 2019-02-12 | 广州华玺生物科技有限公司 | A kind of Folium Artemisiae Argyi extract and its application in cosmetics |
| CN111449999A (en) * | 2020-04-03 | 2020-07-28 | 广州暨南生物医药研究开发基地有限公司 | A hand sanitizer containing folium Artemisiae Argyi extract, and its preparation method |
| CN113143815A (en) * | 2021-02-06 | 2021-07-23 | 澳宝化妆品（惠州）有限公司 | Folium Artemisiae Argyi extract, its preparation method, and composition and tear-off facial mask containing the same |
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| CN101700218A (en) * | 2009-11-26 | 2010-05-05 | 孙淑萍 | Skin whitening, moisturizing and nourishing gel and method for preparing same |
| CN104194917A (en) * | 2014-09-05 | 2014-12-10 | 南京泽朗生物科技有限公司 | Method for extracting folium artemisiae argyi essential oil |
| CN104922000A (en) * | 2015-06-29 | 2015-09-23 | 南阳市汇博生物技术有限公司 | Sunscreen repair gel and preparing method thereof |
| CN105943487A (en) * | 2016-06-21 | 2016-09-21 | 景金发 | Whitening and nourishing gel |
| CN105997648A (en) * | 2016-06-21 | 2016-10-12 | 江苏奇力康皮肤药业有限公司 | Skin protection gel containing natural extracts |
| CN106833895A (en) * | 2016-12-23 | 2017-06-13 | 湖南汉众农业发展有限公司 | A kind of extracting method of volatile argyi leaf oil |
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2017
- 2017-11-18 CN CN201711151358.4A patent/CN107744483A/en not_active Withdrawn
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101700218A (en) * | 2009-11-26 | 2010-05-05 | 孙淑萍 | Skin whitening, moisturizing and nourishing gel and method for preparing same |
| CN104194917A (en) * | 2014-09-05 | 2014-12-10 | 南京泽朗生物科技有限公司 | Method for extracting folium artemisiae argyi essential oil |
| CN104922000A (en) * | 2015-06-29 | 2015-09-23 | 南阳市汇博生物技术有限公司 | Sunscreen repair gel and preparing method thereof |
| CN105943487A (en) * | 2016-06-21 | 2016-09-21 | 景金发 | Whitening and nourishing gel |
| CN105997648A (en) * | 2016-06-21 | 2016-10-12 | 江苏奇力康皮肤药业有限公司 | Skin protection gel containing natural extracts |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109316416A (en) * | 2018-09-06 | 2019-02-12 | 广州华玺生物科技有限公司 | A kind of Folium Artemisiae Argyi extract and its application in cosmetics |
| CN111449999A (en) * | 2020-04-03 | 2020-07-28 | 广州暨南生物医药研究开发基地有限公司 | A hand sanitizer containing folium Artemisiae Argyi extract, and its preparation method |
| CN113143815A (en) * | 2021-02-06 | 2021-07-23 | 澳宝化妆品（惠州）有限公司 | Folium Artemisiae Argyi extract, its preparation method, and composition and tear-off facial mask containing the same |
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Application publication date: 20180302 |