CN103045150B - 水性聚氨酯胶粘剂及其制备方法 - Google Patents
水性聚氨酯胶粘剂及其制备方法 Download PDFInfo
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- CN103045150B CN103045150B CN201310015021.6A CN201310015021A CN103045150B CN 103045150 B CN103045150 B CN 103045150B CN 201310015021 A CN201310015021 A CN 201310015021A CN 103045150 B CN103045150 B CN 103045150B
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- 229920002635 polyurethane Polymers 0.000 title claims abstract description 82
- 239000004814 polyurethane Substances 0.000 title claims abstract description 82
- 230000001070 adhesive effect Effects 0.000 title claims abstract description 60
- 239000000853 adhesive Substances 0.000 title claims abstract description 59
- 238000002360 preparation method Methods 0.000 title claims description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 133
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 70
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 45
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 38
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 claims abstract description 25
- UEEJHVSXFDXPFK-UHFFFAOYSA-N N-dimethylaminoethanol Chemical compound CN(C)CCO UEEJHVSXFDXPFK-UHFFFAOYSA-N 0.000 claims abstract description 23
- 229960002887 deanol Drugs 0.000 claims abstract description 23
- 239000012972 dimethylethanolamine Substances 0.000 claims abstract description 23
- 239000003795 chemical substances by application Substances 0.000 claims description 64
- 238000003756 stirring Methods 0.000 claims description 42
- 238000006243 chemical reaction Methods 0.000 claims description 40
- 239000000463 material Substances 0.000 claims description 32
- 239000013530 defoamer Substances 0.000 claims description 25
- PTBDIHRZYDMNKB-UHFFFAOYSA-N 2,2-Bis(hydroxymethyl)propionic acid Chemical compound OCC(C)(CO)C(O)=O PTBDIHRZYDMNKB-UHFFFAOYSA-N 0.000 claims description 21
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 claims description 21
- 229920003009 polyurethane dispersion Polymers 0.000 claims description 21
- 239000002562 thickening agent Substances 0.000 claims description 21
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 claims description 18
- 239000002904 solvent Substances 0.000 claims description 18
- MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 claims description 16
- 239000004902 Softening Agent Substances 0.000 claims description 16
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 claims description 16
- -1 vulcabond Chemical compound 0.000 claims description 14
- 239000003112 inhibitor Substances 0.000 claims description 12
- 230000003647 oxidation Effects 0.000 claims description 12
- 238000007254 oxidation reaction Methods 0.000 claims description 12
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims description 10
- 238000006116 polymerization reaction Methods 0.000 claims description 9
- 230000035484 reaction time Effects 0.000 claims description 9
- KSBAEPSJVUENNK-UHFFFAOYSA-L tin(ii) 2-ethylhexanoate Chemical group [Sn+2].CCCCC(CC)C([O-])=O.CCCCC(CC)C([O-])=O KSBAEPSJVUENNK-UHFFFAOYSA-L 0.000 claims description 8
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical group CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 7
- 239000005057 Hexamethylene diisocyanate Substances 0.000 claims description 6
- 239000005058 Isophorone diisocyanate Substances 0.000 claims description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-M acrylate group Chemical group C(C=C)(=O)[O-] NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 6
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- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 claims description 6
- 235000019260 propionic acid Nutrition 0.000 claims description 5
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims description 5
- 230000008719 thickening Effects 0.000 claims description 4
- KXBFLNPZHXDQLV-UHFFFAOYSA-N [cyclohexyl(diisocyanato)methyl]cyclohexane Chemical compound C1CCCCC1C(N=C=O)(N=C=O)C1CCCCC1 KXBFLNPZHXDQLV-UHFFFAOYSA-N 0.000 claims description 3
- 125000002462 isocyano group Chemical group *[N+]#[C-] 0.000 claims description 3
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- 229920000728 polyester Polymers 0.000 abstract description 14
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- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 2
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 abstract 1
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- 238000000425 proton nuclear magnetic resonance spectrum Methods 0.000 description 6
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 description 5
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 4
- ODFJASQFYDKXEE-UHFFFAOYSA-N 3,3,3-trihydroxy-2-methylpropanoic acid Chemical compound OC(O)(O)C(C(=O)O)C ODFJASQFYDKXEE-UHFFFAOYSA-N 0.000 description 3
- 238000010276 construction Methods 0.000 description 3
- 150000002009 diols Chemical class 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
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- DGADNPLBVRLJGD-UHFFFAOYSA-N 2,3-dihydroxy-2-methylpropanoic acid Chemical compound OCC(O)(C)C(O)=O DGADNPLBVRLJGD-UHFFFAOYSA-N 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- WNLRTRBMVRJNCN-UHFFFAOYSA-L adipate(2-) Chemical compound [O-]C(=O)CCCCC([O-])=O WNLRTRBMVRJNCN-UHFFFAOYSA-L 0.000 description 1
- 125000003158 alcohol group Chemical group 0.000 description 1
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- 150000002148 esters Chemical class 0.000 description 1
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- Polyurethanes Or Polyureas (AREA)
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Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103409098B (zh) * | 2013-07-15 | 2015-01-28 | 长春市三化实业有限责任公司 | 木质素改性阳离子水性聚氨酯胶粘剂及其制备方法 |
CN103409100B (zh) * | 2013-08-16 | 2015-04-22 | 长春市三化实业有限责任公司 | 环氧树脂改性的水性聚氨酯胶粘剂及其制备方法 |
CN103483539B (zh) * | 2013-08-27 | 2015-09-16 | 中国科学院长春应用化学研究所 | 聚(碳酸酯-醚)型水性聚氨酯、水性聚氨酯胶粘剂及其制备方法 |
CN103509514B (zh) * | 2013-09-06 | 2015-11-25 | 繁昌县倍思生产力促进中心有限公司 | 一种快速固化反应型热熔胶 |
CN104004486B (zh) * | 2014-05-08 | 2015-08-05 | 中国科学院长春应用化学研究所 | 汽车内饰水性聚氨酯胶粘剂及其制备方法 |
CN103980457B (zh) * | 2014-06-11 | 2017-01-04 | 中国科学院长春应用化学研究所 | 一种水性聚氨酯、其制备方法和水性聚氨酯胶粘剂 |
JP6238850B2 (ja) * | 2014-07-17 | 2017-11-29 | 日本化薬株式会社 | 液晶シール剤及びそれを用いた液晶表示セル |
CN104974541A (zh) * | 2015-07-06 | 2015-10-14 | 兰州科天环保节能科技有限公司 | 一种含有秸秆的人造板及其制备方法 |
CN105968295B (zh) * | 2016-05-26 | 2019-02-12 | 湖南本安亚大新材料有限公司 | 一种水性聚氨酯树脂、水性聚氨酯胶粘剂及其制备方法 |
CN106750118A (zh) * | 2016-11-28 | 2017-05-31 | 中国科学院长春应用化学研究所 | 阳离子水性聚氨酯树脂、其制备方法与水性聚氨酯胶粘剂 |
CN106750175A (zh) * | 2017-01-18 | 2017-05-31 | 中国科学院长春应用化学研究所 | 一种阻燃型水性聚氨酯及其制备方法、胶粘剂及其制备方法 |
CN107841875A (zh) * | 2017-11-29 | 2018-03-27 | 苏州润弘贸易有限公司 | 水性聚氨酯浆料 |
CN111501127B (zh) * | 2020-05-22 | 2021-08-17 | 中国科学院长春应用化学研究所 | 一种二氧化碳基聚氨酯纤维及其制备方法 |
CN111534215B (zh) * | 2020-05-22 | 2021-07-02 | 中国科学院长春应用化学研究所 | 用于汽车保险杠的水性涂料及其制备方法 |
CN111823745A (zh) * | 2020-05-26 | 2020-10-27 | 湖南天琪智慧印刷有限公司 | 对机械浆具有耐受性的热敏纸及其制作方法 |
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TW201005053A (en) * | 2008-04-28 | 2010-02-01 | Bayer Materialscience Ag | Block-resistant, radiation-curable coating systems based on high molecular mass, aqueous polyurethane dispersions |
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DE102005019430A1 (de) * | 2005-04-25 | 2006-10-26 | Bayer Materialscience Ag | N-Methylpyrrolidon-freie Polyurethan-Dispersionen auf Basis von Dimethylolpropionsäure |
DE102010019504A1 (de) * | 2010-05-06 | 2011-11-10 | Bayer Materialscience Ag | Polyisocyanatprepolymere und deren Verwendung |
CN102102005B (zh) * | 2010-12-13 | 2013-06-05 | 嘉兴禾欣化学工业有限公司 | 环保型水性聚氨酯胶粘剂的制备方法 |
CN102093836B (zh) * | 2010-12-31 | 2013-06-05 | 广东达志环保科技股份有限公司 | 一种聚碳酸亚乙酯型聚氨酯水性粘合剂 |
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TW201005053A (en) * | 2008-04-28 | 2010-02-01 | Bayer Materialscience Ag | Block-resistant, radiation-curable coating systems based on high molecular mass, aqueous polyurethane dispersions |
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