CN103031053A - UV-cured peelable blue gel for temporary protection of touch screen and preparation method thereof - Google Patents
UV-cured peelable blue gel for temporary protection of touch screen and preparation method thereof Download PDFInfo
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- CN103031053A CN103031053A CN2013100032686A CN201310003268A CN103031053A CN 103031053 A CN103031053 A CN 103031053A CN 2013100032686 A CN2013100032686 A CN 2013100032686A CN 201310003268 A CN201310003268 A CN 201310003268A CN 103031053 A CN103031053 A CN 103031053A
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Abstract
The invention provides a UV-cured peelable blue gel for temporary protection of a touch screen and a preparation method thereof. The UV-cured peelable blue gel comprises the following components of 50-70 parts of modified acrylate resin, 20-30 parts of acrylate monomer, 1.0-5.0 parts of light curing agent, 0.1-1.0 part of thixotropic agent, 0.1-5.0 parts of auxiliary and 0.1-1.0 part of pigment; and the preparation method comprises the following steps of: accurately weighing various raw materials according to a formula ratio; firstly adding the modified acrylate resin, the acrylate monomer, the light curing agent, the auxiliary and the pigment to a reaction kettle in sequence and then stirring these materials in the reaction kettle; after these materials are uniformly stirred, adding the thixotropic agent to these materials; and uniformly dispersing an obtained mixture to discharge out a material. The UV-cured peelable blue gel provided by the invention is a non-solvent and a system containing no phthalate substance and is much safer and more environment-friendly. Through the adoption of a UV curing system, the film curing and forming speed is high and the production efficiency of the touch screen is greatly increased.
Description
Technical field
The present invention relates to a kind of UV and solidify peelable blue glue and preparation method thereof, this peelable blue glue is mainly used in the temporary protection in the process for manufacturing touch panel.
Background technology
[0002] along with the developing rapidly of information technology and plane technique of display, the application of touch-screen is more and more general.Large Referral information system to the public place, little of PC, panel computer, mobile phone, touch-screen and our life are closely bound up.In the production process of touch-screen, need to carry out repeatedly temporary protection to touch-screen glass by using peelable blue glue.Traditional peelable blue glue contains the interference human endocrine, affects the phthalic ester plasticizer of human body reproductive performance, is restricted in application.And the technique of the peelable blue adhesive curing film forming of tradition is generally 120 ℃-150 ℃, 20min-60min, owing in the production process of touch-screen, need repeatedly temporary protection, thereby consuming time longer in the process of peelable blue adhesive curing film forming, affect production efficiency.
The system that adopts UV to solidify can fundamentally address the above problem, UV solidifies peelable blue glue has been stopped the phthalate material from composition use, more environmental protection, nontoxic, its film-forming time is short, greatly improved the efficient that touch-screen is produced with interior fully film-forming in 30 seconds.
Summary of the invention
The object of the present invention is to provide a kind of UV for the touch-screen temporary protection to solidify peelable blue glue, this peelable blue glue does not contain the phthalate material, more environmental protection, and the mode that UV solidifies can improve the efficient that touch-screen is produced.
In order to realize purpose of the present invention, propose a kind of touch-screen temporary protection and solidify peelable blue glue with UV, it is composed as follows that described UV solidifies peelable blue glue prescription:
50 ~ 70 parts of modified acrylic ester resins
20 ~ 30 parts of acrylate monomers
Light curing agent 1.0-5.0 part
Thixotropic agent 0.1-1.0 part
Auxiliary agent 0.1-5.0 part
Pigment 0.1-1.0 part.
Wherein, described modified acrylic ester resin is one or more in polyurethane-modified polyacrylate resin, aliphatic polyurethane modified acrylic ester resin, epoxy modification acrylate resin, Silicone-Modified Acrylate Resin, organic fluorine modified acrylic ester resin, polyester modification acrylic resin and the polyether-modified acrylate resin;
Described acrylate monomer is one or more in (methyl) methyl acrylate, (methyl) Hydroxyethyl acrylate, (methyl) Propylene glycol monoacrylate, (methyl) vinylformic acid tetrahydrofuran ester, 2-benzene oxygen ethyl-methyl acrylate, (methyl) isobornyl acrylate, (methyl) n-butyl acrylate, (methyl) lauryl acrylate, Ethylene glycol dimethacrylate, ethoxyquin double A diacrylate and the 1,4 butanediol diacrylate;
Described light curing agent is one or more in bitter almond oil camphor, ethoxybenzoin, benzil ketals, benzophenone, methyl o-benzoylbenzoate, 2-isopropyl thioxanthone, sulfonic group thioxanthone and the thiophenyl benzophenone;
Described thixotropic agent is one or more in fumed silica, precipitated silica, organobentonite, asbestos, kaolin and the attapulgite;
Described auxiliary agent is flow agent or defoamer;
Described pigment is barba hispanica, ultramarine blue, cobalt blue or phthalocyanine blue.
The present invention also proposes two kinds of UV, and to solidify the concrete prescription of peelable blue glue composed as follows:
Prescription 1
30 parts of polyurethane-modified polyacrylate resins
40 parts of epoxy modification acrylate resins
23 parts of isobornyl acrylate
3.0 parts of benzophenone
1.0 parts of flow agents
1.0 parts of defoamers
1.0 parts of organobentonites
1.0 parts of phthalocyanine blues
Prescription 2
30 parts of polyurethane-modified polyacrylate resins
20 parts of epoxy modification acrylate resins
20 parts of Silicone-Modified Acrylate Resins
23 parts of isobornyl methacrylates
3.0 parts of benzophenone
1.0 parts of flow agents
1.0 parts of defoamers
1.0 parts of precipitated silicas
1.0 parts of phthalocyanine blues
The present invention also proposes a kind of touch-screen temporary protection: accurately take by weighing various raw materials by formula rate; first modified acrylic ester resin, acrylate monomer, light curing agent, auxiliary agent, pigment are added in the reactor successively and stir; after stirring; add thixotropic agent, rear discharging is uniformly dispersed.
Advantage of the present invention:
1. non-solvent and do not contain phthalate substance system, more safety and environmental protection.
2.UV curing system film-forming speed is fast, greatly improves the efficient that touch-screen is produced.
Embodiment
For making the purpose, technical solutions and advantages of the present invention clearer, below in conjunction with specific embodiment, the present invention is described in more detail.
Embodiment 1
30 parts of polyurethane-modified polyacrylate resins
40 parts of epoxy modification acrylate resins
23 parts of isobornyl acrylate
3.0 parts of benzophenone
1.0 parts of flow agents
1.0 parts of defoamers
1.0 parts of organobentonites
1.0 parts of phthalocyanine blues
The preparation method:
Accurately take by weighing various raw materials by formula rate, first polyurethane-modified polyacrylate resin, epoxy modification acrylate resin, isobornyl acrylate, benzophenone, flow agent, defoamer, phthalocyanine blue are added in the reactor successively and stir, after stirring, add organobentonite, rear discharging is uniformly dispersed.
Embodiment 2
30 parts of polyurethane-modified polyacrylate resins
20 parts of epoxy modification acrylate resins
20 parts of Silicone-Modified Acrylate Resins
23 parts of isobornyl methacrylates
3.0 parts of benzophenone
1.0 parts of flow agents
1.0 parts of defoamers
1.0 parts of precipitated silicas
1.0 parts of phthalocyanine blues
The preparation method:
Accurately take by weighing various raw materials by formula rate, first polyurethane-modified polyacrylate resin, epoxy modification acrylate resin, Silicone-Modified Acrylate Resin, isobornyl methacrylate, benzophenone, flow agent, defoamer, phthalocyanine blue are added in the reactor successively and stir, after stirring, add precipitated silica, rear discharging is uniformly dispersed.
The performance test results after the listed embodiment of table 1 and the curing thereof.Test result shows: peelable blue glue of the present invention has good storage stability, excellent Technological adaptability, good rippability and insulativity, can satisfy the processing requirement that touch-screen is produced temporary protection comprehensively.
Table 1
Peelable blue glue of the present invention solves following problem:
1, environmental issue
The peelable blue glue of tradition contains phthalic ester plasticizer.Studies show that, but the phthalic ester disturbance endocrine makes the minimizing of mankind spermatozoon quantity, low, the paramophia of motor capacity, serious also can cause necrospermia and carcinoma of testis, is " arch-criminal " who causes the male genetic problem.Various countries launch respectively the use of such material of regulation limitations.UV solidifies the use that peelable blue glue has been stopped the phthalate material from composition among the present invention, and more environmental protection is nontoxic.
2, touch-screen production efficiency problem
The technique of the peelable blue adhesive curing film forming of tradition is generally 120 ℃-150 ℃, 20min-60min, owing in the production process of touch-screen, need repeatedly temporary protection, thereby consuming time longer in the process of peelable blue adhesive curing film forming, affect its production efficiency.It is short that UV solidifies peelable blue adhesive curing film formation time among the present invention, and 30s has improved the efficient that touch-screen is produced greatly with interior fully film-forming.
According to the above results, this peelable blue glue satisfies the manufacturing technique requirent of touch-screen fully, more environmental protection, and can improve the production efficiency of touch-screen.
With preferred embodiment openly as above they are not to limit the present invention although the present invention is own, and the content that protection scope of the present invention should be defined with the application's claim protection domain is as the criterion.Anyly have the knack of the art person, without departing from the spirit and scope of the present invention, various variations of doing or be equal to replacement all should belong to protection scope of the present invention.
Claims (5)
1. a touch-screen temporary protection solidifies peelable blue glue with UV, it is characterized in that: it is composed as follows that described UV solidifies peelable blue glue prescription:
50 ~ 70 parts of modified acrylic ester resins
20 ~ 30 parts of acrylate monomers
Light curing agent 1.0-5.0 part
Thixotropic agent 0.1-1.0 part
Auxiliary agent 0.1-5.0 part
Pigment 0.1-1.0 part.
2. UV according to claim 1 solidifies peelable blue glue, it is characterized in that:
Described modified acrylic ester resin is one or more in polyurethane-modified polyacrylate resin, aliphatic polyurethane modified acrylic ester resin, epoxy modification acrylate resin, Silicone-Modified Acrylate Resin, organic fluorine modified acrylic ester resin, polyester modification acrylic resin and the polyether-modified acrylate resin;
Described acrylate monomer is one or more in (methyl) methyl acrylate, (methyl) Hydroxyethyl acrylate, (methyl) Propylene glycol monoacrylate, (methyl) vinylformic acid tetrahydrofuran ester, 2-benzene oxygen ethyl-methyl acrylate, (methyl) isobornyl acrylate, (methyl) n-butyl acrylate, (methyl) lauryl acrylate, Ethylene glycol dimethacrylate, ethoxyquin double A diacrylate and the 1,4 butanediol diacrylate;
Described light curing agent is one or more in bitter almond oil camphor, ethoxybenzoin, benzil ketals, benzophenone, methyl o-benzoylbenzoate, 2-isopropyl thioxanthone, sulfonic group thioxanthone and the thiophenyl benzophenone;
Described thixotropic agent is one or more in fumed silica, precipitated silica, organobentonite, asbestos, kaolin and the attapulgite;
Described auxiliary agent is flow agent or defoamer;
Described pigment is barba hispanica, ultramarine blue, cobalt blue or phthalocyanine blue.
3. UV according to claim 2 solidifies peelable blue glue, it is characterized in that:
It is composed as follows that described UV solidifies peelable blue glue prescription:
30 parts of polyurethane-modified polyacrylate resins
40 parts of epoxy modification acrylate resins
23 parts of isobornyl acrylate
3.0 parts of benzophenone
1.0 parts of flow agents
1.0 parts of defoamers
1.0 parts of organobentonites
1.0 parts of phthalocyanine blues.
4. UV according to claim 2 solidifies peelable blue glue, it is characterized in that:
It is composed as follows that described UV solidifies peelable blue glue prescription:
30 parts of polyurethane-modified polyacrylate resins
20 parts of epoxy modification acrylate resins
20 parts of Silicone-Modified Acrylate Resins
23 parts of isobornyl methacrylates
3.0 parts of benzophenone
1.0 parts of flow agents
1.0 parts of defoamers
1.0 parts of precipitated silicas
1.0 parts of phthalocyanine blues.
5. the touch-screen temporary protection solidifies peelable blue glue with UV preparation method; it is characterized in that: described preparation method is: accurately take by weighing various raw materials by formula rate; first modified acrylic ester resin, acrylate monomer, light curing agent, auxiliary agent, pigment are added in the reactor successively and stir; after stirring; add thixotropic agent, rear discharging is uniformly dispersed.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310003268.6A CN103031053B (en) | 2013-01-06 | 2013-01-06 | Touch-screen temporary protection UV solidifies peelable blue gel and preparation method thereof |
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| CN201310003268.6A CN103031053B (en) | 2013-01-06 | 2013-01-06 | Touch-screen temporary protection UV solidifies peelable blue gel and preparation method thereof |
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| CN103031053A true CN103031053A (en) | 2013-04-10 |
| CN103031053B CN103031053B (en) | 2015-07-29 |
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| CN103421459A (en) * | 2013-09-04 | 2013-12-04 | 北京海斯迪克新材料有限公司 | UV solidified generality laminated adhesive suitable for thin film spraying technology |
| CN103421400A (en) * | 2013-08-30 | 2013-12-04 | 东莞市平波电子有限公司 | Touch screen UV curing peelable blue gel and preparing method thereof |
| CN103421418A (en) * | 2013-07-25 | 2013-12-04 | 吴江龙硕金属制品有限公司 | Plastic surface photo curable coating |
| CN103497728A (en) * | 2013-10-18 | 2014-01-08 | 北京海斯迪克新材料有限公司 | Room-temperature-storage type acrylate underfill adhesive and preparation method thereof |
| CN103965779A (en) * | 2014-04-14 | 2014-08-06 | 江苏嘉娜泰有机硅有限公司 | Temporary protection type elastic peelable glue and preparation method thereof |
| CN104231996A (en) * | 2014-09-22 | 2014-12-24 | 北京海斯迪克新材料有限公司 | LOCA (liquid optical clear adhesive) for full-attached module and preparation method of LOCA |
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| CN104710890A (en) * | 2015-03-05 | 2015-06-17 | 深圳市格莱特印刷材料有限公司 | Peelable protective ink and preparation method thereof |
| CN104710882A (en) * | 2015-03-05 | 2015-06-17 | 深圳市格莱特印刷材料有限公司 | Peelable blue glue and preparation method thereof |
| CN105176448A (en) * | 2015-07-24 | 2015-12-23 | 中山市伯伦克专用化学产品有限公司 | Protective elastic peelable blue glue and preparation method therefor |
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| CN105176224A (en) * | 2015-07-24 | 2015-12-23 | 中山市伯伦克专用化学产品有限公司 | Acid and alkali-resistant peelable blue glue |
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| CN105462482A (en) * | 2016-01-08 | 2016-04-06 | 佛山市顺德区百锐新电子材料有限公司 | Protecting adhesive capable of covering silver wires for touch screen and preparation method of adhesive |
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| CN102786839A (en) * | 2012-07-31 | 2012-11-21 | 佛山市三求电子材料有限公司 | Glass protecting ink and preparation method thereof |
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| CN103421418A (en) * | 2013-07-25 | 2013-12-04 | 吴江龙硕金属制品有限公司 | Plastic surface photo curable coating |
| CN103421400A (en) * | 2013-08-30 | 2013-12-04 | 东莞市平波电子有限公司 | Touch screen UV curing peelable blue gel and preparing method thereof |
| CN103421459B (en) * | 2013-09-04 | 2015-12-09 | 北京海斯迪克新材料有限公司 | A kind of UV of applicable thin film coatings technique solidifies conformal coating |
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