CN102740968B - 制备钛沸石催化剂的方法 - Google Patents

制备钛沸石催化剂的方法 Download PDF

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Publication number
CN102740968B
CN102740968B CN201080062435.9A CN201080062435A CN102740968B CN 102740968 B CN102740968 B CN 102740968B CN 201080062435 A CN201080062435 A CN 201080062435A CN 102740968 B CN102740968 B CN 102740968B
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CN
China
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catalyst
titanium zeolite
weight
carbonaceous material
hydrocarbon
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English (en)
Chinese (zh)
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CN102740968A (zh
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U·穆勒
P·鲁道夫
G·克鲁格
R·申克
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BASF SE
Dow Chemical Co
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BASF SE
Dow Chemical Co
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/063—Titanium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/90—Regeneration or reactivation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/082—Decomposition and pyrolysis
    • B01J37/084—Decomposition of carbon-containing compounds into carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/42—Addition of matrix or binder particles

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Catalysts (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201080062435.9A 2009-11-27 2010-11-23 制备钛沸石催化剂的方法 Active CN102740968B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US26473709P 2009-11-27 2009-11-27
US61/264,737 2009-11-27
PCT/EP2010/067987 WO2011064191A1 (en) 2009-11-27 2010-11-23 Process for the preparation of a titanium zeolite catalyst

Publications (2)

Publication Number Publication Date
CN102740968A CN102740968A (zh) 2012-10-17
CN102740968B true CN102740968B (zh) 2015-07-01

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US (1) US9302257B2 (enExample)
EP (1) EP2504098B1 (enExample)
JP (1) JP5933445B2 (enExample)
KR (1) KR101844084B1 (enExample)
CN (1) CN102740968B (enExample)
BR (1) BR112012012634A2 (enExample)
ES (1) ES2596223T3 (enExample)
MX (1) MX339546B (enExample)
MY (1) MY160594A (enExample)
RU (1) RU2561100C2 (enExample)
SG (1) SG10201407829TA (enExample)
WO (1) WO2011064191A1 (enExample)
ZA (1) ZA201204699B (enExample)

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MY182905A (en) * 2013-02-05 2021-02-05 Basf Se Process for preparing a titanium-containing zeolitic material having an mww framework structure
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MY182811A (en) 2013-07-24 2021-02-05 Basf Se Regeneration of a titanium containing zeolite
US10232359B2 (en) 2013-08-30 2019-03-19 Süd-Chemie India Pvt Ltd. Abbreviated process to custom-make titanium silicate based catalysts with variegated physico-chemical properties
CN104512904B (zh) * 2013-09-29 2016-08-10 中国石油化工股份有限公司 一种制备介孔钛硅材料的方法
HUE045892T2 (hu) * 2013-10-02 2020-01-28 Solvay Eljárás tisztított vizes hidrogénperoxid-oldat elõállítására
SG10201803332YA (en) * 2013-10-23 2018-06-28 Basf Se Molding for a hydrophobic zeolitic material and process for its production
KR101799718B1 (ko) * 2014-01-22 2017-11-20 라이온델 케미칼 테크놀로지, 엘.피. 에폭시화 촉매의 제조 방법
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US10850265B2 (en) 2014-06-18 2020-12-01 Basf Corporation Molecular sieve catalyst compositions, catalytic composites, systems, and methods
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CN107548390B (zh) 2015-04-28 2020-11-10 赢创运营有限公司 丙烯环氧化的方法
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CN110072618B (zh) 2016-12-20 2022-12-30 巴斯夫欧洲公司 制备包含具有mww骨架类型的含钛沸石材料的可挤出组合物的方法
EP3438101A1 (en) 2017-08-01 2019-02-06 Evonik Degussa GmbH Process for the epoxidation of propene
RU2672357C1 (ru) * 2017-08-08 2018-11-14 Публичное акционерное общество "Нефтяная компания "Роснефть" (ПАО "НК "Роснефть") Катализатор для получения синтетических углеводородов с высоким содержанием изоалканов и способ его получения
JP6947011B2 (ja) * 2017-12-25 2021-10-13 東ソー株式会社 ゼオライト−シリカ成形体
EP3766574A4 (en) * 2018-03-15 2021-05-19 Sumitomo Chemical Company Limited MANUFACTURING METHOD FOR A TITANIUM-CONTAINING SILICOXIDE SHAPED BODY AND TITANIUM-CONTAINING SILICON OXIDE SHAPED BODY
BR112021005279A2 (pt) * 2018-10-09 2021-06-15 Basf Se moldagem, processo para preparar uma moldagem, e, uso de uma moldagem
JP7574216B2 (ja) * 2019-04-29 2024-10-28 ビーエーエスエフ ソシエタス・ヨーロピア 骨格型ｍｆｉを有するゼオライト材料を含む成形品
WO2020241052A1 (ja) * 2019-05-29 2020-12-03 住友化学株式会社 チタン含有珪素酸化物の製造方法、エポキシドの製造方法、及びチタン含有珪素酸化物
US20220401933A1 (en) 2019-11-20 2022-12-22 Basf Se Zeolite catalyzed process for the amination of propylene oxide
JP2021087901A (ja) * 2019-12-02 2021-06-10 栗田工業株式会社 水処理用浄化剤の製造方法
JP7400421B2 (ja) * 2019-12-06 2023-12-19 栗田工業株式会社 吸着剤、その製造方法及び水処理方法
KR20220157483A (ko) * 2020-03-23 2022-11-29 바스프 에스이 Si, O 및 Ti를 포함하는 프레임워크 구조를 갖는 제올라이트 물질
US20230303765A1 (en) 2020-08-03 2023-09-28 Basf Se A polyester molding having a low outgassing of volatile organic compounds
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Also Published As

Publication number Publication date
US9302257B2 (en) 2016-04-05
ZA201204699B (en) 2013-09-25
RU2561100C2 (ru) 2015-08-20
CN102740968A (zh) 2012-10-17
KR20120087180A (ko) 2012-08-06
EP2504098B1 (en) 2016-07-06
BR112012012634A2 (pt) 2020-09-15
MX339546B (es) 2016-05-30
JP2013512082A (ja) 2013-04-11
MX2012005845A (es) 2012-08-01
ES2596223T3 (es) 2017-01-05
JP5933445B2 (ja) 2016-06-08
US20110130579A1 (en) 2011-06-02
KR101844084B1 (ko) 2018-03-30
SG10201407829TA (en) 2015-01-29
EP2504098A1 (en) 2012-10-03
WO2011064191A1 (en) 2011-06-03
RU2012126602A (ru) 2014-01-10
MY160594A (en) 2017-03-15

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