CN102574779B - 吡唑羧酸酰胺的制备工艺 - Google Patents
吡唑羧酸酰胺的制备工艺 Download PDFInfo
- Publication number
- CN102574779B CN102574779B CN201080034393.8A CN201080034393A CN102574779B CN 102574779 B CN102574779 B CN 102574779B CN 201080034393 A CN201080034393 A CN 201080034393A CN 102574779 B CN102574779 B CN 102574779B
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- 0 CC(*(C)C)c1cccc([C@@]2C=C3)c1C3C2=C(*)*=C Chemical compound CC(*(C)C)c1cccc([C@@]2C=C3)c1C3C2=C(*)*=C 0.000 description 1
- BMHUFYBSDMWTOX-UHFFFAOYSA-N ClC(Cl)=C1C=CC=C1 Chemical compound ClC(Cl)=C1C=CC=C1 BMHUFYBSDMWTOX-UHFFFAOYSA-N 0.000 description 1
- JBEVXPMICLRQGS-UHFFFAOYSA-N OC(CC1)C(C(CCC23)C2=C(Cl)Cl)C3C1=O Chemical compound OC(CC1)C(C(CCC23)C2=C(Cl)Cl)C3C1=O JBEVXPMICLRQGS-UHFFFAOYSA-N 0.000 description 1
- ZZRIKLZFKKNHSS-UHFFFAOYSA-N [O-][N+](c1cccc(C2CC3)c1C3C2=O)=O Chemical compound [O-][N+](c1cccc(C2CC3)c1C3C2=O)=O ZZRIKLZFKKNHSS-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/32—Oximes
- C07C251/34—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
- C07C251/44—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups being part of a ring other than a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/62—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by hydrogenation of carbon-to-carbon double or triple bonds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/65—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by splitting-off hydrogen atoms or functional groups; by hydrogenolysis of functional groups
- C07C45/66—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by splitting-off hydrogen atoms or functional groups; by hydrogenolysis of functional groups by dehydration
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
- C07C45/68—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
- C07C45/69—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by addition to carbon-to-carbon double or triple bonds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
- C07C49/687—Unsaturated compounds containing a keto groups being part of a ring containing halogen
- C07C49/693—Unsaturated compounds containing a keto groups being part of a ring containing halogen polycyclic
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
- C07C49/703—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups
- C07C49/743—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups having unsaturation outside the rings, e.g. humulones, lupulones
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/42—One nitrogen atom
- C07D251/44—One nitrogen atom with halogen atoms attached to the two other ring carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2603/00—Systems containing at least three condensed rings
- C07C2603/56—Ring systems containing bridged rings
- C07C2603/58—Ring systems containing bridged rings containing three rings
- C07C2603/60—Ring systems containing bridged rings containing three rings containing at least one ring with less than six members
- C07C2603/66—Ring systems containing bridged rings containing three rings containing at least one ring with less than six members containing five-membered rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09167363 | 2009-08-06 | ||
| EP09167363.2 | 2009-08-06 | ||
| EP09169501.5 | 2009-09-04 | ||
| EP09169501 | 2009-09-04 | ||
| PCT/EP2010/059703 WO2011015416A1 (en) | 2009-08-06 | 2010-07-07 | Process for the preparation of pyrazole carboxylic acid amides |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102574779A CN102574779A (zh) | 2012-07-11 |
| CN102574779B true CN102574779B (zh) | 2014-10-15 |
Family
ID=42670451
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201080034393.8A Active CN102574779B (zh) | 2009-08-06 | 2010-07-07 | 吡唑羧酸酰胺的制备工艺 |
Country Status (28)
| Country | Link |
|---|---|
| US (1) | US8507694B2 (enExample) |
| EP (1) | EP2462108B1 (enExample) |
| JP (1) | JP5667186B2 (enExample) |
| KR (1) | KR101712083B1 (enExample) |
| CN (1) | CN102574779B (enExample) |
| AR (1) | AR077707A1 (enExample) |
| AU (1) | AU2010280923B2 (enExample) |
| BR (1) | BR112012002641B1 (enExample) |
| CA (1) | CA2770144C (enExample) |
| CL (1) | CL2012000272A1 (enExample) |
| CO (1) | CO6430457A2 (enExample) |
| CR (1) | CR20120056A (enExample) |
| DK (1) | DK2462108T3 (enExample) |
| EA (1) | EA019475B1 (enExample) |
| EC (1) | ECSP12011647A (enExample) |
| EG (1) | EG26957A (enExample) |
| ES (1) | ES2417315T3 (enExample) |
| GE (1) | GEP20146010B (enExample) |
| IL (1) | IL217692A (enExample) |
| IN (1) | IN2012DN00289A (enExample) |
| MX (1) | MX2012001480A (enExample) |
| MY (1) | MY161666A (enExample) |
| NZ (1) | NZ597576A (enExample) |
| PL (1) | PL2462108T3 (enExample) |
| TW (1) | TWI441812B (enExample) |
| UY (1) | UY32835A (enExample) |
| WO (1) | WO2011015416A1 (enExample) |
| ZA (1) | ZA201200413B (enExample) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI534126B (zh) | 2011-01-25 | 2016-05-21 | 先正達合夥公司 | 用於製備吡唑羧酸醯胺之方法 |
| TWI510472B (zh) | 2012-02-15 | 2015-12-01 | Syngenta Participations Ag | 立體選擇性製備吡唑羧醯胺之方法 |
| GB201403438D0 (en) * | 2014-02-27 | 2014-04-16 | Syngenta Participations Ag | Polymorphs |
| WO2015141867A1 (en) | 2014-03-20 | 2015-09-24 | Mitsui Chemicals Agro, Inc. | Plant disease control composition and method for controlling plant disease by application of same |
| IL318101A (en) | 2022-07-22 | 2025-02-01 | Syngenta Crop Protection Ag | Solid form of a heterocyclic amide derivative |
| CN120835879A (zh) * | 2022-10-11 | 2025-10-24 | 先正达农作物保护股份公司 | 用于制备吡唑羧酸酰胺的方法 |
| CN117362179B (zh) * | 2023-09-22 | 2025-07-08 | 浙江工业大学 | 一种苯并烯氟菌唑中间体9-二氯亚甲基-1,4-二氢-5-硝基-1,4-甲桥萘的制备方法 |
| WO2025157998A1 (en) | 2024-01-26 | 2025-07-31 | Syngenta Crop Protection Ag | Chemical process |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004035589A1 (en) * | 2002-10-18 | 2004-04-29 | Syngenta Participations Ag | Heterocyclocarboxamide derivatives |
| CN101296913A (zh) * | 2005-10-25 | 2008-10-29 | 先正达参股股份有限公司 | 用作杀微生物剂的杂环酰胺衍生物 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4370341A (en) * | 1980-12-11 | 1983-01-25 | Ayerst, Mckenna & Harrison, Ltd. | 6,7,8,9-Tetrahydro-3H-benz[E]indol-8-amine derivatives |
| JPS58194853A (ja) * | 1982-05-11 | 1983-11-12 | Showa Denko Kk | シクロヘキセン−アセチルオキシム誘導体 |
| US5093347A (en) | 1991-01-28 | 1992-03-03 | Monsanto Company | 3-difluoromethylpyrazolecarboxamide fungicides, compositions and use |
| US5932752A (en) * | 1995-12-29 | 1999-08-03 | Council Of Scientific And Industrial Research | Process for the C-C bond forming reaction using solid acid catalysts |
| CN1618783A (zh) * | 2004-04-22 | 2005-05-25 | 复旦大学 | 一种多取代苯醌的制备方法 |
-
2010
- 2010-07-07 IN IN289DEN2012 patent/IN2012DN00289A/en unknown
- 2010-07-07 JP JP2012523260A patent/JP5667186B2/ja active Active
- 2010-07-07 ES ES10729880T patent/ES2417315T3/es active Active
- 2010-07-07 EA EA201200246A patent/EA019475B1/ru not_active IP Right Cessation
- 2010-07-07 KR KR1020127005767A patent/KR101712083B1/ko active Active
- 2010-07-07 US US13/389,000 patent/US8507694B2/en active Active
- 2010-07-07 MX MX2012001480A patent/MX2012001480A/es active IP Right Grant
- 2010-07-07 EP EP10729880.4A patent/EP2462108B1/en active Active
- 2010-07-07 BR BR112012002641-0A patent/BR112012002641B1/pt active IP Right Grant
- 2010-07-07 CN CN201080034393.8A patent/CN102574779B/zh active Active
- 2010-07-07 GE GEAP201012617A patent/GEP20146010B/en unknown
- 2010-07-07 MY MYPI2012000229A patent/MY161666A/en unknown
- 2010-07-07 PL PL10729880T patent/PL2462108T3/pl unknown
- 2010-07-07 DK DK10729880.4T patent/DK2462108T3/da active
- 2010-07-07 WO PCT/EP2010/059703 patent/WO2011015416A1/en not_active Ceased
- 2010-07-07 AU AU2010280923A patent/AU2010280923B2/en active Active
- 2010-07-07 CA CA2770144A patent/CA2770144C/en active Active
- 2010-07-07 NZ NZ597576A patent/NZ597576A/xx unknown
- 2010-08-04 AR ARP100102863A patent/AR077707A1/es active IP Right Grant
- 2010-08-04 TW TW099125901A patent/TWI441812B/zh active
- 2010-08-06 UY UY0001032835A patent/UY32835A/es active IP Right Grant
-
2012
- 2012-01-18 ZA ZA2012/00413A patent/ZA201200413B/en unknown
- 2012-01-22 EG EG2012010118A patent/EG26957A/xx active
- 2012-01-23 IL IL217692A patent/IL217692A/en active IP Right Grant
- 2012-02-01 CR CR20120056A patent/CR20120056A/es unknown
- 2012-02-02 CL CL2012000272A patent/CL2012000272A1/es unknown
- 2012-02-02 EC ECSP12011647 patent/ECSP12011647A/es unknown
- 2012-02-03 CO CO12019264A patent/CO6430457A2/es active IP Right Grant
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004035589A1 (en) * | 2002-10-18 | 2004-04-29 | Syngenta Participations Ag | Heterocyclocarboxamide derivatives |
| CN101296913A (zh) * | 2005-10-25 | 2008-10-29 | 先正达参股股份有限公司 | 用作杀微生物剂的杂环酰胺衍生物 |
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| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |