CN102557055B - 一种硅酸锆粉体的制备方法 - Google Patents
一种硅酸锆粉体的制备方法 Download PDFInfo
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- CN102557055B CN102557055B CN201110455917.7A CN201110455917A CN102557055B CN 102557055 B CN102557055 B CN 102557055B CN 201110455917 A CN201110455917 A CN 201110455917A CN 102557055 B CN102557055 B CN 102557055B
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- Prior art keywords
- zirconium silicate
- sol
- preparation
- silicate powder
- reactant
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- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 title claims abstract description 24
- 239000000843 powder Substances 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000006243 chemical reaction Methods 0.000 claims abstract description 12
- 239000002243 precursor Substances 0.000 claims abstract description 12
- 239000000376 reactant Substances 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 7
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 7
- 238000005406 washing Methods 0.000 claims abstract description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000012153 distilled water Substances 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims abstract description 6
- 239000007788 liquid Substances 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 5
- 150000003839 salts Chemical class 0.000 claims description 5
- 238000000967 suction filtration Methods 0.000 claims description 5
- 238000000034 method Methods 0.000 abstract description 10
- 239000013078 crystal Substances 0.000 abstract description 4
- 238000002425 crystallisation Methods 0.000 abstract description 2
- 230000008025 crystallization Effects 0.000 abstract description 2
- 239000007791 liquid phase Substances 0.000 abstract description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 abstract 1
- 229910006251 ZrOCl2.8H2O Inorganic materials 0.000 abstract 1
- 238000000137 annealing Methods 0.000 abstract 1
- 238000007664 blowing Methods 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000002386 leaching Methods 0.000 abstract 1
- 229910006501 ZrSiO Inorganic materials 0.000 description 4
- 238000001027 hydrothermal synthesis Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 239000012716 precipitator Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000003980 solgel method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 241000272816 Anser cygnoides Species 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- BRSGXJFLRBKDFE-UHFFFAOYSA-N [Zr].[O].[Cl] Chemical compound [Zr].[O].[Cl] BRSGXJFLRBKDFE-UHFFFAOYSA-N 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 238000003837 high-temperature calcination Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 229910052604 silicate mineral Inorganic materials 0.000 description 1
- IMNMWKFKHDPTSB-UHFFFAOYSA-N silicic acid zirconium Chemical compound [Zr].[Si](O)(O)(O)O IMNMWKFKHDPTSB-UHFFFAOYSA-N 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000010532 solid phase synthesis reaction Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- DUNKXUFBGCUVQW-UHFFFAOYSA-J zirconium tetrachloride Chemical compound Cl[Zr](Cl)(Cl)Cl DUNKXUFBGCUVQW-UHFFFAOYSA-J 0.000 description 1
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- Silicates, Zeolites, And Molecular Sieves (AREA)
Abstract
Description
Claims (1)
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CN201110455917.7A CN102557055B (zh) | 2011-11-23 | 2011-12-30 | 一种硅酸锆粉体的制备方法 |
Applications Claiming Priority (3)
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CN201110375803 | 2011-11-23 | ||
CN201110375803.1 | 2011-11-23 | ||
CN201110455917.7A CN102557055B (zh) | 2011-11-23 | 2011-12-30 | 一种硅酸锆粉体的制备方法 |
Publications (2)
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CN102557055A CN102557055A (zh) | 2012-07-11 |
CN102557055B true CN102557055B (zh) | 2014-03-12 |
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CN201110455917.7A Expired - Fee Related CN102557055B (zh) | 2011-11-23 | 2011-12-30 | 一种硅酸锆粉体的制备方法 |
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Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103922354A (zh) * | 2014-04-24 | 2014-07-16 | 北京化工大学 | 溶胶-凝胶法合成高产率的硅酸锆粉体 |
CN108706597B (zh) * | 2018-06-12 | 2020-07-14 | 湖北大学 | 一种硅酸锆粉体及其制备方法与应用 |
CN110498691A (zh) * | 2019-10-09 | 2019-11-26 | 江苏脒诺甫纳米材料有限公司 | 一种基于陶瓷烧结技术的硅基陶瓷气凝胶制备工艺 |
CN111661852A (zh) * | 2020-06-11 | 2020-09-15 | 大冶市都鑫摩擦粉体有限公司 | 一种硅酸锆粉体的制备装置及其工艺 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2008137502A1 (en) * | 2007-05-04 | 2008-11-13 | University Of Massachusetts | Highly condensed mesoporous silicate compositions and methods |
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2011
- 2011-12-30 CN CN201110455917.7A patent/CN102557055B/zh not_active Expired - Fee Related
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
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WO2008137502A1 (en) * | 2007-05-04 | 2008-11-13 | University Of Massachusetts | Highly condensed mesoporous silicate compositions and methods |
Non-Patent Citations (6)
Title |
---|
Eduardo Blanco等.Sonogels and Derived Materials.《applied organometallic chemistry》.1999,第13卷(第5期),第399-418页. |
Sonogels and Derived Materials;Eduardo Blanco等;《applied organometallic chemistry》;19991231;第13卷(第5期);全文 * |
ZrSiO4纳米粉体的微波水热法合成及其合成机理;刘大为等;《陕西科技大学学报》;20110228;第29卷(第1期);第44页第2-4段 * |
刘大为等.ZrSiO4纳米粉体的微波水热法合成及其合成机理.《陕西科技大学学报》.2011,第29卷(第1期),第43-46页. |
肖锋等.超声技术在无机材料合成与制备中的应用.《硅酸盐学报》.2002,第30卷(第5期),第617-618页. |
超声技术在无机材料合成与制备中的应用;肖锋等;《硅酸盐学报》;20021031;第30卷(第5期);第617页第2栏第2段,第617页第2栏倒数第1段-第618页第1栏第1段 * |
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