CN102522530A - 一种稀土锂硫电池用纳米硫复合正极材料及其制备方法 - Google Patents
一种稀土锂硫电池用纳米硫复合正极材料及其制备方法 Download PDFInfo
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- CN102522530A CN102522530A CN2011104437663A CN201110443766A CN102522530A CN 102522530 A CN102522530 A CN 102522530A CN 2011104437663 A CN2011104437663 A CN 2011104437663A CN 201110443766 A CN201110443766 A CN 201110443766A CN 102522530 A CN102522530 A CN 102522530A
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- sulfur
- rare earth
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- carbon nano
- nano
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- 239000002131 composite material Substances 0.000 title claims abstract description 48
- 229910052761 rare earth metal Inorganic materials 0.000 title claims abstract description 36
- 150000002910 rare earth metals Chemical class 0.000 title claims abstract description 36
- JDZCKJOXGCMJGS-UHFFFAOYSA-N [Li].[S] Chemical compound [Li].[S] JDZCKJOXGCMJGS-UHFFFAOYSA-N 0.000 title claims abstract description 28
- 229910052717 sulfur Inorganic materials 0.000 title claims abstract description 12
- 239000011593 sulfur Substances 0.000 title claims abstract description 12
- 238000002360 preparation method Methods 0.000 title abstract description 11
- 239000010406 cathode material Substances 0.000 title abstract 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 60
- 239000002041 carbon nanotube Substances 0.000 claims abstract description 31
- 229910021393 carbon nanotube Inorganic materials 0.000 claims abstract description 31
- 239000000463 material Substances 0.000 claims abstract description 28
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 13
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000001354 calcination Methods 0.000 claims abstract description 11
- 239000007789 gas Substances 0.000 claims abstract description 11
- 238000000034 method Methods 0.000 claims abstract description 8
- 229910052786 argon Inorganic materials 0.000 claims abstract description 6
- 239000005864 Sulphur Substances 0.000 claims description 35
- -1 carbon nano tube compound Chemical class 0.000 claims description 19
- 229910052799 carbon Inorganic materials 0.000 claims description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 10
- 230000003647 oxidation Effects 0.000 claims description 10
- 238000007254 oxidation reaction Methods 0.000 claims description 10
- 238000012545 processing Methods 0.000 claims description 10
- 229910052727 yttrium Inorganic materials 0.000 claims description 10
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 claims description 10
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 239000002048 multi walled nanotube Substances 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- 150000001875 compounds Chemical class 0.000 claims 1
- 238000011282 treatment Methods 0.000 abstract 2
- 238000000498 ball milling Methods 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 238000009413 insulation Methods 0.000 abstract 1
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 8
- 229910001416 lithium ion Inorganic materials 0.000 description 8
- 230000009286 beneficial effect Effects 0.000 description 3
- 229910002097 Lithium manganese(III,IV) oxide Inorganic materials 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003792 electrolyte Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- GLNWILHOFOBOFD-UHFFFAOYSA-N lithium sulfide Chemical compound [Li+].[Li+].[S-2] GLNWILHOFOBOFD-UHFFFAOYSA-N 0.000 description 2
- 229910052493 LiFePO4 Inorganic materials 0.000 description 1
- 102100023116 Sodium/nucleoside cotransporter 1 Human genes 0.000 description 1
- 101710123675 Sodium/nucleoside cotransporter 1 Proteins 0.000 description 1
- 239000010405 anode material Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 238000003837 high-temperature calcination Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/0471—Processes of manufacture in general involving thermal treatment, e.g. firing, sintering, backing particulate active material, thermal decomposition, pyrolysis
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/136—Electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/139—Processes of manufacture
- H01M4/1397—Processes of manufacture of electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/38—Selection of substances as active materials, active masses, active liquids of elements or alloys
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
- H01M4/624—Electric conductive fillers
- H01M4/625—Carbon or graphite
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Carbon And Carbon Compounds (AREA)
- Secondary Cells (AREA)
Abstract
Description
Claims (3)
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110443766.3A CN102522530B (zh) | 2011-12-27 | 2011-12-27 | 一种稀土锂硫电池用纳米硫复合正极材料及其制备方法 |
TW101101412A TWI524583B (zh) | 2011-12-27 | 2012-01-13 | Nano - sulfur composite cathode material for rare earth lithium - sulfur battery and its preparation method |
KR1020120017779A KR101390585B1 (ko) | 2011-12-27 | 2012-02-22 | 희토류 리튬 황 전지용 나노황 복합 양극 재료 및 그의 제조 방법 |
US13/403,952 US8858840B2 (en) | 2011-12-27 | 2012-02-23 | Nano-sulfur composite anode material for rare earth lithium-sulfur battery and its preparation method thereof |
JP2012053317A JP5738222B2 (ja) | 2011-12-27 | 2012-03-09 | 希土類リチウム硫黄電池用のナノメートル硫黄複合正極材及びその製造方法 |
HK12107494.2A HK1166883A1 (zh) | 2011-12-27 | 2012-07-31 | 種稀土鋰硫電池用納米硫複合正極材料及其製備方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110443766.3A CN102522530B (zh) | 2011-12-27 | 2011-12-27 | 一种稀土锂硫电池用纳米硫复合正极材料及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102522530A true CN102522530A (zh) | 2012-06-27 |
CN102522530B CN102522530B (zh) | 2014-08-20 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201110443766.3A Active CN102522530B (zh) | 2011-12-27 | 2011-12-27 | 一种稀土锂硫电池用纳米硫复合正极材料及其制备方法 |
Country Status (6)
Country | Link |
---|---|
US (1) | US8858840B2 (zh) |
JP (1) | JP5738222B2 (zh) |
KR (1) | KR101390585B1 (zh) |
CN (1) | CN102522530B (zh) |
HK (1) | HK1166883A1 (zh) |
TW (1) | TWI524583B (zh) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102891292A (zh) * | 2012-09-24 | 2013-01-23 | 上海锦众信息科技有限公司 | 一种锂硫电池正极复合材料的制备方法 |
CN103022500A (zh) * | 2012-12-05 | 2013-04-03 | 上海锦众信息科技有限公司 | 一种硫锂电池正极复合材料的制备方法 |
WO2013097116A1 (zh) * | 2011-12-28 | 2013-07-04 | Chung Winston | 一种稀土锂硫电池用纳米硫复合正极材料及其制备方法 |
CN108598415A (zh) * | 2018-04-24 | 2018-09-28 | 中国石油大学(华东) | 一种用于锂硫电池正极的复合材料及其制备方法 |
CN109301230A (zh) * | 2018-11-13 | 2019-02-01 | 南昌大学 | 一种锂硫电池用复合正极材料及其制备方法 |
CN115566251A (zh) * | 2022-09-29 | 2023-01-03 | 重庆邮电大学 | 可在低温工作的柔性全固态光热锂硫电池及其制备方法 |
Families Citing this family (16)
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CN105900268B (zh) * | 2013-10-18 | 2018-10-26 | 株式会社Lg化学 | 包含碳纳米管聚集体的碳纳米管-硫复合材料及其制备方法 |
CN103715403B (zh) * | 2013-12-18 | 2015-08-12 | 湘潭大学 | 一种基于蛭石的锂硫电池正极材料及其制备和应用方法 |
JP6541774B2 (ja) | 2014-05-15 | 2019-07-10 | エムエスエムエイチ,エルエルシー | リチウムによってインターカレートされたナノ結晶系アノード |
US10629320B2 (en) | 2014-05-15 | 2020-04-21 | Msmh, Llc | Method for producing sulfur charged carbon nanotubes and cathodes for lithium ion batteries |
EP3142965A4 (en) | 2014-05-15 | 2018-01-24 | Msmh, Llc | Methods and systems for the synthesis of nanoparticles including strained nanoparticles |
JP6796254B2 (ja) * | 2014-11-13 | 2020-12-09 | 株式会社Gsユアサ | 硫黄−カーボン複合体、硫黄―カーボン複合体を含む電極を備えた非水電解質電池、及び硫黄−カーボン複合体の製造方法 |
FR3030890B1 (fr) | 2014-12-22 | 2019-07-26 | Arkema France | Matiere active d'electrode pour batterie li/s |
CN109638231B (zh) * | 2017-10-09 | 2020-09-25 | 卡博特高性能材料(珠海)有限公司 | 氧化亚硅复合负极材料及其制备方法和锂离子电池 |
CN108269999B (zh) * | 2017-12-20 | 2020-07-17 | 合肥国轩高科动力能源有限公司 | 一种锂离子电池用容量缓释型高镍三元材料的制备方法 |
CN108054377B (zh) * | 2017-12-27 | 2020-08-04 | 湖南工业大学 | 一种毛线球状碳/硫复合微球材料的制备方法及锂硫电池 |
FR3076952B1 (fr) * | 2018-01-16 | 2023-08-11 | Arkema France | Formulation sous la forme d'une dispersion solide-liquide pour la fabrication d'une cathode pour batterie li/s et procede de preparation de ladite formulation |
CN108682813A (zh) * | 2018-05-10 | 2018-10-19 | 厦门大学 | 一种硅碳复合材料的制备方法及应用 |
CN109004196A (zh) * | 2018-07-24 | 2018-12-14 | 大连理工大学 | 一种棉花包覆钛酸锂负极材料的制备方法 |
KR102293892B1 (ko) | 2018-09-19 | 2021-08-24 | 주식회사 엘지화학 | 황-탄소 복합체의 제조방법, 그에 의해 제조된 황-탄소 복합체, 상기 황-탄소 복합체를 포함하는 양극, 및 상기 양극을 포함하는 리튬 이차 전지 |
CN109461905B (zh) * | 2018-09-30 | 2022-01-14 | 肇庆市华师大光电产业研究院 | 一种锂硫电池正极材料及其制备方法 |
CN112662204B (zh) * | 2020-12-23 | 2022-03-01 | 哈尔滨工业大学 | 一种用于锂硫电池的多孔/类空心状碳黑材料的制备方法 |
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2011
- 2011-12-27 CN CN201110443766.3A patent/CN102522530B/zh active Active
-
2012
- 2012-01-13 TW TW101101412A patent/TWI524583B/zh active
- 2012-02-22 KR KR1020120017779A patent/KR101390585B1/ko active IP Right Grant
- 2012-02-23 US US13/403,952 patent/US8858840B2/en active Active
- 2012-03-09 JP JP2012053317A patent/JP5738222B2/ja active Active
- 2012-07-31 HK HK12107494.2A patent/HK1166883A1/zh unknown
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2013097116A1 (zh) * | 2011-12-28 | 2013-07-04 | Chung Winston | 一种稀土锂硫电池用纳米硫复合正极材料及其制备方法 |
CN102891292A (zh) * | 2012-09-24 | 2013-01-23 | 上海锦众信息科技有限公司 | 一种锂硫电池正极复合材料的制备方法 |
CN103022500A (zh) * | 2012-12-05 | 2013-04-03 | 上海锦众信息科技有限公司 | 一种硫锂电池正极复合材料的制备方法 |
CN108598415A (zh) * | 2018-04-24 | 2018-09-28 | 中国石油大学(华东) | 一种用于锂硫电池正极的复合材料及其制备方法 |
CN108598415B (zh) * | 2018-04-24 | 2020-05-29 | 中国石油大学(华东) | 一种用于锂硫电池正极的复合材料及其制备方法 |
CN109301230A (zh) * | 2018-11-13 | 2019-02-01 | 南昌大学 | 一种锂硫电池用复合正极材料及其制备方法 |
CN109301230B (zh) * | 2018-11-13 | 2021-08-13 | 南昌大学 | 一种锂硫电池用复合正极材料及其制备方法 |
CN115566251A (zh) * | 2022-09-29 | 2023-01-03 | 重庆邮电大学 | 可在低温工作的柔性全固态光热锂硫电池及其制备方法 |
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US20130161557A1 (en) | 2013-06-27 |
TW201328004A (zh) | 2013-07-01 |
JP5738222B2 (ja) | 2015-06-17 |
HK1166883A1 (zh) | 2012-11-09 |
JP2013137981A (ja) | 2013-07-11 |
KR101390585B1 (ko) | 2014-04-30 |
US8858840B2 (en) | 2014-10-14 |
TWI524583B (zh) | 2016-03-01 |
CN102522530B (zh) | 2014-08-20 |
KR20130075621A (ko) | 2013-07-05 |
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