CN102357070B - Hydrolyzed silk protein/ recombinant human Epidermal Growth Factor (rhEGF) compound skin care facial mask and preparation method thereof - Google Patents
Hydrolyzed silk protein/ recombinant human Epidermal Growth Factor (rhEGF) compound skin care facial mask and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a hydrolyzed silk protein/ recombinant human Epidermal Growth Factor (rhEGF) compound skin care facial mask and a preparation method thereof. The hydrolyzed silk protein/ rhEGF compound skin care facial mask is prepared by components of 18 materials, and comprises two main components including, by weight, 1.5% to 2.5% of hydrolyzed silk protein and 0.01% to 0.1% of rhEGF. The skin care facial mask utilizes natural silk which contains a plurality of amino acids and proteins, and has the skin care effect of whitening, moisture preservation, skin smoothing, skin ageing retarding and the like. Each piece of silk facial mask converges rich silk protein essence, rhEGF and whitening moisture preservation components, provides dense whitening moistening for the skin, instantly brightens the skin color, enables the skin to be white and tender, solves the problems of withered and yellow skin color, dryness, roughness, fine wrinkles, elasticity lacking, thick pores and the like, retains corneum moisture and integrity of a fiber structure, enables dark skin to reproduce silky smoothness and regain the touching color.
Description
Technical field
The present invention relates to a kind of skin protection cosmetics, especially a kind of hydrolyzed silkworm silk albumen/rhEGF composition skin-care facial film and preparation method thereof.
Background technology
Aging for slowing down face skin has various ways, such as: the use of diet control, defying age elite etc.And the facial film that contains hydrolyzed silkworm silk albumen/rhEGF compositions directly acts on the skin after the cleaning, can more effectively infiltrate through skin, but effectively real, the anti-ageing face mask that has no side effect is rare.
Summary of the invention
The technical problem to be solved in the present invention provides a kind of goodish oxidation resistance that has, and the energy slowing down skin aging has prevention and subtracts light facial microgroove, the hydrolyzed silkworm silk albumen of the delaying senility of the unique effects such as mottle/rhEGF composition skin-care facial film.
The present invention also provides the preparation method of a kind of said hydrolyzed fibroin/rhEGF composition skin-care facial film simultaneously.
To achieve these goals, the technical solution used in the present invention is that a kind of hydrolyzed silkworm silk albumen/rhEGF composition skin-care facial film is by weight percentage by following constituent content:
The A phase materials:
(1) deionized water 53.17-76.66%;
(2) glycerol 3.5-4.5%;
(3) trehalose 2.6-8.8%;
(4) trimethyl glycine 1.0-3.0%;
(5) hydrolyzed silkworm silk albumen 1.5-2.5%;
(6) pentanediol 3.0-6.0%;
The B phase materials:
(7) active yeast extract 0.1-2.1%;
(8) Flos Rosae Rugosae extracting solution 1.0-2.0%;
(9) aloe gel 1:1 .5-2.5%;
(10) chlorella elite 1.3-2.3%;
(11) Fructus Mori elite 2.0-3.0%;
(12) L-vitamin C 4.0-5.5%;
The C phase materials:
(13) Argireline 1.2-2.2%;
(14) Wushengtai 0.1-0.8%;
(15) taurine 0.5-1.4%;
(16) hyaluronic acid 0.02-0.1%;
(17) Herba Lysimachiae foenum-graeci quintessence oil 0.01.-0.03%;
(18)rhEGF 0.01-0.1％。
Preferably, described hydrolyzed silkworm silk albumen/rhEGF composition skin-care facial film by following constituent content is by weight percentage:
The A phase materials:
(1) deionized water 53.17-76.67%;
(2) glycerol 2.7-8.6%;
(3) trehalose 1.0-5.0%;
(4) trimethyl glycine 0-3.0%;
(5) hydrolyzed silkworm silk albumen 1.0-6.0%;
(6) pentanediol 1.0-4.0%;
The B phase materials:
(7) active yeast extract 0.1-2.1%;
(8) Flos Rosae Rugosae extracting solution 1.0-2.0%;
(9) Aloe gel 0.5-4.5%;
(10) chlorella elite 1.0-4.3%;
(11) Fructus Mori elite 1.0-2.0%;
(12) L-vitamin C 1.0-5.5%;
The C phase materials:
(13) Argireline 0.2-2.0%;
(14) Wushengtai 0.1-1.8%;
(15) taurine 0.5-4.4%;
(16) hyaluronic acid 0.05-0.1%;
(17) Herba Lysimachiae foenum-graeci quintessence oil 0.01.-0.03%;
(18)rhEGF 0.05-0.3％。
The preparation method of a kind of said hydrolyzed fibroin/rhEGF composition skin-care facial film may further comprise the steps:
(1) by each phase raw material of above-mentioned percentage by weight weighing;
(2) each component of A phase materials is mixed stir evenly after, add in the emulsifying pot and be heated to 80 ℃-85 ℃, under the vacuum state, constant temperature sterilization 25-35 minute;
(3) step (2) products therefrom is cooled to 40 ℃ and adds successively each component of B phase materials, stir transparent;
(4) step (3) products therefrom is cooled to 35 ℃ and adds successively each component of C phase materials, stir;
(5) 35 ℃ of whipping steps (4) products therefrom detected qualified rear discharging after 10 minutes.
The invention has the beneficial effects as follows that a kind of composition skin-care product of delaying senility contain deionized water, glycerol in every part; trehalose, trimethyl glycine, hydrolyzed silkworm silk albumen, pentanediol; the active yeast extract, Flos Rosae Rugosae extracting solution, Aloe gel; the chlorella elite, Fructus Mori elite, L-vitamin C; Argireline, Wushengtai, taurine; hyaluronic acid, Herba Lysimachiae foenum-graeci quintessence oil, oligopeptide-1.After thorough clean, this facial film is applied to face, after 20 minutes, cleans with clean product.Goodish oxidation resistance is originally arranged, and the energy slowing down skin aging has prevention and subtracts light facial microgroove, the unique effects of mottle.
The aging of skin can bring facial wrinkles, the facial beautiful problem of the various impacts such as mottle.Active ingredient among the present invention can be absorbed by the skin by the distinctive hydration of keratin, for skin provides sufficient moisture and prevents that the moisture evaporation in the keratodermatitis from reducing.Make additional moist nutrition skin-protection composition be easy to absorb, can keep facial and moisten, avoid the skin of face accelerated ageing, reduce the appearance of skin of face matter wrinkle.In addition, unique Antioxidative Factors can fundamentally make the skin anti-aging ability increase delaying skin aging.
The specific embodiment
Embodiment 1
The raw material total amount is 100 kilograms.Wherein, the A phase materials is: 3.5 kilograms of glycerol, 2.6 kilograms of trehaloses, 1.0 kilograms of trimethyl glycine, 1.5 kilograms in hydrolyzed silkworm silk albumen, 3.0 kilograms of pentanediols; The B phase materials is: 0.1 kilogram of active yeast extract, 1.0 kilograms of Flos Rosae Rugosae extracting solution, aloe gel 1:1 .5 kilogram, 1.3 kilograms of chlorella elite, 2.0 kilograms of Fructus Mori elite, L-vitamin C4.0 kilogram; The C phase materials is: 1.2 kilograms of Argirelines, 0.1 kilogram of Wushengtai, 0.5 kilogram of taurine, 0.02 kilogram of hyaluronic acid, 0.01 kilogram of Herba Lysimachiae foenum-graeci quintessence oil, 0.01 kilogram of rhEGF; Surplus is supplied by the deionized water of A phase.
Preparation technology:
(1) by each phase raw material of above-mentioned percentage by weight weighing;
(2) each component of A phase materials is mixed stir evenly after, add in the emulsifying pot and be heated to 80 ℃-85 ℃, under the vacuum state, constant temperature sterilization 25-35 minute;
(3) step (2) products therefrom is cooled to 40 ℃ and adds successively each component of B phase materials, stir transparent;
(4) step (3) products therefrom is cooled to 35 ℃ and adds successively each component of C phase materials, stir;
(5) 35 ℃ of whipping steps (4) products therefrom detected qualified rear discharging after 10 minutes.
Embodiment 2
The raw material total amount is 100 kilograms.Wherein, A phase materials: 4.0 kilograms of glycerol, 3.1 kilograms of trehaloses, 1.5 kilograms of trimethyl glycine, 2.0 kilograms in hydrolyzed silkworm silk albumen, 3.5 kilograms of pentanediols; The B phase materials is: 0.6 kilogram of active yeast extract, 1.5 kilograms of Flos Rosae Rugosae extracting solution, 2.0 kilograms of Aloe gels, 1.8 kilograms of chlorella elite, 2.5 kilograms of Fructus Mori elite, L-vitamin C4.5 kilogram; The C phase materials is: 1.7 kilograms of Argirelines, 0.6 kilogram of Wushengtai, 1.0 kilograms of taurines, 0.07 kilogram of hyaluronic acid, 0.03 kilogram of Herba Lysimachiae foenum-graeci quintessence oil, rhEGF0.06 kilogram; Surplus is supplied by the deionized water of A phase.
Preparation technology is with embodiment 1.
Embodiment 3
The raw material total amount is 100 kilograms.Wherein, A phase materials: 4.5 kilograms of glycerol, 3.6 kilograms of trehaloses, 2.0 kilograms of trimethyl glycine, 2.5 kilograms in hydrolyzed silkworm silk albumen, 4.0 kilograms of pentanediols; The B phase materials is: 1.1 kilograms of active yeast extracts, 2.0 kilograms of Flos Rosae Rugosae extracting solution, 2.5 kilograms of Aloe gels, 2.3 kilograms of chlorella elite, 3.0 kilograms of Fructus Mori elite, L-vitamin C5.0 kilogram; The C phase materials is: 2.2 kilograms of Argirelines, 0.8 kilogram of Wushengtai, 1.4 kilograms of taurines, 0.1 kilogram of hyaluronic acid, 0.03 kilogram of Herba Lysimachiae foenum-graeci quintessence oil, rhEGF0.1 kilogram; Surplus is supplied by the deionized water of A phase.
Preparation technology is with embodiment 1.
Embodiment 4
The raw material total amount is 100 kilograms.Wherein, A phase materials: 4.5 kilograms of glycerol, 4.1 kilograms of trehaloses, 2.5 kilograms of trimethyl glycine, 2.5 kilograms in hydrolyzed silkworm silk albumen, 4.5 kilograms of pentanediols; The B phase materials is: 1.6 kilograms of active yeast extracts, 2.0 kilograms of Flos Rosae Rugosae extracting solution, 2.5 kilograms of Aloe gels, 2.3 kilograms of chlorella elite, 3.0 kilograms of Fructus Mori elite, L-vitamin C5.5 kilogram; The C phase materials is: 2.2 kilograms of Argirelines, 0.8 kilogram of Wushengtai, 1.4 kilograms of taurines, 0.1 kilogram of hyaluronic acid, 0.03 kilogram of Herba Lysimachiae foenum-graeci quintessence oil, rhEGF0.1 kilogram; Surplus is supplied by the deionized water of A phase.
Preparation technology is with embodiment 1.
Embodiment 5
The raw material total amount is 100 kilograms.Wherein, A phase materials: 4.5 kilograms of glycerol, 4.6 kilograms of trehaloses, 3.0 kilograms of trimethyl glycine, 2.5 kilograms in hydrolyzed silkworm silk albumen, 5.0 kilograms of pentanediols; The B phase materials is: 2.1 kilograms of active yeast extracts, 2.0 kilograms of Flos Rosae Rugosae extracting solution, 2.5 kilograms of Aloe gels, 2.3 kilograms of chlorella elite, 3.0 kilograms of Fructus Mori elite, L-vitamin C5.5 kilogram; The C phase materials is: 2.2 kilograms of Argirelines, 0.8 kilogram of Wushengtai, 1.4 kilograms of taurines, 0.1 kilogram of hyaluronic acid, 0.03 kilogram of Herba Lysimachiae foenum-graeci quintessence oil, rhEGF0.1 kilogram; Surplus is supplied by the deionized water of A phase.
Preparation technology is with embodiment 1.
Embodiment 6
The raw material total amount is 100 kilograms.Wherein, A phase materials: 4.5 kilograms of glycerol, 5.1 kilograms of trehaloses, 3.0 kilograms of trimethyl glycine, 2.5 kilograms in hydrolyzed silkworm silk albumen, 5.5 kilograms of pentanediols; The B phase materials is: 2.1 kilograms of active yeast extracts, 2.0 kilograms of Flos Rosae Rugosae extracting solution, 2.5 kilograms of Aloe gels, 2.3 kilograms of chlorella elite, 3.0 kilograms of Fructus Mori elite, L-vitamin C5.5 kilogram; The C phase materials is: 2.2 kilograms of Argirelines, 0.8 kilogram of Wushengtai, 1.4 kilograms of taurines, 0.1 kilogram of hyaluronic acid, 0.03 kilogram of Herba Lysimachiae foenum-graeci quintessence oil, rhEGF0.1 kilogram; Surplus is supplied by the deionized water of A phase.
Preparation technology is with embodiment 1.
Embodiment 7
The raw material total amount is 100 kilograms.Wherein, A phase materials: 4.5 kilograms of glycerol, 5.6 kilograms of trehaloses, 3.0 kilograms of trimethyl glycine, 2.5 kilograms in hydrolyzed silkworm silk albumen, 6.0 kilograms of pentanediols; The B phase materials is: 2.1 kilograms of active yeast extracts, 2.0 kilograms of Flos Rosae Rugosae extracting solution, 2.5 kilograms of Aloe gels, 2.3 kilograms of chlorella elite, 3.0 kilograms of Fructus Mori elite, L-vitamin C5.5 kilogram; The C phase materials is: 2.2 kilograms of Argirelines, 0.8 kilogram of Wushengtai, 1.4 kilograms of taurines, 0.1 kilogram of hyaluronic acid, 0.03 kilogram of Herba Lysimachiae foenum-graeci quintessence oil, rhEGF0.1 kilogram; Surplus is supplied by the deionized water of A phase.
Preparation technology is with embodiment 1.
Embodiment 8
The raw material total amount is 100 kilograms.Wherein, A phase materials: 4.5 kilograms of glycerol, 6.1 kilograms of trehaloses, 3.0 kilograms of trimethyl glycine, 2.5 kilograms in hydrolyzed silkworm silk albumen, 6.0 kilograms of pentanediols; The B phase materials is: 2.1 kilograms of active yeast extracts, 2.0 kilograms of Flos Rosae Rugosae extracting solution, 2.5 kilograms of Aloe gels, 2.3 kilograms of chlorella elite, 3.0 kilograms of Fructus Mori elite, L-vitamin C5.5 kilogram; The C phase materials is: 2.2 kilograms of Argirelines, 0.8 kilogram of Wushengtai, 1.4 kilograms of taurines, 0.1 kilogram of hyaluronic acid, 0.03 kilogram of Herba Lysimachiae foenum-graeci quintessence oil, rhEGF0.1 kilogram; Surplus is supplied by the deionized water of A phase.Preparation technology is with embodiment 1.
Embodiment 9
The raw material total amount is 100 kilograms.Wherein, A phase materials: 4.5 kilograms of glycerol, 6.6 kilograms of trehaloses, 3.0 kilograms of trimethyl glycine, 2.5 kilograms in hydrolyzed silkworm silk albumen, 6.0 kilograms of pentanediols; The B phase materials is: 2.1 kilograms of active yeast extracts, 2.0 kilograms of Flos Rosae Rugosae extracting solution, 2.5 kilograms of Aloe gels, 2.3 kilograms of chlorella elite, 3.0 kilograms of Fructus Mori elite, L-vitamin C5.5 kilogram; The C phase materials is: 2.2 kilograms of Argirelines, 0.8 kilogram of Wushengtai, 1.4 kilograms of taurines, 0.1 kilogram of hyaluronic acid, 0.03 kilogram of Herba Lysimachiae foenum-graeci quintessence oil, rhEGF0.1 kilogram; Surplus is supplied by the deionized water of A phase.
Preparation technology is with embodiment 1.
Embodiment 10
The raw material total amount is 100 kilograms.Wherein, A phase materials: 4.5 kilograms of glycerol, 7.1 kilograms of trehaloses, 3.0 kilograms of trimethyl glycine, 2.5 kilograms in hydrolyzed silkworm silk albumen, 6.0 kilograms of pentanediols; The B phase materials is: 2.1 kilograms of active yeast extracts, 2.0 kilograms of Flos Rosae Rugosae extracting solution, 2.5 kilograms of Aloe gels, 2.3 kilograms of chlorella elite, 3.0 kilograms of Fructus Mori elite, L-vitamin C5.5 kilogram; The C phase materials is: 2.2 kilograms of Argirelines, 0.8 kilogram of Wushengtai, 1.4 kilograms of taurines, 0.1 kilogram of hyaluronic acid, 0.03 kilogram of Herba Lysimachiae foenum-graeci quintessence oil, rhEGF0.1 kilogram; Surplus is supplied by the deionized water of A phase.
Preparation technology is with embodiment 1.
Embodiment 11
The raw material total amount is 100 kilograms.Wherein, A phase materials: 2.7 kilograms of glycerol, 1.0 kilograms of trehaloses, 1.0 kilograms in hydrolyzed silkworm silk albumen, 1.0 kilograms of pentanediols; The B phase materials is: 0.1 kilogram of active yeast extract, 1.0 kilograms of Flos Rosae Rugosae extracting solution, 0.5 kilogram of Aloe gel, 1.0 kilograms of chlorella elite, 1.0 kilograms of Fructus Mori elite, L-vitamin C1.0 kilogram; The C phase materials is: 0.2 kilogram of Argireline, 0.1 kilogram of Wushengtai, 0.5 kilogram of taurine, 0.02 kilogram of hyaluronic acid, 0.01 kilogram of Herba Lysimachiae foenum-graeci quintessence oil, 0.01 kilogram of rhEGF; Surplus is supplied by the deionized water of A phase.Preparation technology is with embodiment 1.
Embodiment 12
The raw material total amount is 100 kilograms.Wherein, A phase materials: 8.6 kilograms of glycerol, 8.8 kilograms of trehaloses, 3.0 kilograms of trimethyl glycine, 6.0 kilograms in hydrolyzed silkworm silk albumen, 6.0 kilograms of pentanediols; The B phase materials is: 2.1 kilograms of active yeast extracts, 2.0 kilograms of Flos Rosae Rugosae extracting solution, 4.5 kilograms of Aloe gels, 4.3 kilograms of chlorella elite, 3.0 kilograms of Fructus Mori elite, L-vitamin C5.5 kilogram; The C phase materials is: 2.2 kilograms of Argirelines, 1.8 kilograms of Wushengtais, 4.4 kilograms of taurines, 0.1 kilogram of hyaluronic acid, 0.03 kilogram of Herba Lysimachiae foenum-graeci quintessence oil, rhEGF0.3 kilogram; Surplus is supplied by the deionized water of A phase.
Preparation technology is with embodiment 1.
Only be preferred implementation of the present invention in sum, should be understood that for the person of ordinary skill of the art that without departing from the inventive concept of the premise, can also make several distortion and improvement, these also should be considered as within protection scope of the present invention.
Claims (3)
1. hydrolyzed silkworm silk albumen/rhEGF composition skin-care facial film is characterized in that, by following constituent content is by weight percentage:
The A phase materials:
(1) deionized water 53.17-76.66%;
(2) glycerol 3.5-4.5%;
(3) trehalose 2.6-8.8%;
(4) trimethyl glycine 1.0-3.0%;
(5) hydrolyzed silkworm silk albumen 1.5-2.5%;
(6) pentanediol 3.0-6.0%;
The B phase materials:
(7) active yeast extract 0.1-2.1%;
(8) Flos Rosae Rugosae extracting solution 1.0-2.0%;
(9) aloe gel 1:1 .5-2.5%;
(10) chlorella elite 1.3-2.3%;
(11) Fructus Mori elite 2.0-3.0%;
(12) L-vitamin C 4.0-5.5%;
The C phase materials:
(13) Argireline 1.2-2.2%;
(14) Wushengtai 0.1-0.8%;
(15) taurine 0.5-1.4%;
(16) hyaluronic acid 0.02-0.1%;
(17) Herba Lysimachiae foenum-graeci quintessence oil 0.01-0.03%;
(18)rhEGF 0.01-0.1％。
2. hydrolyzed silkworm silk albumen/rhEGF composition skin-care facial film is characterized in that, by following constituent content is by weight percentage:
The A phase materials:
(1) deionized water 53.17-76.67%;
(2) glycerol 2.7-8.6%;
(3) trehalose 1.0-5.0%;
(4) trimethyl glycine 0-3.0%;
(5) hydrolyzed silkworm silk albumen 1.0-6.0%;
(6) pentanediol 1.0-4.0%;
The B phase materials:
(7) active yeast extract 0.1-2.1%;
(8) Flos Rosae Rugosae extracting solution 1.0-2.0%;
(9) Aloe gel 0.5-4.5%;
(10) chlorella elite 1.0-4.3%;
(11) Fructus Mori elite 1.0-2.0%;
(12) L-vitamin C 1.0-5.5%;
The C phase materials:
(13) Argireline 0.2-2.0%;
(14) Wushengtai 0.1-1.8%;
(15) taurine 0.5-4.4%;
(16) hyaluronic acid 0.05-0.1%;
(17) Herba Lysimachiae foenum-graeci quintessence oil 0.01-0.03%;
(18)rhEGF 0.05-0.3％。
3. the preparation method of a kind of hydrolyzed silkworm silk albumen according to claim 1 and 2/rhEGF composition skin-care facial film is characterized in that, may further comprise the steps:
(1) by claim 1 or each phase raw material of percentage by weight weighing of 2;
(2) each component of A phase materials is mixed stir evenly after, add in the emulsifying pot and be heated to 80 ℃-85 ℃, under the vacuum state, constant temperature sterilization 25-35 minute;
(3) step (2) products therefrom is cooled to 40 ℃ and adds successively each component of B phase materials, stir transparent;
(4) step (3) products therefrom is cooled to 35 ℃ and adds successively each component of C phase materials, stir;
(5) 35 ℃ of whipping steps (4) products therefrom detected qualified rear discharging after 10 minutes.
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| 陈秋东.中等纯度重组人表皮生长因子（rhEGF）的分离纯化及在美.《中国优秀硕士学位论文全文数据库工程技术Ⅰ辑》.2003,(第2期),第75-76页. * |
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