CN102256923B - 制备羧酸酯的方法 - Google Patents

制备羧酸酯的方法 Download PDF

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Publication number
CN102256923B
CN102256923B CN2009801506516A CN200980150651A CN102256923B CN 102256923 B CN102256923 B CN 102256923B CN 2009801506516 A CN2009801506516 A CN 2009801506516A CN 200980150651 A CN200980150651 A CN 200980150651A CN 102256923 B CN102256923 B CN 102256923B
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organic phase
alcohol
reaction system
acid
recycled
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Chinese (zh)
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CN102256923A (zh
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W·迪斯特多尔夫
J·彼得斯
T·沙福尔
K·弗里泽
C·于布勒
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
CN2009801506516A 2008-12-16 2009-12-15 制备羧酸酯的方法 Expired - Fee Related CN102256923B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP08171796.9 2008-12-16
EP08171796 2008-12-16
PCT/EP2009/067177 WO2010076192A1 (de) 2008-12-16 2009-12-15 Verfahren zur herstellung von carbonsäureestern

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CN102256923A CN102256923A (zh) 2011-11-23
CN102256923B true CN102256923B (zh) 2013-12-04

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CN2009801506516A Expired - Fee Related CN102256923B (zh) 2008-12-16 2009-12-15 制备羧酸酯的方法

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US (2) US8901343B2 (enExample)
EP (1) EP2379481B1 (enExample)
JP (1) JP5780967B2 (enExample)
KR (1) KR101757936B1 (enExample)
CN (1) CN102256923B (enExample)
CA (1) CA2746599A1 (enExample)
ES (1) ES2554518T3 (enExample)
MY (1) MY158588A (enExample)
WO (1) WO2010076192A1 (enExample)

Families Citing this family (43)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101967098A (zh) * 2010-09-26 2011-02-09 昆山合峰化工有限公司 邻苯二甲酸二(2-丙基庚)酯的制备方法
CN102001948B (zh) * 2010-10-18 2015-04-15 华侨大学 一种酯化合成对苯二甲酸二异辛酯的方法
DE102011006557A1 (de) * 2011-03-31 2012-10-04 Evonik Oxeno Gmbh Gemisch von Bersteinsäureestern
US9926257B2 (en) 2012-12-11 2018-03-27 Bracco Imaging S.P.A. Continuous process for the preparation of (S)-2-acetyloxypropionic acid chloride
US20150014148A1 (en) * 2013-07-11 2015-01-15 Celanese Acetate Llc Process for Energy Recovery in Manufacturing Cellulose Esters
CN104418747B (zh) * 2013-08-22 2016-08-10 中国科学院大连化学物理研究所 一种制备邻苯二甲酸二（2-丙基庚）酯的方法
TWI654177B (zh) 2013-10-31 2019-03-21 德商巴斯夫歐洲公司 製備羧酸酯的方法及其作爲塑化劑的用途
CN106232571B (zh) 2014-04-22 2019-05-28 巴斯夫欧洲公司 在离子液体和酸性酯化催化剂的存在下制备羧酸酯的方法及其作为塑化剂的用途
LT3154928T (lt) 2014-06-10 2020-05-11 Bracco Imaging S.P.A. (s)-2-acetiloksipropioninės rūgšties ir jos darinių gavimo būdas
EP3160931B1 (en) 2014-06-24 2018-11-14 Dow Global Technologies LLC Process for producing low voc coalescing aids
BR112016029033B1 (pt) 2014-06-24 2021-05-11 Dow Global Technologies Llc processo para a preparação de um éster de éter glicólico
TWI686444B (zh) 2014-09-04 2020-03-01 德商巴斯夫歐洲公司 包含聚合二羧酸酯的塑化劑組成物
US9988338B2 (en) 2014-09-24 2018-06-05 Basf Se Method for producing diesters of terephthalic acid
CA2962305C (en) * 2014-09-24 2019-06-11 Basf Se Method for producing diesters of terephthalic acid with a dehydration of recirculated alcohol
EP3197860A1 (de) 2014-09-24 2017-08-02 Basf Se Verfahren zur herstellung von terephthalsäurediestern mit rückalkohol-anreicherung
PL3197858T3 (pl) 2014-09-24 2019-08-30 Basf Se Sposób wytwarzania diestrów kwasu tereftalowego z cyrkulacją mieszaniny reakcyjnej
KR102138788B1 (ko) 2017-09-07 2020-07-28 주식회사 엘지화학 에스터 조성물의 제조 시스템 및 이를 이용한 에스터 조성물의 제조 방법
WO2019185409A1 (de) 2018-03-29 2019-10-03 Basf Se Pvc-zusammensetzung, enthaltend wenigstens einen weichmacher der wenigstens eine carbonsäureestergruppe aufweist und wenigstens eine carbodiimidverbindung
WO2020173818A1 (de) 2019-02-25 2020-09-03 Basf Se Verfahren zur aufarbeitung von benzolpolycarbonsäureestern und deren verwendung zur herstellung von cyclohexanpolycarbonsäureestern
JP7342320B2 (ja) * 2019-04-04 2023-09-12 エルジー・ケム・リミテッド エステル系組成物の製造方法及び製造システム
CN112955424A (zh) * 2019-04-04 2021-06-11 株式会社Lg化学 酯类组合物的制备方法和制备系统
EP3854774B1 (en) * 2019-04-04 2024-03-20 LG Chem, Ltd. Method for preparing ester-based composition
US11512166B2 (en) 2019-04-04 2022-11-29 Lg Chem, Ltd. Method and system for manufacturing ester-based composition
JP7148036B2 (ja) * 2019-04-04 2022-10-05 エルジー・ケム・リミテッド エステル化反応生成物の連続精製システム
KR102489171B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 물질의 제조 유닛 및 이를 포함하는 디에스터계 물질의 제조 시스템
KR102488351B1 (ko) * 2019-07-04 2023-01-13 주식회사 엘지화학 디에스터계 물질의 연속식 제조방법
KR102489174B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 조성물의 제조 시스템 및 방법
KR102489173B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 열교환 시스템 및 이를 포함하는 디에스터계 조성물 제조 시스템
KR102489172B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 물질의 제조 유닛 및 이를 포함하는 디에스터계 물질의 제조 시스템
CN112239405B (zh) * 2019-07-17 2023-05-02 中国石油化工股份有限公司 2,6-萘二甲酸二甲酯的合成方法
KR102501597B1 (ko) * 2019-09-25 2023-02-20 주식회사 엘지화학 디에스테르계 조성물의 제조 시스템 및 제조방법
KR102595882B1 (ko) * 2019-09-25 2023-10-30 주식회사 엘지화학 디에스터계 조성물의 제조 시스템 및 제조방법
KR102819374B1 (ko) * 2020-08-13 2025-06-11 주식회사 엘지화학 에스터의 제조방법
JP2023534443A (ja) * 2020-09-24 2023-08-09 エルジー・ケム・リミテッド エステル系組成物の製造方法
KR102390132B1 (ko) * 2020-09-24 2022-04-25 주식회사 엘지화학 에스터계 조성물의 제조방법
EP4219442B1 (en) * 2020-09-24 2025-06-04 Lg Chem, Ltd. Method for producing ester-based composition
EP4219440A4 (en) * 2020-09-24 2024-04-10 Lg Chem, Ltd. DISCONTINUOUS PREPARATION PROCESS FOR ESTER-BASED MATERIAL
KR20220067352A (ko) * 2020-11-17 2022-05-24 주식회사 엘지화학 디에스터계 물질의 제조방법
KR102797134B1 (ko) * 2020-11-17 2025-04-21 주식회사 엘지화학 디에스터계 화합물의 제조방법
KR102797150B1 (ko) * 2020-11-17 2025-04-21 주식회사 엘지화학 디에스터계 물질의 제조방법
KR102797136B1 (ko) * 2020-11-17 2025-04-18 주식회사 엘지화학 디에스터계 화합물의 제조방법
CN112439216A (zh) * 2020-12-14 2021-03-05 河南久圣化工有限公司 一种从己二酸废液中回收二元羧酸的三级蒸发系统
CN119657021A (zh) * 2024-12-18 2025-03-21 中国石油化工股份有限公司 一种撬装式邻苯二甲酸二异壬酯合成装置及合成方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020028963A1 (en) * 2000-09-05 2002-03-07 Oxeno Olefinchemie Gmbh Process for preparing carboxylic esters
CN1355780A (zh) * 1999-06-17 2002-06-26 联合碳化化学及塑料技术公司 进行平衡限制反应的方法
CN1400963A (zh) * 2000-02-17 2003-03-05 巴斯福股份公司 制备α,β－不饱和羧酸酯的方法
US20040192957A1 (en) * 2003-03-31 2004-09-30 Wickens Danita Inez Method of recovering 2-ethylhexyl alcohol from a mixture comprising 2-ethylhexyl acrylate

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2648711A (en) * 1949-07-19 1953-08-11 Standard Oil Dev Co Recovery of alcohols from direct hydration of olefins
DE1921110A1 (de) 1969-04-25 1970-11-26 Basf Ag Verfahren zur kontinuierlichen Herstellung von Dicarbonsaeuredialkylestern
IN171820B (enExample) * 1989-12-22 1993-01-16 Lever Hindustan Ltd
GB9102513D0 (en) 1991-02-06 1991-03-27 Exxon Chemical Patents Inc Hydrocarbon production
DE4339713A1 (de) 1993-11-22 1995-05-24 Basf Ag Verfahren zur Oligomerisierung von Olefinen zu hochlinearen Oligomeren und Katalysatoren dafür
DE19955593A1 (de) 1999-11-18 2001-05-23 Basf Ag C13-Alkoholgemisch und funktionalisiertes C13-Alkoholgemisch
US6271410B1 (en) * 2000-06-06 2001-08-07 Creanova Inc. Higher alkyl esters of cyanoacetic acid
DE10149350A1 (de) 2001-10-06 2003-04-17 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
TWI324592B (en) * 2002-11-28 2010-05-11 Sulzer Chemtech Ag A method for the esterification of a fatty acid
JP2007153814A (ja) * 2005-12-06 2007-06-21 Mitsubishi Chemicals Corp ジカルボン酸ジエステルの製造方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1355780A (zh) * 1999-06-17 2002-06-26 联合碳化化学及塑料技术公司 进行平衡限制反应的方法
CN1400963A (zh) * 2000-02-17 2003-03-05 巴斯福股份公司 制备α,β－不饱和羧酸酯的方法
US20020028963A1 (en) * 2000-09-05 2002-03-07 Oxeno Olefinchemie Gmbh Process for preparing carboxylic esters
US20040192957A1 (en) * 2003-03-31 2004-09-30 Wickens Danita Inez Method of recovering 2-ethylhexyl alcohol from a mixture comprising 2-ethylhexyl acrylate

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US20150141691A1 (en) 2015-05-21
JP5780967B2 (ja) 2015-09-16
KR101757936B1 (ko) 2017-07-13
US9260373B2 (en) 2016-02-16
EP2379481B1 (de) 2015-08-26
ES2554518T3 (es) 2015-12-21
US20110251420A1 (en) 2011-10-13
CA2746599A1 (en) 2010-07-08
MY158588A (en) 2016-10-31
EP2379481A1 (de) 2011-10-26
WO2010076192A1 (de) 2010-07-08
KR20110101205A (ko) 2011-09-15
US8901343B2 (en) 2014-12-02
CN102256923A (zh) 2011-11-23
JP2012512229A (ja) 2012-05-31

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