KR101757936B1 - 카르복실산 에스테르의 제조 방법 - Google Patents

카르복실산 에스테르의 제조 방법 Download PDF

Info

Publication number
KR101757936B1
KR101757936B1 KR1020117016501A KR20117016501A KR101757936B1 KR 101757936 B1 KR101757936 B1 KR 101757936B1 KR 1020117016501 A KR1020117016501 A KR 1020117016501A KR 20117016501 A KR20117016501 A KR 20117016501A KR 101757936 B1 KR101757936 B1 KR 101757936B1
Authority
KR
South Korea
Prior art keywords
organic phase
alcohol
acid
recycled
reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1020117016501A
Other languages
English (en)
Korean (ko)
Other versions
KR20110101205A (ko
Inventor
발터 디스텔도르프
자렌 페터스
토마스 샤이퍼
카트린 프리제
크리스토프 위브러
Original Assignee
바스프 에스이
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=42167505&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=KR101757936(B1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by 바스프 에스이 filed Critical 바스프 에스이
Publication of KR20110101205A publication Critical patent/KR20110101205A/ko
Application granted granted Critical
Publication of KR101757936B1 publication Critical patent/KR101757936B1/ko
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
KR1020117016501A 2008-12-16 2009-12-15 카르복실산 에스테르의 제조 방법 Expired - Fee Related KR101757936B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP08171796.9 2008-12-16
EP08171796 2008-12-16
PCT/EP2009/067177 WO2010076192A1 (de) 2008-12-16 2009-12-15 Verfahren zur herstellung von carbonsäureestern

Publications (2)

Publication Number Publication Date
KR20110101205A KR20110101205A (ko) 2011-09-15
KR101757936B1 true KR101757936B1 (ko) 2017-07-13

Family

ID=42167505

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020117016501A Expired - Fee Related KR101757936B1 (ko) 2008-12-16 2009-12-15 카르복실산 에스테르의 제조 방법

Country Status (9)

Country Link
US (2) US8901343B2 (enExample)
EP (1) EP2379481B1 (enExample)
JP (1) JP5780967B2 (enExample)
KR (1) KR101757936B1 (enExample)
CN (1) CN102256923B (enExample)
CA (1) CA2746599A1 (enExample)
ES (1) ES2554518T3 (enExample)
MY (1) MY158588A (enExample)
WO (1) WO2010076192A1 (enExample)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102162205B1 (ko) * 2019-04-04 2020-10-06 주식회사 엘지화학 에스터화 반응 생성물의 연속 정제 시스템
KR102162204B1 (ko) * 2019-04-04 2020-10-06 주식회사 엘지화학 에스터계 조성물의 제조방법 및 제조 시스템
KR20220021253A (ko) * 2020-08-13 2022-02-22 주식회사 엘지화학 에스터의 제조방법

Families Citing this family (40)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101967098A (zh) * 2010-09-26 2011-02-09 昆山合峰化工有限公司 邻苯二甲酸二(2-丙基庚)酯的制备方法
CN102001948B (zh) * 2010-10-18 2015-04-15 华侨大学 一种酯化合成对苯二甲酸二异辛酯的方法
DE102011006557A1 (de) * 2011-03-31 2012-10-04 Evonik Oxeno Gmbh Gemisch von Bersteinsäureestern
US9926257B2 (en) 2012-12-11 2018-03-27 Bracco Imaging S.P.A. Continuous process for the preparation of (S)-2-acetyloxypropionic acid chloride
US20150014148A1 (en) * 2013-07-11 2015-01-15 Celanese Acetate Llc Process for Energy Recovery in Manufacturing Cellulose Esters
CN104418747B (zh) * 2013-08-22 2016-08-10 中国科学院大连化学物理研究所 一种制备邻苯二甲酸二（2-丙基庚）酯的方法
TWI654177B (zh) 2013-10-31 2019-03-21 德商巴斯夫歐洲公司 製備羧酸酯的方法及其作爲塑化劑的用途
CN106232571B (zh) 2014-04-22 2019-05-28 巴斯夫欧洲公司 在离子液体和酸性酯化催化剂的存在下制备羧酸酯的方法及其作为塑化剂的用途
LT3154928T (lt) 2014-06-10 2020-05-11 Bracco Imaging S.P.A. (s)-2-acetiloksipropioninės rūgšties ir jos darinių gavimo būdas
EP3160931B1 (en) 2014-06-24 2018-11-14 Dow Global Technologies LLC Process for producing low voc coalescing aids
BR112016029033B1 (pt) 2014-06-24 2021-05-11 Dow Global Technologies Llc processo para a preparação de um éster de éter glicólico
TWI686444B (zh) 2014-09-04 2020-03-01 德商巴斯夫歐洲公司 包含聚合二羧酸酯的塑化劑組成物
US9988338B2 (en) 2014-09-24 2018-06-05 Basf Se Method for producing diesters of terephthalic acid
CA2962305C (en) * 2014-09-24 2019-06-11 Basf Se Method for producing diesters of terephthalic acid with a dehydration of recirculated alcohol
EP3197860A1 (de) 2014-09-24 2017-08-02 Basf Se Verfahren zur herstellung von terephthalsäurediestern mit rückalkohol-anreicherung
PL3197858T3 (pl) 2014-09-24 2019-08-30 Basf Se Sposób wytwarzania diestrów kwasu tereftalowego z cyrkulacją mieszaniny reakcyjnej
KR102138788B1 (ko) 2017-09-07 2020-07-28 주식회사 엘지화학 에스터 조성물의 제조 시스템 및 이를 이용한 에스터 조성물의 제조 방법
WO2019185409A1 (de) 2018-03-29 2019-10-03 Basf Se Pvc-zusammensetzung, enthaltend wenigstens einen weichmacher der wenigstens eine carbonsäureestergruppe aufweist und wenigstens eine carbodiimidverbindung
WO2020173818A1 (de) 2019-02-25 2020-09-03 Basf Se Verfahren zur aufarbeitung von benzolpolycarbonsäureestern und deren verwendung zur herstellung von cyclohexanpolycarbonsäureestern
CN112955424A (zh) * 2019-04-04 2021-06-11 株式会社Lg化学 酯类组合物的制备方法和制备系统
EP3854774B1 (en) * 2019-04-04 2024-03-20 LG Chem, Ltd. Method for preparing ester-based composition
US11512166B2 (en) 2019-04-04 2022-11-29 Lg Chem, Ltd. Method and system for manufacturing ester-based composition
KR102489171B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 물질의 제조 유닛 및 이를 포함하는 디에스터계 물질의 제조 시스템
KR102488351B1 (ko) * 2019-07-04 2023-01-13 주식회사 엘지화학 디에스터계 물질의 연속식 제조방법
KR102489174B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 조성물의 제조 시스템 및 방법
KR102489173B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 열교환 시스템 및 이를 포함하는 디에스터계 조성물 제조 시스템
KR102489172B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 물질의 제조 유닛 및 이를 포함하는 디에스터계 물질의 제조 시스템
CN112239405B (zh) * 2019-07-17 2023-05-02 中国石油化工股份有限公司 2,6-萘二甲酸二甲酯的合成方法
KR102501597B1 (ko) * 2019-09-25 2023-02-20 주식회사 엘지화학 디에스테르계 조성물의 제조 시스템 및 제조방법
KR102595882B1 (ko) * 2019-09-25 2023-10-30 주식회사 엘지화학 디에스터계 조성물의 제조 시스템 및 제조방법
JP2023534443A (ja) * 2020-09-24 2023-08-09 エルジー・ケム・リミテッド エステル系組成物の製造方法
KR102390132B1 (ko) * 2020-09-24 2022-04-25 주식회사 엘지화학 에스터계 조성물의 제조방법
EP4219442B1 (en) * 2020-09-24 2025-06-04 Lg Chem, Ltd. Method for producing ester-based composition
EP4219440A4 (en) * 2020-09-24 2024-04-10 Lg Chem, Ltd. DISCONTINUOUS PREPARATION PROCESS FOR ESTER-BASED MATERIAL
KR20220067352A (ko) * 2020-11-17 2022-05-24 주식회사 엘지화학 디에스터계 물질의 제조방법
KR102797134B1 (ko) * 2020-11-17 2025-04-21 주식회사 엘지화학 디에스터계 화합물의 제조방법
KR102797150B1 (ko) * 2020-11-17 2025-04-21 주식회사 엘지화학 디에스터계 물질의 제조방법
KR102797136B1 (ko) * 2020-11-17 2025-04-18 주식회사 엘지화학 디에스터계 화합물의 제조방법
CN112439216A (zh) * 2020-12-14 2021-03-05 河南久圣化工有限公司 一种从己二酸废液中回收二元羧酸的三级蒸发系统
CN119657021A (zh) * 2024-12-18 2025-03-21 中国石油化工股份有限公司 一种撬装式邻苯二甲酸二异壬酯合成装置及合成方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007153814A (ja) 2005-12-06 2007-06-21 Mitsubishi Chemicals Corp ジカルボン酸ジエステルの製造方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2648711A (en) * 1949-07-19 1953-08-11 Standard Oil Dev Co Recovery of alcohols from direct hydration of olefins
DE1921110A1 (de) 1969-04-25 1970-11-26 Basf Ag Verfahren zur kontinuierlichen Herstellung von Dicarbonsaeuredialkylestern
IN171820B (enExample) * 1989-12-22 1993-01-16 Lever Hindustan Ltd
GB9102513D0 (en) 1991-02-06 1991-03-27 Exxon Chemical Patents Inc Hydrocarbon production
DE4339713A1 (de) 1993-11-22 1995-05-24 Basf Ag Verfahren zur Oligomerisierung von Olefinen zu hochlinearen Oligomeren und Katalysatoren dafür
CN100347146C (zh) * 1999-06-17 2007-11-07 联合碳化化学及塑料技术公司 进行平衡限制反应的方法
DE19955593A1 (de) 1999-11-18 2001-05-23 Basf Ag C13-Alkoholgemisch und funktionalisiertes C13-Alkoholgemisch
DE10007213A1 (de) * 2000-02-17 2001-08-23 Basf Ag Verfahren zur Herstellung von Estern alpha,beta-ungesättigter Carbonsäuren
US6271410B1 (en) * 2000-06-06 2001-08-07 Creanova Inc. Higher alkyl esters of cyanoacetic acid
DE10043545A1 (de) * 2000-09-05 2002-03-14 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
DE10149350A1 (de) 2001-10-06 2003-04-17 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
TWI324592B (en) * 2002-11-28 2010-05-11 Sulzer Chemtech Ag A method for the esterification of a fatty acid
US20040192957A1 (en) * 2003-03-31 2004-09-30 Wickens Danita Inez Method of recovering 2-ethylhexyl alcohol from a mixture comprising 2-ethylhexyl acrylate

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007153814A (ja) 2005-12-06 2007-06-21 Mitsubishi Chemicals Corp ジカルボン酸ジエステルの製造方法

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102162205B1 (ko) * 2019-04-04 2020-10-06 주식회사 엘지화학 에스터화 반응 생성물의 연속 정제 시스템
KR102162204B1 (ko) * 2019-04-04 2020-10-06 주식회사 엘지화학 에스터계 조성물의 제조방법 및 제조 시스템
KR20220021253A (ko) * 2020-08-13 2022-02-22 주식회사 엘지화학 에스터의 제조방법
KR102819374B1 (ko) 2020-08-13 2025-06-11 주식회사 엘지화학 에스터의 제조방법

Also Published As

Publication number Publication date
US20150141691A1 (en) 2015-05-21
JP5780967B2 (ja) 2015-09-16
US9260373B2 (en) 2016-02-16
EP2379481B1 (de) 2015-08-26
ES2554518T3 (es) 2015-12-21
US20110251420A1 (en) 2011-10-13
CN102256923B (zh) 2013-12-04
CA2746599A1 (en) 2010-07-08
MY158588A (en) 2016-10-31
EP2379481A1 (de) 2011-10-26
WO2010076192A1 (de) 2010-07-08
KR20110101205A (ko) 2011-09-15
US8901343B2 (en) 2014-12-02
CN102256923A (zh) 2011-11-23
JP2012512229A (ja) 2012-05-31

Similar Documents

Publication Publication Date Title
KR101757936B1 (ko) 카르복실산 에스테르의 제조 방법
KR101733814B1 (ko) 알콜 증기를 사용하는 스트립핑에 의한 카르복실산 에스테르의 제조
KR100853632B1 (ko) 카복실산 에스테르의 제조방법
US8729292B2 (en) Method for regeneration of raw ester
EP3197859B1 (de) Verfahren zur herstellung von terephthalsäurediestern mit rückalkohol-entwässerung
PL205694B1 (pl) Sposób wytwarzania estrów kwasów karboksylowych
EP1719753B1 (de) Verfahren zur Herstellung von Carbonsäureestern

Legal Events

Date Code Title Description
E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
AMND Amendment
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

P22-X000 Classification modified

St.27 status event code: A-2-2-P10-P22-nap-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

AMND Amendment
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E601 Decision to refuse application
PE0601 Decision on rejection of patent

St.27 status event code: N-2-6-B10-B15-exm-PE0601

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

T13-X000 Administrative time limit extension granted

St.27 status event code: U-3-3-T10-T13-oth-X000

AMND Amendment
E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PX0901 Re-examination

St.27 status event code: A-2-3-E10-E12-rex-PX0901

PX0701 Decision of registration after re-examination

St.27 status event code: A-3-4-F10-F13-rex-PX0701

X701 Decision to grant (after re-examination)
GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20200708

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20200708

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000