JP5780967B2 - カルボン酸エステルの製造方法 - Google Patents

カルボン酸エステルの製造方法

Info

Publication number
JP5780967B2
JP5780967B2 JP2011541389A JP2011541389A JP5780967B2 JP 5780967 B2 JP5780967 B2 JP 5780967B2 JP 2011541389 A JP2011541389 A JP 2011541389A JP 2011541389 A JP2011541389 A JP 2011541389A JP 5780967 B2 JP5780967 B2 JP 5780967B2
Authority
JP
Japan
Prior art keywords
alcohol
reactor
acid
organic phase
carboxylic acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2011541389A
Other languages
English (en)
Japanese (ja)
Other versions
JP2012512229A5 (enExample
JP2012512229A (ja
Inventor
ヴァルター　ディステルドルフ
ディステルドルフ ヴァルター
ペータース ヤレン
ペータース ヤレン
シェーファー トーマス
シェーファー トーマス
フリーゼ カトリン
フリーゼ カトリン
イュープラー クリストフ
イュープラー クリストフ
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=42167505&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=JP5780967(B2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by BASF SE filed Critical BASF SE
Publication of JP2012512229A publication Critical patent/JP2012512229A/ja
Publication of JP2012512229A5 publication Critical patent/JP2012512229A5/ja
Application granted granted Critical
Publication of JP5780967B2 publication Critical patent/JP5780967B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0042—Essential oils; Perfumes compounds containing condensed hydrocarbon rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
JP2011541389A 2008-12-16 2009-12-15 カルボン酸エステルの製造方法 Expired - Fee Related JP5780967B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP08171796.9 2008-12-16
EP08171796 2008-12-16
PCT/EP2009/067177 WO2010076192A1 (de) 2008-12-16 2009-12-15 Verfahren zur herstellung von carbonsäureestern

Publications (3)

Publication Number Publication Date
JP2012512229A JP2012512229A (ja) 2012-05-31
JP2012512229A5 JP2012512229A5 (enExample) 2015-04-30
JP5780967B2 true JP5780967B2 (ja) 2015-09-16

Family

ID=42167505

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2011541389A Expired - Fee Related JP5780967B2 (ja) 2008-12-16 2009-12-15 カルボン酸エステルの製造方法

Country Status (9)

Country Link
US (2) US8901343B2 (enExample)
EP (1) EP2379481B1 (enExample)
JP (1) JP5780967B2 (enExample)
KR (1) KR101757936B1 (enExample)
CN (1) CN102256923B (enExample)
CA (1) CA2746599A1 (enExample)
ES (1) ES2554518T3 (enExample)
MY (1) MY158588A (enExample)
WO (1) WO2010076192A1 (enExample)

Families Citing this family (43)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101967098A (zh) * 2010-09-26 2011-02-09 昆山合峰化工有限公司 邻苯二甲酸二(2-丙基庚)酯的制备方法
CN102001948B (zh) * 2010-10-18 2015-04-15 华侨大学 一种酯化合成对苯二甲酸二异辛酯的方法
DE102011006557A1 (de) * 2011-03-31 2012-10-04 Evonik Oxeno Gmbh Gemisch von Bersteinsäureestern
US9926257B2 (en) 2012-12-11 2018-03-27 Bracco Imaging S.P.A. Continuous process for the preparation of (S)-2-acetyloxypropionic acid chloride
US20150014148A1 (en) * 2013-07-11 2015-01-15 Celanese Acetate Llc Process for Energy Recovery in Manufacturing Cellulose Esters
CN104418747B (zh) * 2013-08-22 2016-08-10 中国科学院大连化学物理研究所 一种制备邻苯二甲酸二（2-丙基庚）酯的方法
TWI654177B (zh) 2013-10-31 2019-03-21 德商巴斯夫歐洲公司 製備羧酸酯的方法及其作爲塑化劑的用途
CN106232571B (zh) 2014-04-22 2019-05-28 巴斯夫欧洲公司 在离子液体和酸性酯化催化剂的存在下制备羧酸酯的方法及其作为塑化剂的用途
LT3154928T (lt) 2014-06-10 2020-05-11 Bracco Imaging S.P.A. (s)-2-acetiloksipropioninės rūgšties ir jos darinių gavimo būdas
EP3160931B1 (en) 2014-06-24 2018-11-14 Dow Global Technologies LLC Process for producing low voc coalescing aids
BR112016029033B1 (pt) 2014-06-24 2021-05-11 Dow Global Technologies Llc processo para a preparação de um éster de éter glicólico
TWI686444B (zh) 2014-09-04 2020-03-01 德商巴斯夫歐洲公司 包含聚合二羧酸酯的塑化劑組成物
US9988338B2 (en) 2014-09-24 2018-06-05 Basf Se Method for producing diesters of terephthalic acid
CA2962305C (en) * 2014-09-24 2019-06-11 Basf Se Method for producing diesters of terephthalic acid with a dehydration of recirculated alcohol
EP3197860A1 (de) 2014-09-24 2017-08-02 Basf Se Verfahren zur herstellung von terephthalsäurediestern mit rückalkohol-anreicherung
PL3197858T3 (pl) 2014-09-24 2019-08-30 Basf Se Sposób wytwarzania diestrów kwasu tereftalowego z cyrkulacją mieszaniny reakcyjnej
KR102138788B1 (ko) 2017-09-07 2020-07-28 주식회사 엘지화학 에스터 조성물의 제조 시스템 및 이를 이용한 에스터 조성물의 제조 방법
WO2019185409A1 (de) 2018-03-29 2019-10-03 Basf Se Pvc-zusammensetzung, enthaltend wenigstens einen weichmacher der wenigstens eine carbonsäureestergruppe aufweist und wenigstens eine carbodiimidverbindung
WO2020173818A1 (de) 2019-02-25 2020-09-03 Basf Se Verfahren zur aufarbeitung von benzolpolycarbonsäureestern und deren verwendung zur herstellung von cyclohexanpolycarbonsäureestern
JP7342320B2 (ja) * 2019-04-04 2023-09-12 エルジー・ケム・リミテッド エステル系組成物の製造方法及び製造システム
CN112955424A (zh) * 2019-04-04 2021-06-11 株式会社Lg化学 酯类组合物的制备方法和制备系统
EP3854774B1 (en) * 2019-04-04 2024-03-20 LG Chem, Ltd. Method for preparing ester-based composition
US11512166B2 (en) 2019-04-04 2022-11-29 Lg Chem, Ltd. Method and system for manufacturing ester-based composition
JP7148036B2 (ja) * 2019-04-04 2022-10-05 エルジー・ケム・リミテッド エステル化反応生成物の連続精製システム
KR102489171B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 물질의 제조 유닛 및 이를 포함하는 디에스터계 물질의 제조 시스템
KR102488351B1 (ko) * 2019-07-04 2023-01-13 주식회사 엘지화학 디에스터계 물질의 연속식 제조방법
KR102489174B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 조성물의 제조 시스템 및 방법
KR102489173B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 열교환 시스템 및 이를 포함하는 디에스터계 조성물 제조 시스템
KR102489172B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 물질의 제조 유닛 및 이를 포함하는 디에스터계 물질의 제조 시스템
CN112239405B (zh) * 2019-07-17 2023-05-02 中国石油化工股份有限公司 2,6-萘二甲酸二甲酯的合成方法
KR102501597B1 (ko) * 2019-09-25 2023-02-20 주식회사 엘지화학 디에스테르계 조성물의 제조 시스템 및 제조방법
KR102595882B1 (ko) * 2019-09-25 2023-10-30 주식회사 엘지화학 디에스터계 조성물의 제조 시스템 및 제조방법
KR102819374B1 (ko) * 2020-08-13 2025-06-11 주식회사 엘지화학 에스터의 제조방법
JP2023534443A (ja) * 2020-09-24 2023-08-09 エルジー・ケム・リミテッド エステル系組成物の製造方法
KR102390132B1 (ko) * 2020-09-24 2022-04-25 주식회사 엘지화학 에스터계 조성물의 제조방법
EP4219442B1 (en) * 2020-09-24 2025-06-04 Lg Chem, Ltd. Method for producing ester-based composition
EP4219440A4 (en) * 2020-09-24 2024-04-10 Lg Chem, Ltd. DISCONTINUOUS PREPARATION PROCESS FOR ESTER-BASED MATERIAL
KR20220067352A (ko) * 2020-11-17 2022-05-24 주식회사 엘지화학 디에스터계 물질의 제조방법
KR102797134B1 (ko) * 2020-11-17 2025-04-21 주식회사 엘지화학 디에스터계 화합물의 제조방법
KR102797150B1 (ko) * 2020-11-17 2025-04-21 주식회사 엘지화학 디에스터계 물질의 제조방법
KR102797136B1 (ko) * 2020-11-17 2025-04-18 주식회사 엘지화학 디에스터계 화합물의 제조방법
CN112439216A (zh) * 2020-12-14 2021-03-05 河南久圣化工有限公司 一种从己二酸废液中回收二元羧酸的三级蒸发系统
CN119657021A (zh) * 2024-12-18 2025-03-21 中国石油化工股份有限公司 一种撬装式邻苯二甲酸二异壬酯合成装置及合成方法

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2648711A (en) * 1949-07-19 1953-08-11 Standard Oil Dev Co Recovery of alcohols from direct hydration of olefins
DE1921110A1 (de) 1969-04-25 1970-11-26 Basf Ag Verfahren zur kontinuierlichen Herstellung von Dicarbonsaeuredialkylestern
IN171820B (enExample) * 1989-12-22 1993-01-16 Lever Hindustan Ltd
GB9102513D0 (en) 1991-02-06 1991-03-27 Exxon Chemical Patents Inc Hydrocarbon production
DE4339713A1 (de) 1993-11-22 1995-05-24 Basf Ag Verfahren zur Oligomerisierung von Olefinen zu hochlinearen Oligomeren und Katalysatoren dafür
CN100347146C (zh) * 1999-06-17 2007-11-07 联合碳化化学及塑料技术公司 进行平衡限制反应的方法
DE19955593A1 (de) 1999-11-18 2001-05-23 Basf Ag C13-Alkoholgemisch und funktionalisiertes C13-Alkoholgemisch
DE10007213A1 (de) * 2000-02-17 2001-08-23 Basf Ag Verfahren zur Herstellung von Estern alpha,beta-ungesättigter Carbonsäuren
US6271410B1 (en) * 2000-06-06 2001-08-07 Creanova Inc. Higher alkyl esters of cyanoacetic acid
DE10043545A1 (de) * 2000-09-05 2002-03-14 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
DE10149350A1 (de) 2001-10-06 2003-04-17 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von Carbonsäureestern
TWI324592B (en) * 2002-11-28 2010-05-11 Sulzer Chemtech Ag A method for the esterification of a fatty acid
US20040192957A1 (en) * 2003-03-31 2004-09-30 Wickens Danita Inez Method of recovering 2-ethylhexyl alcohol from a mixture comprising 2-ethylhexyl acrylate
JP2007153814A (ja) * 2005-12-06 2007-06-21 Mitsubishi Chemicals Corp ジカルボン酸ジエステルの製造方法

Also Published As

Publication number Publication date
US20150141691A1 (en) 2015-05-21
KR101757936B1 (ko) 2017-07-13
US9260373B2 (en) 2016-02-16
EP2379481B1 (de) 2015-08-26
ES2554518T3 (es) 2015-12-21
US20110251420A1 (en) 2011-10-13
CN102256923B (zh) 2013-12-04
CA2746599A1 (en) 2010-07-08
MY158588A (en) 2016-10-31
EP2379481A1 (de) 2011-10-26
WO2010076192A1 (de) 2010-07-08
KR20110101205A (ko) 2011-09-15
US8901343B2 (en) 2014-12-02
CN102256923A (zh) 2011-11-23
JP2012512229A (ja) 2012-05-31

Similar Documents

Publication Publication Date Title
JP5780967B2 (ja) カルボン酸エステルの製造方法
JP5698146B2 (ja) アルコール蒸気によるストリッピング下にカルボン酸エステルを製造する方法
KR100853632B1 (ko) 카복실산 에스테르의 제조방법
PL204384B1 (pl) Sposób wytwarzania estrów
US8729292B2 (en) Method for regeneration of raw ester
CZ33697A3 (cs) Kontinuální příprava alkylesterů kyseliny (meth)akrylové
EP3218359B1 (en) Preparation of dialkyl esters of 2,5-furandicarboxylic acid
PL205694B1 (pl) Sposób wytwarzania estrów kwasów karboksylowych
JP5059400B2 (ja) 平衡制限反応の実施方法

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20121212

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20140206

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20140310

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20140609

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20150126

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20150313

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20150615

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20150714

R150 Certificate of patent or registration of utility model

Ref document number: 5780967

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

LAPS Cancellation because of no payment of annual fees