CN102123943B - 制备包含锂、钒和磷酸根的多孔材料的方法 - Google Patents

制备包含锂、钒和磷酸根的多孔材料的方法 Download PDF

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Publication number
CN102123943B
CN102123943B CN2008801186284A CN200880118628A CN102123943B CN 102123943 B CN102123943 B CN 102123943B CN 2008801186284 A CN2008801186284 A CN 2008801186284A CN 200880118628 A CN200880118628 A CN 200880118628A CN 102123943 B CN102123943 B CN 102123943B
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compound
gaseous
oxidation state
mixture
vanadium
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Chinese (zh)
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CN102123943A (zh
Inventor
H·希布施特
B·罗伯茨
J·兰伯特
K·布拉姆尼克
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/45—Phosphates containing plural metal, or metal and ammonium
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/136—Electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Secondary Cells (AREA)
CN2008801186284A 2007-10-01 2008-09-18 制备包含锂、钒和磷酸根的多孔材料的方法 Expired - Fee Related CN102123943B (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US97664007P 2007-10-01 2007-10-01
US60/976,640 2007-10-01
US2463108P 2008-01-30 2008-01-30
US61/024,631 2008-01-30
PCT/EP2008/062427 WO2009043729A2 (en) 2007-10-01 2008-09-18 Process for the preparation of porous lithium-, vanadium and phosphate-comprising materials

Publications (2)

Publication Number Publication Date
CN102123943A CN102123943A (zh) 2011-07-13
CN102123943B true CN102123943B (zh) 2013-07-10

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CN2008801186284A Expired - Fee Related CN102123943B (zh) 2007-10-01 2008-09-18 制备包含锂、钒和磷酸根的多孔材料的方法

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Country Link
US (3) US20100301281A1 (enExample)
EP (1) EP2207751B1 (enExample)
JP (1) JP5702145B2 (enExample)
KR (1) KR101540133B1 (enExample)
CN (1) CN102123943B (enExample)
CA (1) CA2701144A1 (enExample)
TW (1) TWI401207B (enExample)
WO (1) WO2009043729A2 (enExample)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW200951066A (en) * 2008-04-17 2009-12-16 Basf Se Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials
TW201010944A (en) 2008-04-17 2010-03-16 Basf Se Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials
KR20110139281A (ko) 2009-03-17 2011-12-28 바스프 에스이 열수 조건 하의 리튬-철-포스페이트의 합성 방법
EP2445834B1 (en) 2009-06-24 2020-04-01 Advanced Lithium Electrochemistry Co., Ltd. Process for the preparation of lifepo4-carbon composites
KR101939415B1 (ko) * 2010-09-27 2019-01-16 니폰 가가쿠 고교 가부시키가이샤 인산바나듐리튬 탄소 복합체의 제조 방법
US20140004473A1 (en) * 2011-03-16 2014-01-02 Hanwha Chemical Corporation Method for calcining electrode materials using a rotary kiln
CN102569797B (zh) * 2012-01-20 2015-04-29 中国科学院宁波材料技术与工程研究所 一种新型磷酸盐基正极复合材料及其制备方法和用途
CN102544497A (zh) * 2012-03-08 2012-07-04 苏州大学 用于锂离子二次电池的正极材料及其制备方法、锂离子二次电池正极和锂离子二次电池
FR2989378B1 (fr) 2012-04-16 2015-10-02 Commissariat Energie Atomique Polymere comme materiau d'electrode pour des batteries secondaires au lithium.
FR3012450B1 (fr) 2013-10-30 2017-10-13 Commissariat Energie Atomique Materiau d'electrode pour batterie organique
CN105118968B (zh) * 2015-09-29 2018-10-16 中南大学 一种巢状v2o3包覆磷酸钒锂的锂离子正极材料
CN105470479B (zh) * 2015-11-26 2017-12-01 中南大学 一种改性的磷酸锰锂复合正极材料及其制备方法
CN106784597A (zh) * 2016-12-19 2017-05-31 苏州格瑞动力电源科技有限公司 一种锂离子电池电极片的制备方法
US11909046B2 (en) 2017-03-07 2024-02-20 The Research Foundation For The State University Of New York Synthetic methods for crystallite size control of bimetallic polyanionic battery compositions
US11251430B2 (en) 2018-03-05 2022-02-15 The Research Foundation For The State University Of New York ϵ-VOPO4 cathode for lithium ion batteries
CN108963235B (zh) * 2018-08-01 2021-07-23 武汉理工大学 石墨烯增强碳包覆磷酸钛锰钠微米球电极材料及其制备方法和应用

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6203946B1 (en) * 1998-12-03 2001-03-20 Valence Technology, Inc. Lithium-containing phosphates, method of preparation, and uses thereof
CN1677718A (zh) * 2004-03-30 2005-10-05 中国科学院物理研究所 一种锂离子电池的磷酸盐正极材料的制备方法
CN1785798A (zh) * 2005-12-19 2006-06-14 南开大学 溶胶凝胶法合成锂离子电池正极材料磷酸钒锂

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4567158A (en) * 1983-12-28 1986-01-28 Monsanto Company Process for preparing phosphorus-vanadium mixed oxide oxidation catalysts
US5102836A (en) * 1990-06-06 1992-04-07 Center For Innovative Technology Ceramic materials with low thermal conductivity and low coefficients of thermal expansion
US5910382A (en) * 1996-04-23 1999-06-08 Board Of Regents, University Of Texas Systems Cathode materials for secondary (rechargeable) lithium batteries
US5871866A (en) * 1996-09-23 1999-02-16 Valence Technology, Inc. Lithium-containing phosphates, method of preparation, and use thereof
JP2949229B1 (ja) * 1998-09-16 1999-09-13 大阪大学長 燐酸リチウム・バナジウム複合化合物及び同複合化合物からなるリチウムイオン二次電池用正極材料
US6528033B1 (en) * 2000-01-18 2003-03-04 Valence Technology, Inc. Method of making lithium-containing materials
US7001690B2 (en) * 2000-01-18 2006-02-21 Valence Technology, Inc. Lithium-based active materials and preparation thereof
US6777132B2 (en) * 2000-04-27 2004-08-17 Valence Technology, Inc. Alkali/transition metal halo—and hydroxy-phosphates and related electrode active materials
FR2852148B1 (fr) 2003-03-07 2014-04-11 Batscap Sa Materiau pour electrode composite, procede pour sa preparation
US20040202935A1 (en) * 2003-04-08 2004-10-14 Jeremy Barker Cathode active material with increased alkali/metal content and method of making same
JP4794833B2 (ja) * 2004-07-21 2011-10-19 日本コークス工業株式会社 リチウムイオン二次電池用正極材料、その製造方法、及びリチウムイオン二次電池
WO2006116251A2 (en) * 2005-04-26 2006-11-02 The University Of Chicago Processes for making dense, spherical, active materials for lithium-ion cells
TWI254031B (en) * 2005-05-10 2006-05-01 Aquire Energy Co Ltd Manufacturing method of LixMyPO4 compound with olivine structure
WO2007034823A1 (ja) * 2005-09-21 2007-03-29 Kanto Denka Kogyo Co., Ltd. 正極活物質の製造方法およびそれを用いた非水電解質電池
US8491861B2 (en) * 2006-05-26 2013-07-23 Eltron Research, Inc. Synthetic process for preparation of high surface area electroactive compounds for battery applications
JP4926607B2 (ja) * 2006-08-23 2012-05-09 住友大阪セメント株式会社 電極材料の製造方法及び正極材料並びに電池
US20100133467A1 (en) * 2007-02-28 2010-06-03 Santoku Corporation Compound having olivine-type structure, positive electrode for nonaqueous electrolyte secondary battery, and nonaqueous electrolyte secondary battery
JP5182626B2 (ja) * 2007-06-29 2013-04-17 株式会社Ｇｓユアサ 正極活物質および非水電解質電池
TW200951066A (en) * 2008-04-17 2009-12-16 Basf Se Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials
KR20110139281A (ko) * 2009-03-17 2011-12-28 바스프 에스이 열수 조건 하의 리튬-철-포스페이트의 합성 방법

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6203946B1 (en) * 1998-12-03 2001-03-20 Valence Technology, Inc. Lithium-containing phosphates, method of preparation, and uses thereof
CN1677718A (zh) * 2004-03-30 2005-10-05 中国科学院物理研究所 一种锂离子电池的磷酸盐正极材料的制备方法
CN1785798A (zh) * 2005-12-19 2006-06-14 南开大学 溶胶凝胶法合成锂离子电池正极材料磷酸钒锂

Also Published As

Publication number Publication date
KR20100091954A (ko) 2010-08-19
TW200930660A (en) 2009-07-16
WO2009043729A3 (en) 2009-10-29
US8808576B2 (en) 2014-08-19
JP5702145B2 (ja) 2015-04-15
US20130214201A1 (en) 2013-08-22
JP2010540393A (ja) 2010-12-24
KR101540133B1 (ko) 2015-07-28
WO2009043729A2 (en) 2009-04-09
EP2207751A2 (en) 2010-07-21
US20100301281A1 (en) 2010-12-02
CN102123943A (zh) 2011-07-13
US8808575B2 (en) 2014-08-19
CA2701144A1 (en) 2009-04-09
US20130214212A1 (en) 2013-08-22
EP2207751B1 (en) 2013-07-03
TWI401207B (zh) 2013-07-11

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