JP5702145B2 - リチウム、バナジウム、及びフォスフェイトを含有する化合物、及び該化合物と導電性材料を含む混合物を製造するための方法 - Google Patents

リチウム、バナジウム、及びフォスフェイトを含有する化合物、及び該化合物と導電性材料を含む混合物を製造するための方法 Download PDF

Info

Publication number
JP5702145B2
JP5702145B2 JP2010527394A JP2010527394A JP5702145B2 JP 5702145 B2 JP5702145 B2 JP 5702145B2 JP 2010527394 A JP2010527394 A JP 2010527394A JP 2010527394 A JP2010527394 A JP 2010527394A JP 5702145 B2 JP5702145 B2 JP 5702145B2
Authority
JP
Japan
Prior art keywords
compound
gaseous
oxidation state
mixture
vanadium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2010527394A
Other languages
English (en)
Japanese (ja)
Other versions
JP2010540393A5 (enExample
JP2010540393A (ja
Inventor
ヒプスト，ハルトムート
ロバーツ，ブライアン
ラムペルト，ヨルダン
ブラムニク，キリル
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JP2010540393A publication Critical patent/JP2010540393A/ja
Publication of JP2010540393A5 publication Critical patent/JP2010540393A5/ja
Application granted granted Critical
Publication of JP5702145B2 publication Critical patent/JP5702145B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/45—Phosphates containing plural metal, or metal and ammonium
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/136—Electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Secondary Cells (AREA)
JP2010527394A 2007-10-01 2008-09-18 リチウム、バナジウム、及びフォスフェイトを含有する化合物、及び該化合物と導電性材料を含む混合物を製造するための方法 Expired - Fee Related JP5702145B2 (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US97664007P 2007-10-01 2007-10-01
US60/976,640 2007-10-01
US2463108P 2008-01-30 2008-01-30
US61/024,631 2008-01-30
PCT/EP2008/062427 WO2009043729A2 (en) 2007-10-01 2008-09-18 Process for the preparation of porous lithium-, vanadium and phosphate-comprising materials

Publications (3)

Publication Number Publication Date
JP2010540393A JP2010540393A (ja) 2010-12-24
JP2010540393A5 JP2010540393A5 (enExample) 2011-10-27
JP5702145B2 true JP5702145B2 (ja) 2015-04-15

Family

ID=40457750

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2010527394A Expired - Fee Related JP5702145B2 (ja) 2007-10-01 2008-09-18 リチウム、バナジウム、及びフォスフェイトを含有する化合物、及び該化合物と導電性材料を含む混合物を製造するための方法

Country Status (8)

Country Link
US (3) US20100301281A1 (enExample)
EP (1) EP2207751B1 (enExample)
JP (1) JP5702145B2 (enExample)
KR (1) KR101540133B1 (enExample)
CN (1) CN102123943B (enExample)
CA (1) CA2701144A1 (enExample)
TW (1) TWI401207B (enExample)
WO (1) WO2009043729A2 (enExample)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW201010944A (en) 2008-04-17 2010-03-16 Basf Se Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials
TW200951066A (en) * 2008-04-17 2009-12-16 Basf Se Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials
TW201038469A (en) 2009-03-17 2010-11-01 Basf Se Synthesis of lithium-iron-phosphates
US9209461B2 (en) 2009-06-24 2015-12-08 Basf Se Process for the preparation of LiFePO4-carbon composites
KR101939415B1 (ko) * 2010-09-27 2019-01-16 니폰 가가쿠 고교 가부시키가이샤 인산바나듐리튬 탄소 복합체의 제조 방법
WO2012124990A2 (ko) * 2011-03-16 2012-09-20 한화케미칼 주식회사 로타리 킬른을 이용한 전극물질의 하소 방법
CN102569797B (zh) * 2012-01-20 2015-04-29 中国科学院宁波材料技术与工程研究所 一种新型磷酸盐基正极复合材料及其制备方法和用途
CN102544497A (zh) * 2012-03-08 2012-07-04 苏州大学 用于锂离子二次电池的正极材料及其制备方法、锂离子二次电池正极和锂离子二次电池
FR2989378B1 (fr) 2012-04-16 2015-10-02 Commissariat Energie Atomique Polymere comme materiau d'electrode pour des batteries secondaires au lithium.
FR3012450B1 (fr) 2013-10-30 2017-10-13 Commissariat Energie Atomique Materiau d'electrode pour batterie organique
CN105118968B (zh) * 2015-09-29 2018-10-16 中南大学 一种巢状v2o3包覆磷酸钒锂的锂离子正极材料
CN105470479B (zh) * 2015-11-26 2017-12-01 中南大学 一种改性的磷酸锰锂复合正极材料及其制备方法
CN106784597A (zh) * 2016-12-19 2017-05-31 苏州格瑞动力电源科技有限公司 一种锂离子电池电极片的制备方法
US11909046B2 (en) 2017-03-07 2024-02-20 The Research Foundation For The State University Of New York Synthetic methods for crystallite size control of bimetallic polyanionic battery compositions
US11251430B2 (en) 2018-03-05 2022-02-15 The Research Foundation For The State University Of New York ϵ-VOPO4 cathode for lithium ion batteries
CN108963235B (zh) * 2018-08-01 2021-07-23 武汉理工大学 石墨烯增强碳包覆磷酸钛锰钠微米球电极材料及其制备方法和应用

Family Cites Families (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4567158A (en) * 1983-12-28 1986-01-28 Monsanto Company Process for preparing phosphorus-vanadium mixed oxide oxidation catalysts
US5102836A (en) * 1990-06-06 1992-04-07 Center For Innovative Technology Ceramic materials with low thermal conductivity and low coefficients of thermal expansion
US5910382A (en) * 1996-04-23 1999-06-08 Board Of Regents, University Of Texas Systems Cathode materials for secondary (rechargeable) lithium batteries
US6203946B1 (en) * 1998-12-03 2001-03-20 Valence Technology, Inc. Lithium-containing phosphates, method of preparation, and uses thereof
US5871866A (en) * 1996-09-23 1999-02-16 Valence Technology, Inc. Lithium-containing phosphates, method of preparation, and use thereof
JP2949229B1 (ja) * 1998-09-16 1999-09-13 大阪大学長 燐酸リチウム・バナジウム複合化合物及び同複合化合物からなるリチウムイオン二次電池用正極材料
US6528033B1 (en) * 2000-01-18 2003-03-04 Valence Technology, Inc. Method of making lithium-containing materials
US7001690B2 (en) * 2000-01-18 2006-02-21 Valence Technology, Inc. Lithium-based active materials and preparation thereof
US6777132B2 (en) * 2000-04-27 2004-08-17 Valence Technology, Inc. Alkali/transition metal halo—and hydroxy-phosphates and related electrode active materials
FR2852148B1 (fr) 2003-03-07 2014-04-11 Batscap Sa Materiau pour electrode composite, procede pour sa preparation
US20040202935A1 (en) * 2003-04-08 2004-10-14 Jeremy Barker Cathode active material with increased alkali/metal content and method of making same
CN100336247C (zh) * 2004-03-30 2007-09-05 中国科学院物理研究所 一种锂离子电池的磷酸盐正极材料的制备方法
JP4794833B2 (ja) * 2004-07-21 2011-10-19 日本コークス工業株式会社 リチウムイオン二次電池用正極材料、その製造方法、及びリチウムイオン二次電池
US8062792B2 (en) * 2005-04-26 2011-11-22 Uchicago Argonne Llc Processes for making dense, spherical active materials for lithium-ion cells
TWI254031B (en) * 2005-05-10 2006-05-01 Aquire Energy Co Ltd Manufacturing method of LixMyPO4 compound with olivine structure
CN101268572B (zh) * 2005-09-21 2011-08-03 国立大学法人九州大学 制造正极活性材料的方法和使用其的非水电解质电池
CN100420076C (zh) * 2005-12-19 2008-09-17 南开大学 溶胶凝胶法合成锂离子电池正极材料磷酸钒锂的方法
US8491861B2 (en) * 2006-05-26 2013-07-23 Eltron Research, Inc. Synthetic process for preparation of high surface area electroactive compounds for battery applications
JP4926607B2 (ja) * 2006-08-23 2012-05-09 住友大阪セメント株式会社 電極材料の製造方法及び正極材料並びに電池
CN101636351B (zh) * 2007-02-28 2011-12-14 株式会社三德 具有橄榄石型结构的化合物、非水电解质二次电池用正极、非水电解质二次电池
JP5182626B2 (ja) * 2007-06-29 2013-04-17 株式会社Ｇｓユアサ 正極活物質および非水電解質電池
TW200951066A (en) * 2008-04-17 2009-12-16 Basf Se Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials
TW201038469A (en) * 2009-03-17 2010-11-01 Basf Se Synthesis of lithium-iron-phosphates

Also Published As

Publication number Publication date
TW200930660A (en) 2009-07-16
US20100301281A1 (en) 2010-12-02
CN102123943A (zh) 2011-07-13
US20130214212A1 (en) 2013-08-22
EP2207751A2 (en) 2010-07-21
US8808575B2 (en) 2014-08-19
WO2009043729A3 (en) 2009-10-29
KR101540133B1 (ko) 2015-07-28
CA2701144A1 (en) 2009-04-09
US8808576B2 (en) 2014-08-19
EP2207751B1 (en) 2013-07-03
TWI401207B (zh) 2013-07-11
WO2009043729A2 (en) 2009-04-09
US20130214201A1 (en) 2013-08-22
KR20100091954A (ko) 2010-08-19
JP2010540393A (ja) 2010-12-24
CN102123943B (zh) 2013-07-10

Similar Documents

Publication Publication Date Title
JP5702145B2 (ja) リチウム、バナジウム、及びフォスフェイトを含有する化合物、及び該化合物と導電性材料を含む混合物を製造するための方法
JP5705541B2 (ja) 結晶性リチウム−、バナジウム−、及びフォスフェイト−含有材料を製造するための方法
JP5653905B2 (ja) リチウム、鉄及びリン酸を含有する結晶性材料の製造方法
JP2011519806A (ja) リチウム、鉄及びリン酸を含有する結晶性材料の製造方法
JP5886193B2 (ja) ＬｉＦｅＰＯ４−炭素合成物を製造するための方法
JP5957225B2 (ja) 熱水条件下でのリチウム−金属−フォスフェイトの合成
JP5722866B2 (ja) リチウム−イオン−フォスフェイトの合成
WO2022145323A1 (ja) リン酸バナジウムリチウムの製造方法

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20110907

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20110907

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20130702

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20130920

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20130930

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20131028

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20140715

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20141105

A911 Transfer to examiner for re-examination before appeal (zenchi)

Free format text: JAPANESE INTERMEDIATE CODE: A911

Effective date: 20141113

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20150120

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20150219

R150 Certificate of patent or registration of utility model

Ref document number: 5702145

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

LAPS Cancellation because of no payment of annual fees