CN101941706A - 一种大孔容消光剂的制备方法 - Google Patents
一种大孔容消光剂的制备方法 Download PDFInfo
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- CN101941706A CN101941706A CN 201010296802 CN201010296802A CN101941706A CN 101941706 A CN101941706 A CN 101941706A CN 201010296802 CN201010296802 CN 201010296802 CN 201010296802 A CN201010296802 A CN 201010296802A CN 101941706 A CN101941706 A CN 101941706A
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- China
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- pore volume
- preparation
- matting agent
- large pore
- water
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- 239000011148 porous material Substances 0.000 title claims abstract description 39
- 238000002360 preparation method Methods 0.000 title claims abstract description 30
- 238000003756 stirring Methods 0.000 claims abstract description 37
- 238000000034 method Methods 0.000 claims abstract description 23
- 238000006243 chemical reaction Methods 0.000 claims abstract description 19
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 16
- 239000010703 silicon Substances 0.000 claims abstract description 16
- 239000012456 homogeneous solution Substances 0.000 claims abstract description 15
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 13
- 230000032683 aging Effects 0.000 claims abstract description 12
- 238000001354 calcination Methods 0.000 claims abstract description 12
- 238000001035 drying Methods 0.000 claims abstract description 12
- 238000005406 washing Methods 0.000 claims abstract description 12
- 239000002253 acid Substances 0.000 claims abstract description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 57
- 229920002635 polyurethane Polymers 0.000 claims description 43
- 239000004814 polyurethane Substances 0.000 claims description 43
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 40
- 239000006224 matting agent Substances 0.000 claims description 32
- 239000000377 silicon dioxide Substances 0.000 claims description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 26
- 235000012239 silicon dioxide Nutrition 0.000 claims description 21
- 239000000839 emulsion Substances 0.000 claims description 19
- 229960001866 silicon dioxide Drugs 0.000 claims description 19
- 229920000728 polyester Polymers 0.000 claims description 11
- 229940059574 pentaerithrityl Drugs 0.000 claims description 8
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 8
- XXZNHVPIQYYRCG-UHFFFAOYSA-N trihydroxy(propoxy)silane Chemical compound CCCO[Si](O)(O)O XXZNHVPIQYYRCG-UHFFFAOYSA-N 0.000 claims description 7
- 239000003995 emulsifying agent Substances 0.000 claims description 6
- 230000001737 promoting effect Effects 0.000 claims description 5
- 239000013256 coordination polymer Substances 0.000 claims description 4
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 claims description 4
- PTBDIHRZYDMNKB-UHFFFAOYSA-N 2,2-Bis(hydroxymethyl)propionic acid Chemical compound OCC(C)(CO)C(O)=O PTBDIHRZYDMNKB-UHFFFAOYSA-N 0.000 claims description 3
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 claims description 3
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 claims description 3
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 claims description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 3
- 229940017219 methyl propionate Drugs 0.000 claims description 3
- 239000000178 monomer Substances 0.000 claims description 3
- 238000012643 polycondensation polymerization Methods 0.000 claims description 3
- 235000019353 potassium silicate Nutrition 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 3
- UQMOLLPKNHFRAC-UHFFFAOYSA-N tetrabutyl silicate Chemical compound CCCCO[Si](OCCCC)(OCCCC)OCCCC UQMOLLPKNHFRAC-UHFFFAOYSA-N 0.000 claims description 3
- 238000010521 absorption reaction Methods 0.000 abstract description 5
- 230000008901 benefit Effects 0.000 abstract description 5
- 238000013461 design Methods 0.000 abstract description 3
- 230000008569 process Effects 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 230000002349 favourable effect Effects 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 description 9
- 239000008367 deionised water Substances 0.000 description 9
- 229910021641 deionized water Inorganic materials 0.000 description 9
- 238000002156 mixing Methods 0.000 description 9
- 239000000203 mixture Substances 0.000 description 9
- VDGJOQCBCPGFFD-UHFFFAOYSA-N oxygen(2-) silicon(4+) titanium(4+) Chemical compound [Si+4].[O-2].[O-2].[Ti+4] VDGJOQCBCPGFFD-UHFFFAOYSA-N 0.000 description 9
- 238000010792 warming Methods 0.000 description 9
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 8
- 238000005516 engineering process Methods 0.000 description 6
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000012716 precipitator Substances 0.000 description 3
- 239000001993 wax Substances 0.000 description 3
- 230000008859 change Effects 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 2
- 239000012808 vapor phase Substances 0.000 description 2
- 239000013543 active substance Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000009775 high-speed stirring Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 229920000962 poly(amidoamine) Polymers 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
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- Silicon Compounds (AREA)
Abstract
Description
项目名称 | 实施例1 | 实施例2 | 实施例3 | 实施例4 | 对比实施例 |
二氧化硅(干基) % | 99.1 | 99.0 | 99.2 | 99.3 | 99.0 |
DBP吸收值ml/g | 2.88 | 2.83 | 2.90 | 2.76 | 2.92 |
孔容ml/g | 1.45 | 1.79 | 2.25 | 2.54 | 2.18 |
孔径 nm | 8.2 | 9.7 | 15.1 | 19.4 | 14.2 |
灼烧减量% | 5.11 | 8.49 | 12.64 | 9.65 | 15.87 |
比表面积m2/g | 560 | 610 | 767 | 853 | 801 |
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2010102968023A CN101941706B (zh) | 2010-09-29 | 2010-09-29 | 一种大孔容消光剂的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2010102968023A CN101941706B (zh) | 2010-09-29 | 2010-09-29 | 一种大孔容消光剂的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101941706A true CN101941706A (zh) | 2011-01-12 |
CN101941706B CN101941706B (zh) | 2012-01-25 |
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CN2010102968023A Expired - Fee Related CN101941706B (zh) | 2010-09-29 | 2010-09-29 | 一种大孔容消光剂的制备方法 |
Country Status (1)
Country | Link |
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CN (1) | CN101941706B (zh) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104828828A (zh) * | 2015-05-08 | 2015-08-12 | 江西纳宇纳米新材料有限公司 | 具有小粒径、超高比表面积的纳米氧化硅 |
CN114560468A (zh) * | 2022-02-25 | 2022-05-31 | 金三江(肇庆)硅材料股份有限公司 | 一种化学机械抛光用二氧化硅及其制备方法和应用 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101837981A (zh) * | 2010-04-30 | 2010-09-22 | 南开大学 | 一种多级孔结构介孔二氧化硅材料及其制备方法 |
-
2010
- 2010-09-29 CN CN2010102968023A patent/CN101941706B/zh not_active Expired - Fee Related
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101837981A (zh) * | 2010-04-30 | 2010-09-22 | 南开大学 | 一种多级孔结构介孔二氧化硅材料及其制备方法 |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104828828A (zh) * | 2015-05-08 | 2015-08-12 | 江西纳宇纳米新材料有限公司 | 具有小粒径、超高比表面积的纳米氧化硅 |
CN114560468A (zh) * | 2022-02-25 | 2022-05-31 | 金三江(肇庆)硅材料股份有限公司 | 一种化学机械抛光用二氧化硅及其制备方法和应用 |
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Publication number | Publication date |
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CN101941706B (zh) | 2012-01-25 |
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Denomination of invention: Preparation method of large-pore volume flatting agent Effective date of registration: 20170728 Granted publication date: 20120125 Pledgee: Bank of Beijing, Limited by Share Ltd, Hangzhou branch Pledgor: Hangzhou ZFC New Materials Technology Co., Ltd. Registration number: 2017330000075 |
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Date of cancellation: 20180926 Granted publication date: 20120125 Pledgee: Bank of Beijing, Limited by Share Ltd, Hangzhou branch Pledgor: Hangzhou ZFC New Materials Technology Co., Ltd. Registration number: 2017330000075 |
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Effective date of registration: 20191114 Address after: No.30, Ninghong Road, Tianning Town, Jiashan County, Jiaxing City, Zhejiang Province Patentee after: Jiaxing Bohao Home Textile Co., Ltd Address before: Hangzhou City, Zhejiang Province, Gongshu District Cambridge 310000 Zhenkang No. 22 Zheng Lu Patentee before: Hangzhou ZFC New Materials Technology Co., Ltd. |
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CF01 | Termination of patent right due to non-payment of annual fee | ||
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Granted publication date: 20120125 Termination date: 20200929 |