CN101928640B - Method for extracting natural perfume and application of extract - Google Patents
Method for extracting natural perfume and application of extract Download PDFInfo
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- CN101928640B CN101928640B CN2010102832555A CN201010283255A CN101928640B CN 101928640 B CN101928640 B CN 101928640B CN 2010102832555 A CN2010102832555 A CN 2010102832555A CN 201010283255 A CN201010283255 A CN 201010283255A CN 101928640 B CN101928640 B CN 101928640B
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Abstract
The invention relates to a method for extracting natural perfume and application of an extract. The method comprises the following steps of: (1) pretreating raw materials; (2) performing reflux extraction on petroleum ether for two times, namely putting liquoric root particles and the petroleum ether into an extractor with a stirring device and performing the reflux extraction on the petroleum ether for two times; (3) collecting the liquoric root particles from the extractor after two-time extraction of the petroleum ether and drying the liquoric root particles; (4) performing microwave reflux extraction for three times, namely putting the dried liquoric root particles into a microwave extractor with a stirring device, adding deionized water and performing the microwave reflux extraction for three times; (5) filtering, namely mixing first, second and third extract and filtering to remove sediment; and (6) concentrating, namely concentrating the mixed liquor of the filtered three-time extract under reduced pressure to obtain the extract of the natural perfume. The method shortens extraction time, improves extraction effect and has the advantages of simple equipment and easy operation.
Description
Technical field
The present invention relates to a kind of application of extracting process and extract of natural perfume material, especially a kind of extraction that is used for tobacco spice belongs to the Phytochemistry technical field.
Background technology
In tobacco product; Fragrance of tobacco and smell are vital; Perfuming cigarette is reinforced then to be one of core technology of tobacco industry, can remedy the shortcomings and deficiencies on the cigarette tobacco leaf formulation through perfuming, reinforced mode, eliminates assorted gas; Make the fragrance of cigarette abundanter, sufficient, thereby inhaling flavor, smelling and have individual style on the perfume (or spice).
The Radix Glycyrrhizae extract is a kind of traditional tobacco aromatics using, has the Hui Tian of increasing, reduces stimulation, improves the effect of cigarette odor-absorbing; But in the conventional Radix Glycyrrhizae extract except useful composition; Also contain some impurity components, when improving the cigarette quality, also bring the negative interaction of other aspect in various degree; Particularly it has tangible herbal, on using, receives certain restriction.
Summary of the invention
The objective of the invention is to overcome the deficiency that exists in the prior art, a kind of application of extracting process and extract of natural perfume material is provided.
According to technical scheme provided by the invention, the extracting process of said natural perfume material comprises following processing step, and its component ratio is counted by weight;
(1) pretreatment of raw material: it is 0.3 ~ 0.7 centimetre Radix Glycyrrhizae particle that Radix Glycyrrhizae is cut into particle diameter;
(2) twice benzinum reflux extraction: 490 ~ 510 parts of Radix Glycyrrhizae particles and 2300 ~ 2500 parts of benzinum inputs are had in the extractor of agitating device, carry out the benzinum reflux extraction first time, 3.5 ~ 4 hours time, obtain extract A; Take out extract A, in extractor, add 1980 ~ 2000 parts of benzinums, carry out the benzinum reflux extraction second time, 2.5 ~ 3 hours time, obtain extract B; The mixing speed of twice benzinum reflux extraction is 40 ~ 50 rev/mins;
(3) the Radix Glycyrrhizae particle after twice extraction of benzinum in the collection extractor was dried the Radix Glycyrrhizae particle 3.4 ~ 4 hours under 97 ~ 102 ℃ temperature;
(4) three microwave reflux extraction: will throw in the microwave extracter that has agitating device through the Radix Glycyrrhizae particle after oven dry is handled, and add 3500 ~ 3750 parts of deionized waters, and carry out the microwave reflux extraction first time 3.5 ~ 4 hours, and collect extract for the first time; In microwave extracter, add 2400 ~ 2500 parts of deionized waters, carry out the microwave reflux extraction second time 3 ~ 3.5 hours, collect extract for the second time; In microwave extracter, add 1400 ~ 1500 parts of deionized waters again, carried out microwave reflux extraction for the third time 2 ~ 2.5 hours, collect extract for the third time; The mixing speed of three microwave reflux extractions is 40 ~ 50 rev/mins, and the interior temperature of charge of microwave reflux extraction device is 100 ~ 102 ℃ during extraction, and microwave power is 1 ~ 1.5kW;
(5) filter: after first, second, third extract mixed, filter, remove deposition with 300 mesh filter screens;
(6) concentrate: the mixed liquor of inciting somebody to action three extracts after filtering reduces pressure in 75 ~ 80 ℃ water-bath inspissator and concentrates, and vacuum is 0.090 ~ 0.095Mpa, obtains the extract of natural perfume material.
A kind of application of extract of natural perfume material; It is characterized in that: the extract that takes by weighing natural perfume material by 0.04 ~ 0.08% of cigarette shreds quality; It is the propylene glycol solution that obtains the extract of natural perfume material in 45% ~ 65% the propane diols that the extract of natural perfume material is dissolved in concentration; Adopt laryngeal spray that the propylene glycol solution spray of the extract of natural perfume material is added in the cigarette shreds, cigarette shreds is rolled into cigarette.
The particle diameter of said Radix Glycyrrhizae fritter is 0.3 ~ 0.7cm.
The density of the extract of said natural perfume material is 1.1920 ~ 1.2070.
The concentration of the propylene glycol solution of the extract of natural perfume material is 10 ~ 30%.
Said natural perfume material is raw material usually with the Radix Glycyrrhizae.
The invention has the advantages that: use microwave abstracting, shortened extraction time, improved extraction effect, the interior quality improving cigarette does not increase inharmonic herbal to cigarette product again.And the method equipment is also uncomplicated, and operation is pollution-free easily.
The specific embodiment
Below in conjunction with specific embodiment the present invention is described further.
The automatic extractor of AE03-B type that extractor used in the present invention adopts Beijing ChinaInvent Instrument Technology Co., Ltd. to produce;
The microwave abstracting machine that microwave extracter used in the present invention adopts Guangzhou Supreme Being's prestige industrial microwave apparatus Co., Ltd to produce;
Water-bath inspissator used in the present invention adopts the RE-52AA rotary evaporator of Shanghai Yarong Biochemical Instrument Plant;
The laryngeal spray that laryngeal spray used in the present invention adopts Yangzhou safety medicine equipment Co., Ltd to produce.
Embodiment 1: a kind of extracting process of natural perfume material comprises following processing step: its component ratio is counted by weight,
(1) pretreatment of raw material: it is 0.3cm Radix Glycyrrhizae particle that Radix Glycyrrhizae is cut into average grain diameter;
(2) twice benzinum reflux extraction: 490 parts of Radix Glycyrrhizae particles and 2300 parts of benzinum inputs are had in the extractor of agitating device, carry out the benzinum reflux extraction first time 3.5 hours, obtain extract A; Take out extract A, in extractor, add 1980 parts of benzinums, carry out the benzinum reflux extraction second time 2.5 hours, obtain extract B; The mixing speed of twice benzinum reflux extraction is 50 rev/mins;
(3) the Radix Glycyrrhizae fritter after twice extraction of benzinum in the collection extractor is dried the Radix Glycyrrhizae particle 4 hours under 97 ℃ temperature;
(4) three microwave reflux extraction: will throw in the microwave extracter that has agitating device through the Radix Glycyrrhizae particle after oven dry is handled, and add 3500 parts of deionized waters, and carry out the microwave reflux extraction first time 3.5 hours, and collect extract for the first time; In microwave extracter, add 2400 parts of deionized waters, carry out the microwave reflux extraction second time 3 hours, collect extract for the second time; In microwave extracter, add 1400 parts of deionized waters again, carried out microwave reflux extraction for the third time 2 hours, collect extract for the third time; The mixing speed of three microwave reflux extractions is 40 rev/mins, and the interior temperature of charge of microwave reflux extraction device is 102 ℃ during extraction, and microwave power is 1.5kW;
(5) filter: after first, second, third extract mixed, filter, remove deposition with 300 mesh filter screens;
(6) concentrate: the mixed liquor of three extracts that will be after filtering reduce pressure concentrated in 75 ℃ water-bath inspissator, and vacuum is 0.090Mpa, and obtaining is the extract of 1.1920 natural perfume material.
The application of the extract of the natural perfume material of gained: the extract that takes by weighing natural perfume material by 0.04% of cigarette shreds quality; It is to obtain the propylene glycol solution that concentration is the extract of 10% natural perfume material in 45% the propane diols that the extract of natural perfume material is dissolved in concentration; Adopt laryngeal spray that the propylene glycol solution spray of the extract of natural perfume material is added in the cigarette shreds, cigarette shreds is rolled into cigarette.
Embodiment 2: a kind of extracting process of natural perfume material comprises following processing step: its component ratio is counted by weight,
(1) pretreatment of raw material: it is 0.7cm Radix Glycyrrhizae particle that Radix Glycyrrhizae is cut into average grain diameter;
(2) twice benzinum reflux extraction: 510 parts of Radix Glycyrrhizae particles and 2500 parts of benzinum inputs are had in the extractor of agitating device, carry out the benzinum reflux extraction first time 4 hours, obtain extract A; Take out extract A, in extractor, add 2000 parts of benzinums, carry out the benzinum reflux extraction second time 3 hours, obtain extract B; The mixing speed of twice benzinum reflux extraction is 40 rev/mins;
(3) the Radix Glycyrrhizae particle after twice extraction of benzinum in the collection extractor is dried the Radix Glycyrrhizae particle 3.4 hours under 102 ℃ temperature;
(4) three microwave reflux extraction: will throw in the microwave extracter that has agitating device through the Radix Glycyrrhizae particle after oven dry is handled, and add 3750 parts of deionized waters, and carry out the microwave reflux extraction first time 4 hours, and collect extract for the first time; In microwave extracter, add 2500 parts of deionized waters, carry out the microwave reflux extraction second time 3.5 hours, collect extract for the second time; In microwave extracter, add 1500 parts of deionized waters again, carried out microwave reflux extraction for the third time 2.5 hours, collect extract for the third time; The mixing speed of three microwave reflux extractions is 50 rev/mins, and the interior temperature of charge of microwave reflux extraction device is 100 ℃ during extraction, and microwave power is 1kW;
(5) filter: after first, second, third extract mixed, filter, remove deposition with 300 mesh filter screens;
(6) concentrate: the mixed liquor of three extracts that will be after filtering reduce pressure concentrated in 80 ℃ water-bath inspissator, and vacuum is 0.095Mpa, and obtaining is the extract of 1.2070 natural perfume material.
A kind of application of extract of natural perfume material; Take by weighing the extract of natural perfume material by 0.08% of cigarette shreds quality; It is to obtain the propylene glycol solution that concentration is the extract of 30% natural perfume material in 65% the propane diols that the extract of natural perfume material is dissolved in concentration; Adopt laryngeal spray that the propylene glycol solution spray of the extract of natural perfume material is added in the cigarette shreds, cigarette shreds is rolled into cigarette.
Embodiment 3: a kind of extracting process of natural perfume material comprises following processing step: its component ratio is counted by weight,
(1) pretreatment of raw material: it is 0.5cm Radix Glycyrrhizae particle that Radix Glycyrrhizae is cut into average grain diameter;
(2) twice benzinum reflux extraction: 500 parts of Radix Glycyrrhizae fritters and 2400 parts of benzinum inputs are had in the extractor of agitating device, carry out the benzinum reflux extraction first time 3.8 hours, obtain extract A; Take out extract A, in extractor, add 1990 parts of benzinums, carry out the benzinum reflux extraction second time 2.8 hours, obtain extract B; The mixing speed of twice benzinum reflux extraction is 45 rev/mins;
(3) the Radix Glycyrrhizae particle after twice extraction of benzinum in the collection extractor is dried the Radix Glycyrrhizae particle 3.8 hours under 100 ℃ temperature;
(4) three microwave reflux extraction: will throw in the microwave extracter that has agitating device through the Radix Glycyrrhizae particle after oven dry is handled, and add 3600 parts of deionized waters, and carry out the microwave reflux extraction first time 3.6 hours, and collect extract for the first time; In microwave extracter, add 2450 parts of deionized waters, carry out the microwave reflux extraction second time 3.2 hours, collect extract for the second time; In microwave extracter, add 1450 parts of deionized waters again, carried out microwave reflux extraction for the third time 2.3 hours, collect extract for the third time; The mixing speed of three microwave reflux extractions is 45 rev/mins, and the interior temperature of charge of microwave reflux extraction device is 101 ℃ during extraction, and microwave power is 1.2kW;
(5) filter: after first, second, third extract mixed, filter, remove deposition with 300 mesh filter screens;
(6) concentrate: the mixed liquor of three extracts that will be after filtering reduce pressure concentrated in 78 ℃ water-bath inspissator, and vacuum is 0.092Mpa, and obtaining is the extract of 1.1990 natural perfume material.
The application of the extract of gained natural perfume material: the extract that takes by weighing natural perfume material by 0.06% of cigarette shreds quality; It is to obtain the propylene glycol solution that concentration is the extract of 20% natural perfume material in 50% the propane diols that the extract of natural perfume material is dissolved in concentration; Adopt laryngeal spray that the propylene glycol solution spray of the extract of natural perfume material is added in the cigarette shreds, cigarette shreds is rolled into cigarette.
Claims (5)
1. the extracting process of a natural perfume material is characterized in that, its component ratio is counted by weight, comprises following processing step:
(1) pretreatment of raw material: Radix Glycyrrhizae is cut into the Radix Glycyrrhizae particle;
(2) twice benzinum reflux extraction: 490 ~ 510 parts of Radix Glycyrrhizae particles and 2300 ~ 2500 parts of benzinum inputs are had in the extractor of agitating device, carry out the benzinum reflux extraction first time 3.5 ~ 4 hours, obtain extract A; Take out extract A, in extractor, add 1980 ~ 2000 parts of benzinums, carry out the benzinum reflux extraction second time 2.5 ~ 3 hours, obtain extract B; The mixing speed of twice benzinum reflux extraction is 40 ~ 50 rev/mins;
(3) the Radix Glycyrrhizae particle after twice extraction of benzinum in the collection extractor was dried the Radix Glycyrrhizae particle 3.4 ~ 4 hours under 97 ~ 102 ℃ temperature;
(4) three microwave reflux extraction: will throw in the microwave extracter that has agitating device through the Radix Glycyrrhizae particle after oven dry is handled, and add 3500 ~ 3750 parts of deionized waters, and carry out the microwave reflux extraction first time 3.5 ~ 4 hours, and collect extract for the first time; In microwave extracter, add 2400 ~ 2500 parts of deionized waters, carry out the microwave reflux extraction second time 3 ~ 3.5 hours, collect extract for the second time; In microwave extracter, add 1400 ~ 1500 parts of deionized waters again, carried out microwave reflux extraction for the third time 2 ~ 2.5 hours, collect extract for the third time; The mixing speed of three microwave reflux extractions is 40 ~ 50 rev/mins, and microwave heating temperature is 100 ~ 102 ℃, and microwave power is 1 ~ 1.5kW;
(5) filter: after first, second, third extract mixed, filter, remove deposition with 300 mesh filter screens;
(6) concentrate: the mixed liquor of inciting somebody to action three extracts after filtering reduces pressure in 75 ~ 80 ℃ water-bath inspissator and concentrates, and vacuum is 0.090 ~ 0.095Mpa, obtains the extract of natural perfume material.
2. extracting process as claimed in claim 1 is characterized in that, the average grain diameter of said Radix Glycyrrhizae fritter is 0.3 ~ 0.7cm.
3. extracting process as claimed in claim 1 is characterized in that, the density of the extract of said natural perfume material is 1.1920 ~ 1.2070.
4. the application of the extract of the natural perfume material that obtains of an extracting process as claimed in claim 1; It is characterized in that; Take by weighing the extract of natural perfume material by 0.04 ~ 0.08% of cigarette shreds quality; It is the propylene glycol solution that obtains the extract of natural perfume material in 45% ~ 65% the propane diols that the extract of natural perfume material is dissolved in concentration, adopts laryngeal spray that the propylene glycol solution spray of extract is added in the cigarette shreds, and cigarette shreds is rolled into cigarette.
5. the application of extract as claimed in claim 4 is characterized in that, the concentration of the propylene glycol solution of the extract of said natural perfume material is 10 ~ 30%.
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| CN2010102832555A CN101928640B (en) | 2010-09-16 | 2010-09-16 | Method for extracting natural perfume and application of extract |
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| CN2010102832555A CN101928640B (en) | 2010-09-16 | 2010-09-16 | Method for extracting natural perfume and application of extract |
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| CN102321503B (en) * | 2011-08-30 | 2013-04-24 | 无锡华海香料有限公司 | Preparation method of fructus momordicae condensate and application thereof |
| CN105147549A (en) * | 2015-08-30 | 2015-12-16 | 孙国真 | Tissue flavoring agent and preparation method thereof |
| CN105907477A (en) * | 2016-07-06 | 2016-08-31 | 鹰潭华宝香精香料有限公司 | Preparation method of natural flavor |
| CN106047501A (en) * | 2016-07-06 | 2016-10-26 | 鹰潭华宝香精香料有限公司 | Compound natural perfume preparation method |
| CN107653066A (en) * | 2017-09-28 | 2018-02-02 | 河南省新郑金叶香料有限公司 | A kind of cigarette radix glycyrrhizae aroma component and its extracting method and application |
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| US5338557A (en) * | 1989-05-16 | 1994-08-16 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of The Environment | Microwave extraction of volatile oils |
| CN101112254A (en) * | 2007-08-30 | 2008-01-30 | 红云烟草(集团)有限责任公司 | Composite Chinese herbal medicine preparations for making cigarette and method for preparing the same |
| CN101817832A (en) * | 2010-05-13 | 2010-09-01 | 苏州派腾生物医药科技有限公司 | Method for preparing sikimin |
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Address after: 214112 Jiangsu city of Wuxi province new Qumei Wu Cun Mei Yuk Road No. 7, room 117 Patentee after: Wuxi Huahai flavor Co., Ltd. Address before: 214112 Jiangsu Province, Wuxi City District Mei Tin Town Hung Road No. 37, No. 3 Patentee before: Wuxi Huahai Flavors Ltd. |
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Application publication date: 20101229 Assignee: Yingtan Huabao flavors Co. Assignor: Wuxi Huahai flavor Co., Ltd. Contract record no.: 2018320000136 Denomination of invention: Method for extracting natural perfume and application of extract Granted publication date: 20120704 License type: Exclusive License Record date: 20180801 |
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Effective date of registration: 20210918 Address after: 335000 Ying Nan avenue, Longgang area, Yingtan economic and Technological Development Zone, Jiangxi Patentee after: YINGTAN HUABAO ESSENCE Co.,Ltd. Address before: 214112 room 7, No. 117, Meiyu Road, Meicun, Xinwu District, Wuxi City, Jiangsu Province Patentee before: Wuxi Huahai flavor Co.,Ltd. |