CN101503194A - 一种活性高纯石英粉的制备方法 - Google Patents
一种活性高纯石英粉的制备方法 Download PDFInfo
- Publication number
- CN101503194A CN101503194A CNA2009100248843A CN200910024884A CN101503194A CN 101503194 A CN101503194 A CN 101503194A CN A2009100248843 A CNA2009100248843 A CN A2009100248843A CN 200910024884 A CN200910024884 A CN 200910024884A CN 101503194 A CN101503194 A CN 101503194A
- Authority
- CN
- China
- Prior art keywords
- purity
- acid
- flotation
- ground quartz
- quartz
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 295
- 239000000377 silicon dioxide Substances 0.000 title claims description 88
- 235000013312 flour Nutrition 0.000 title claims description 31
- 238000002360 preparation method Methods 0.000 title claims description 29
- 239000000843 powder Substances 0.000 claims abstract description 93
- 239000010453 quartz Substances 0.000 claims abstract description 74
- 239000002253 acid Substances 0.000 claims abstract description 55
- 238000005188 flotation Methods 0.000 claims abstract description 52
- 238000012986 modification Methods 0.000 claims abstract description 42
- 230000004048 modification Effects 0.000 claims abstract description 39
- 239000002699 waste material Substances 0.000 claims abstract description 37
- 238000007885 magnetic separation Methods 0.000 claims abstract description 34
- 239000000463 material Substances 0.000 claims abstract description 28
- 238000000034 method Methods 0.000 claims abstract description 28
- 238000000227 grinding Methods 0.000 claims abstract description 23
- 239000002994 raw material Substances 0.000 claims abstract description 11
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 86
- 238000002156 mixing Methods 0.000 claims description 42
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 40
- 238000005554 pickling Methods 0.000 claims description 40
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 36
- 239000003795 chemical substances by application Substances 0.000 claims description 27
- REYJJPSVUYRZGE-UHFFFAOYSA-N Octadecylamine Chemical compound CCCCCCCCCCCCCCCCCCN REYJJPSVUYRZGE-UHFFFAOYSA-N 0.000 claims description 23
- JRBPAEWTRLWTQC-UHFFFAOYSA-N dodecylamine Chemical compound CCCCCCCCCCCCN JRBPAEWTRLWTQC-UHFFFAOYSA-N 0.000 claims description 23
- 150000001412 amines Chemical class 0.000 claims description 22
- 239000012535 impurity Substances 0.000 claims description 22
- PEEHTFAAVSWFBL-UHFFFAOYSA-N Maleimide Chemical compound O=C1NC(=O)C=C1 PEEHTFAAVSWFBL-UHFFFAOYSA-N 0.000 claims description 17
- 238000012545 processing Methods 0.000 claims description 17
- 238000004519 manufacturing process Methods 0.000 claims description 16
- 239000000919 ceramic Substances 0.000 claims description 12
- 239000011521 glass Substances 0.000 claims description 12
- 238000007603 infrared drying Methods 0.000 claims description 12
- 235000006408 oxalic acid Nutrition 0.000 claims description 12
- 239000004576 sand Substances 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 229920003192 poly(bis maleimide) Polymers 0.000 claims description 11
- 229910001220 stainless steel Inorganic materials 0.000 claims description 9
- 239000010935 stainless steel Substances 0.000 claims description 9
- XEEVLJKYYUVTRC-UHFFFAOYSA-N oxomalonic acid Chemical compound OC(=O)C(=O)C(O)=O XEEVLJKYYUVTRC-UHFFFAOYSA-N 0.000 claims description 8
- 239000006148 magnetic separator Substances 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 5
- 239000006004 Quartz sand Substances 0.000 abstract description 33
- 230000018044 dehydration Effects 0.000 abstract description 14
- 238000006297 dehydration reaction Methods 0.000 abstract description 14
- 239000003822 epoxy resin Substances 0.000 abstract description 5
- 229920000647 polyepoxide Polymers 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 2
- 239000000945 filler Substances 0.000 abstract description 2
- 238000007789 sealing Methods 0.000 abstract description 2
- 239000002910 solid waste Substances 0.000 abstract description 2
- 238000004140 cleaning Methods 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000003756 stirring Methods 0.000 description 18
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 12
- 239000010433 feldspar Substances 0.000 description 9
- 239000010445 mica Substances 0.000 description 9
- 229910052618 mica group Inorganic materials 0.000 description 9
- 239000000047 product Substances 0.000 description 9
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 7
- 238000010438 heat treatment Methods 0.000 description 6
- 239000006246 high-intensity magnetic separator Substances 0.000 description 6
- 238000002386 leaching Methods 0.000 description 6
- 238000012856 packing Methods 0.000 description 6
- 239000004033 plastic Substances 0.000 description 6
- 238000000746 purification Methods 0.000 description 6
- 230000001105 regulatory effect Effects 0.000 description 6
- 238000005406 washing Methods 0.000 description 6
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- 229910052742 iron Inorganic materials 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 239000011044 quartzite Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000004593 Epoxy Substances 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 229910001608 iron mineral Inorganic materials 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 239000005995 Aluminium silicate Substances 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 229920003230 addition polyimide Polymers 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 235000012204 lemonade/lime carbonate Nutrition 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 229960001708 magnesium carbonate Drugs 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- 235000014380 magnesium carbonate Nutrition 0.000 description 1
- 125000005439 maleimidyl group Chemical group C1(C=CC(N1*)=O)=O 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000005304 optical glass Substances 0.000 description 1
- 239000003566 sealing material Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
Landscapes
- Processing Of Solid Wastes (AREA)
- Silicon Compounds (AREA)
Abstract
Description
Claims (6)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2009100248843A CN101503194B (zh) | 2009-03-02 | 2009-03-02 | 一种活性高纯石英粉的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2009100248843A CN101503194B (zh) | 2009-03-02 | 2009-03-02 | 一种活性高纯石英粉的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101503194A true CN101503194A (zh) | 2009-08-12 |
CN101503194B CN101503194B (zh) | 2011-03-30 |
Family
ID=40975584
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2009100248843A Active CN101503194B (zh) | 2009-03-02 | 2009-03-02 | 一种活性高纯石英粉的制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN101503194B (zh) |
Cited By (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102030462A (zh) * | 2010-10-26 | 2011-04-27 | 王成敬 | 精制石英砂的加工方法 |
CN102211774A (zh) * | 2010-04-02 | 2011-10-12 | 南开大学 | 硅微粉的选择性絮凝提纯方法 |
CN102328932A (zh) * | 2011-06-18 | 2012-01-25 | 福建师范大学 | 一种精制石英砂的方法 |
CN102527522A (zh) * | 2012-02-28 | 2012-07-04 | 江西大唐新材料开发有限公司 | 一种硅砂中微量金属杂质浮选分离的工艺方法 |
CN103449455A (zh) * | 2013-08-30 | 2013-12-18 | 连云港市弘扬石英制品有限公司 | 一种以低品位石英矿为原料生产高品质石英砂的方法 |
CN103663469A (zh) * | 2013-11-21 | 2014-03-26 | 成都兴能新材料有限公司 | 石英砂提纯工艺 |
CN103896285A (zh) * | 2014-04-21 | 2014-07-02 | 江苏凯达石英有限公司 | 一种以废旧石英埚制备高纯超细石英粉的方法 |
CN103964444A (zh) * | 2014-05-05 | 2014-08-06 | 临沂晟泉矿业有限公司 | 一种高纯石英砂的生产方法 |
CN105541186A (zh) * | 2016-02-03 | 2016-05-04 | 常州达奥新材料科技有限公司 | 一种利用水晶石废料制备环保建筑装饰材料的方法 |
CN106185954A (zh) * | 2016-07-06 | 2016-12-07 | 王林 | 一种大规模化石英砂酸洗除铁除杂工艺 |
CN106185953A (zh) * | 2016-07-06 | 2016-12-07 | 王林 | 一种大规模化石英砂酸洗除杂增白工艺 |
CN107199120A (zh) * | 2017-07-27 | 2017-09-26 | 中钢集团马鞍山矿山研究院有限公司 | 一种含有磁黄铁矿、黄铁矿的高硫磁铁矿石的选矿方法 |
CN107661810A (zh) * | 2016-07-30 | 2018-02-06 | 湖北永绍科技股份有限公司 | 一种长石石英岩制备高纯石英砂的方法 |
CN110015847A (zh) * | 2018-01-09 | 2019-07-16 | 张学舜 | 一种引入盐渣可制作高档酒店内外墙装饰板及工业防腐、抗磨新材料的方法 |
CN110885239A (zh) * | 2019-11-22 | 2020-03-17 | 苏州溪能环保科技有限公司 | 一种高纯熔融石英粉的制备方法 |
CN111167597A (zh) * | 2019-12-31 | 2020-05-19 | 上杭鑫昌龙实业有限公司 | 石英尾矿矿泥深度提纯方法与设备 |
CN112624124A (zh) * | 2020-12-16 | 2021-04-09 | 新沂市中大石英科技有限公司 | 一种高纯高疏水石英砂的制备工艺 |
CN112723363A (zh) * | 2020-12-27 | 2021-04-30 | 江苏新达石英有限公司 | 一种生产高纯石英粉的耦合纯化工艺 |
CN115178363A (zh) * | 2022-07-08 | 2022-10-14 | 中南大学 | 一种含泥石英岩制备超高纯石英粉及综合利用工艺 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4983370A (en) * | 1990-02-06 | 1991-01-08 | The Feldspar Corporation | Purified quartz and process for purifying quartz |
US6277349B1 (en) * | 1998-11-14 | 2001-08-21 | C. Eric Westbrook | Tridymite-based processing for high purity quartz |
CN101367609A (zh) * | 2008-08-15 | 2009-02-18 | 刘少云 | 石英砂和石英粉的制备与提纯工艺及其产品 |
-
2009
- 2009-03-02 CN CN2009100248843A patent/CN101503194B/zh active Active
Cited By (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102211774A (zh) * | 2010-04-02 | 2011-10-12 | 南开大学 | 硅微粉的选择性絮凝提纯方法 |
CN102211774B (zh) * | 2010-04-02 | 2013-06-19 | 南开大学 | 硅微粉的选择性絮凝提纯方法 |
CN102030462A (zh) * | 2010-10-26 | 2011-04-27 | 王成敬 | 精制石英砂的加工方法 |
CN102328932A (zh) * | 2011-06-18 | 2012-01-25 | 福建师范大学 | 一种精制石英砂的方法 |
CN102527522A (zh) * | 2012-02-28 | 2012-07-04 | 江西大唐新材料开发有限公司 | 一种硅砂中微量金属杂质浮选分离的工艺方法 |
CN103449455B (zh) * | 2013-08-30 | 2015-04-29 | 连云港市弘扬石英制品有限公司 | 一种以低品位石英矿为原料生产高品质石英砂的方法 |
CN103449455A (zh) * | 2013-08-30 | 2013-12-18 | 连云港市弘扬石英制品有限公司 | 一种以低品位石英矿为原料生产高品质石英砂的方法 |
CN103663469A (zh) * | 2013-11-21 | 2014-03-26 | 成都兴能新材料有限公司 | 石英砂提纯工艺 |
CN103663469B (zh) * | 2013-11-21 | 2016-01-20 | 成都兴能新材料有限公司 | 石英砂提纯工艺 |
CN103896285A (zh) * | 2014-04-21 | 2014-07-02 | 江苏凯达石英有限公司 | 一种以废旧石英埚制备高纯超细石英粉的方法 |
CN103964444A (zh) * | 2014-05-05 | 2014-08-06 | 临沂晟泉矿业有限公司 | 一种高纯石英砂的生产方法 |
CN103964444B (zh) * | 2014-05-05 | 2016-08-24 | 临沂晟泉矿业有限公司 | 一种高纯石英砂的生产方法 |
CN105541186A (zh) * | 2016-02-03 | 2016-05-04 | 常州达奥新材料科技有限公司 | 一种利用水晶石废料制备环保建筑装饰材料的方法 |
CN105541186B (zh) * | 2016-02-03 | 2018-03-16 | 广东铭诚智能建筑科技有限公司 | 一种利用水晶石废料制备环保建筑装饰材料的方法 |
CN106185953A (zh) * | 2016-07-06 | 2016-12-07 | 王林 | 一种大规模化石英砂酸洗除杂增白工艺 |
CN106185954A (zh) * | 2016-07-06 | 2016-12-07 | 王林 | 一种大规模化石英砂酸洗除铁除杂工艺 |
CN107661810A (zh) * | 2016-07-30 | 2018-02-06 | 湖北永绍科技股份有限公司 | 一种长石石英岩制备高纯石英砂的方法 |
CN107199120B (zh) * | 2017-07-27 | 2018-09-18 | 中钢集团马鞍山矿山研究院有限公司 | 一种含有磁黄铁矿、黄铁矿的高硫磁铁矿石的选矿方法 |
CN107199120A (zh) * | 2017-07-27 | 2017-09-26 | 中钢集团马鞍山矿山研究院有限公司 | 一种含有磁黄铁矿、黄铁矿的高硫磁铁矿石的选矿方法 |
CN110015847B (zh) * | 2018-01-09 | 2021-12-10 | 张学舜 | 一种引入盐渣可制作高档酒店内外墙装饰板及工业防腐、抗磨新材料的方法 |
CN110015847A (zh) * | 2018-01-09 | 2019-07-16 | 张学舜 | 一种引入盐渣可制作高档酒店内外墙装饰板及工业防腐、抗磨新材料的方法 |
CN110885239A (zh) * | 2019-11-22 | 2020-03-17 | 苏州溪能环保科技有限公司 | 一种高纯熔融石英粉的制备方法 |
CN111167597A (zh) * | 2019-12-31 | 2020-05-19 | 上杭鑫昌龙实业有限公司 | 石英尾矿矿泥深度提纯方法与设备 |
CN111167597B (zh) * | 2019-12-31 | 2021-07-27 | 深圳市鑫昌龙新材料研究所有限公司 | 石英尾矿矿泥深度提纯方法与设备 |
CN112624124A (zh) * | 2020-12-16 | 2021-04-09 | 新沂市中大石英科技有限公司 | 一种高纯高疏水石英砂的制备工艺 |
CN112624124B (zh) * | 2020-12-16 | 2022-05-13 | 新沂市中大石英科技有限公司 | 一种高纯高疏水石英砂的制备工艺 |
CN112723363A (zh) * | 2020-12-27 | 2021-04-30 | 江苏新达石英有限公司 | 一种生产高纯石英粉的耦合纯化工艺 |
CN115178363A (zh) * | 2022-07-08 | 2022-10-14 | 中南大学 | 一种含泥石英岩制备超高纯石英粉及综合利用工艺 |
CN115178363B (zh) * | 2022-07-08 | 2024-03-01 | 中南大学 | 一种含泥石英岩制备超高纯石英粉及综合利用工艺 |
Also Published As
Publication number | Publication date |
---|---|
CN101503194B (zh) | 2011-03-30 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN101503194B (zh) | 一种活性高纯石英粉的制备方法 | |
CN104961123B (zh) | 一种天然石墨矿剥离提纯方法 | |
CN110734068A (zh) | 一种高纯石英砂的制备方法 | |
CN101891902B (zh) | 一种废旧环氧树脂的回收方法 | |
WO2017063580A1 (zh) | 一种铸造用陶粒砂 | |
CN102219226A (zh) | 应用于石英陶瓷坩埚的高纯熔融石英粉体材料制备方法 | |
CN112456502A (zh) | 一种高效节能环保的高纯石英砂的制备工艺 | |
CN110015666A (zh) | 一种高纯亚微米球形硅微粉的制备方法 | |
CN102491330B (zh) | 碳化硅生产工艺 | |
CN112830698B (zh) | 利用锂辉石浮选尾矿酸热激发制备免烧地聚物材料的方法 | |
CN108864765A (zh) | 一种利用普通石英矿物原料制备硅微粉的制备方法 | |
CN107285321A (zh) | 一种亚纳米球形硅微粉的制备方法 | |
CN106082238A (zh) | 一种石英砂的提纯方法 | |
CN103896285B (zh) | 一种以废旧石英埚制备高纯超细石英粉的方法 | |
CN104532000A (zh) | 一种废铝清洗、浮选和烘干一体化预处理方法 | |
CN108394903B (zh) | 一种纳米级碳化硅微粉的制备方法 | |
CN110885239A (zh) | 一种高纯熔融石英粉的制备方法 | |
CN103950940B (zh) | 低介电常数硅微粉的制备方法 | |
CN102134646B (zh) | 以铝业高铁赤泥为原料直接制备金属铁和铝精矿的方法 | |
CN104892982B (zh) | 采用铸造废灰砂加工成橡胶与塑料填充补强剂的工艺方法 | |
CN103396041A (zh) | 一种人造高纯石英石碾轮和碾盘及其制备方法 | |
CN110894158A (zh) | 一种太阳能多晶硅铸锭用低铁熔融石英粉的制备方法 | |
CN102874779A (zh) | 利用中低品位磷矿生产磷铵且无固废排放的新方法 | |
CN113751187B (zh) | 一种石英精砂及其制备方法和应用 | |
CN102489218A (zh) | 碳化硅细粉的造粒成型方法及碳化硅颗粒 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: LIANYUNGANG HONGYANG QUARTZ CO., LTD. Free format text: FORMER OWNER: SHEN SHIFU Effective date: 20130711 Free format text: FORMER OWNER: XU CHUANLONG Effective date: 20130711 |
|
C41 | Transfer of patent application or patent right or utility model | ||
COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 100044 XICHENG, BEIJING TO: 222300 LIANYUNGANG, JIANGSU PROVINCE |
|
TR01 | Transfer of patent right |
Effective date of registration: 20130711 Address after: Ping Road on the eastern side of pingming Town Industrial Park in Donghai County city of Lianyungang province Jiangsu 222300 Patentee after: Lianyungang Hongyang Quartz Products Co., Ltd. Address before: 100044, Beijing, Xicheng District, Xizhimen foreign Hing Street, No. 1 Patentee before: Shen Shifu Patentee before: Xu Chuanlong Effective date of registration: 20130711 Address after: Ping Road on the eastern side of pingming Town Industrial Park in Donghai County city of Lianyungang province Jiangsu 222300 Patentee after: Lianyungang Hongyang Quartz Products Co., Ltd. Address before: 100044, Beijing, Xicheng District, Xizhimen foreign Hing Street, No. 1 Patentee before: Shen Shifu Patentee before: Xu Chuanlong |
|
CP01 | Change in the name or title of a patent holder |
Address after: Ping Road on the eastern side of pingming Town Industrial Park in Donghai County city of Lianyungang province Jiangsu 222300 Patentee after: Jiangsu Kaiyang quartz products Co., Ltd Address before: Ping Road on the eastern side of pingming Town Industrial Park in Donghai County city of Lianyungang province Jiangsu 222300 Patentee before: LIANYUNGANG HONGYANG QUARTZ PRODUCTS Co.,Ltd. |
|
CP01 | Change in the name or title of a patent holder |