CN101417991B - 构树叶黄酮的提取方法 - Google Patents
构树叶黄酮的提取方法 Download PDFInfo
- Publication number
- CN101417991B CN101417991B CN2008102288696A CN200810228869A CN101417991B CN 101417991 B CN101417991 B CN 101417991B CN 2008102288696 A CN2008102288696 A CN 2008102288696A CN 200810228869 A CN200810228869 A CN 200810228869A CN 101417991 B CN101417991 B CN 101417991B
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- CN
- China
- Prior art keywords
- ethyl acetate
- extraction
- extracting
- broussonetia papyrifera
- flavonoid compound
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229930003935 flavonoid Natural products 0.000 title claims abstract description 19
- 235000017173 flavonoids Nutrition 0.000 title claims abstract description 19
- 238000000034 method Methods 0.000 title claims abstract description 9
- 241000705930 Broussonetia papyrifera Species 0.000 title claims abstract description 6
- 150000002215 flavonoids Chemical class 0.000 title claims abstract description 4
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims abstract description 16
- 238000000605 extraction Methods 0.000 claims abstract description 16
- -1 flavonoid compound Chemical class 0.000 claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 10
- 239000002024 ethyl acetate extract Substances 0.000 claims abstract description 6
- 238000004140 cleaning Methods 0.000 claims abstract description 3
- 239000000463 material Substances 0.000 claims abstract description 3
- 238000010992 reflux Methods 0.000 claims abstract description 3
- 241000933832 Broussonetia Species 0.000 claims description 10
- 238000003810 ethyl acetate extraction Methods 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 5
- UGAPHEBNTGUMBB-UHFFFAOYSA-N acetic acid;ethyl acetate Chemical compound CC(O)=O.CCOC(C)=O UGAPHEBNTGUMBB-UHFFFAOYSA-N 0.000 claims description 5
- 239000000284 extract Substances 0.000 claims description 4
- 230000008569 process Effects 0.000 claims description 3
- 238000010298 pulverizing process Methods 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 7
- 238000001035 drying Methods 0.000 abstract description 4
- 229930014626 natural product Natural products 0.000 abstract description 2
- 238000000926 separation method Methods 0.000 abstract description 2
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 abstract 9
- 238000002386 leaching Methods 0.000 abstract 2
- 239000008346 aqueous phase Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- 239000012535 impurity Substances 0.000 description 4
- 230000003068 static effect Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 210000002966 serum Anatomy 0.000 description 2
- 244000144730 Amygdalus persica Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 102000004877 Insulin Human genes 0.000 description 1
- 108090001061 Insulin Proteins 0.000 description 1
- 206010022489 Insulin Resistance Diseases 0.000 description 1
- 235000006040 Prunus persica var persica Nutrition 0.000 description 1
- 206010067130 Spastic diplegia Diseases 0.000 description 1
- 102000019197 Superoxide Dismutase Human genes 0.000 description 1
- 108010012715 Superoxide dismutase Proteins 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 230000003035 anti-peroxidant effect Effects 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 206010008129 cerebral palsy Diseases 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000002481 ethanol extraction Methods 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 230000002440 hepatic effect Effects 0.000 description 1
- 230000002218 hypoglycaemic effect Effects 0.000 description 1
- 230000003859 lipid peroxidation Effects 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
Landscapes
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2008102288696A CN101417991B (zh) | 2008-11-18 | 2008-11-18 | 构树叶黄酮的提取方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN2008102288696A CN101417991B (zh) | 2008-11-18 | 2008-11-18 | 构树叶黄酮的提取方法 |
Publications (2)
Publication Number | Publication Date |
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CN101417991A CN101417991A (zh) | 2009-04-29 |
CN101417991B true CN101417991B (zh) | 2012-05-23 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN2008102288696A Expired - Fee Related CN101417991B (zh) | 2008-11-18 | 2008-11-18 | 构树叶黄酮的提取方法 |
Country Status (1)
Country | Link |
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CN (1) | CN101417991B (zh) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102060828B (zh) * | 2010-11-23 | 2012-12-05 | 苏州派腾生物医药科技有限公司 | 一种构树素的制备方法 |
CN102423343A (zh) * | 2011-11-17 | 2012-04-25 | 大连中植环境生物科技有限公司 | 一种构树叶总黄酮提取物及其制备方法与应用 |
CN103071021A (zh) * | 2012-10-24 | 2013-05-01 | 内蒙古农业大学 | 沙葱叶片黄酮类物质的提取方法 |
CN110974869A (zh) * | 2020-01-03 | 2020-04-10 | 吉林大学 | 构树叶粗提物在制备治疗非酒精性脂肪肝病药物中的应用 |
CN114668792B (zh) * | 2022-05-07 | 2023-05-05 | 江西省农业科学院畜牧兽医研究所 | 一种构树提取物在制备防治猪流行性腹泻病毒或猪急性腹泻综合征冠状病毒的药物中的应用 |
-
2008
- 2008-11-18 CN CN2008102288696A patent/CN101417991B/zh not_active Expired - Fee Related
Non-Patent Citations (3)
Title |
---|
徐小花 等.构树叶的化学成分.《中国天然药物》.2007,第5卷(第3期),190. * |
杜彰礼 等.楮叶中香豆素和黄酮类化学成分研究.《天然产物研究与开发》.2008,第20卷(第4期),630-631. * |
贾东辉 等.构树叶中黄酮成分分析和抗氧化活性的测定.《职业与健康》.2006,第22卷(第17期),1352. * |
Also Published As
Publication number | Publication date |
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CN101417991A (zh) | 2009-04-29 |
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Effective date of registration: 20140227 Address after: 570228 School of materials and chemical engineering, Hainan University, 58 Renmin Road, Hainan, Haikou Patentee after: Hainan University Patentee after: Dalian Polytechnic University Address before: 116034 Ganjingzi Light Industry Zone, Liaoning, No. 1, No. Patentee before: Dalian Polytechnic University |
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