CN101186839B - 使用氧化铝作为有机金属硅络合物的捕获物质 - Google Patents
使用氧化铝作为有机金属硅络合物的捕获物质 Download PDFInfo
- Publication number
- CN101186839B CN101186839B CN2007101929585A CN200710192958A CN101186839B CN 101186839 B CN101186839 B CN 101186839B CN 2007101929585 A CN2007101929585 A CN 2007101929585A CN 200710192958 A CN200710192958 A CN 200710192958A CN 101186839 B CN101186839 B CN 101186839B
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- Prior art keywords
- aluminum oxide
- alumina
- described methods
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- weight
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 title claims abstract description 33
- 239000003795 chemical substances by application Substances 0.000 title description 2
- 238000001179 sorption measurement Methods 0.000 title description 2
- 238000000034 method Methods 0.000 claims abstract description 21
- 239000011148 porous material Substances 0.000 claims abstract description 11
- 239000007787 solid Substances 0.000 claims abstract description 10
- 238000001354 calcination Methods 0.000 claims abstract description 7
- 239000007791 liquid phase Substances 0.000 claims abstract description 3
- 239000011324 bead Substances 0.000 claims description 15
- 229910052746 lanthanum Inorganic materials 0.000 claims description 5
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 2
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 2
- 229910052791 calcium Inorganic materials 0.000 claims description 2
- 239000011575 calcium Substances 0.000 claims description 2
- 229910052749 magnesium Inorganic materials 0.000 claims description 2
- 239000011777 magnesium Substances 0.000 claims description 2
- 229910052700 potassium Inorganic materials 0.000 claims description 2
- 239000011591 potassium Substances 0.000 claims description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims 10
- 229910052728 basic metal Inorganic materials 0.000 claims 1
- 150000003818 basic metals Chemical group 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 239000012071 phase Substances 0.000 claims 1
- 229910052761 rare earth metal Inorganic materials 0.000 claims 1
- 150000002910 rare earth metals Chemical class 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 description 13
- 239000010703 silicon Substances 0.000 description 13
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 239000003054 catalyst Substances 0.000 description 5
- 238000009616 inductively coupled plasma Methods 0.000 description 5
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 4
- -1 organometallic silicon complexes Chemical class 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 2
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000002019 doping agent Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000499 gel Substances 0.000 description 2
- 229910001679 gibbsite Inorganic materials 0.000 description 2
- 238000004442 gravimetric analysis Methods 0.000 description 2
- 238000005470 impregnation Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 125000002524 organometallic group Chemical group 0.000 description 2
- 238000011282 treatment Methods 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 239000002518 antifoaming agent Substances 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000004523 catalytic cracking Methods 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000010981 drying operation Methods 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 238000010335 hydrothermal treatment Methods 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- MRELNEQAGSRDBK-UHFFFAOYSA-N lanthanum oxide Inorganic materials [O-2].[O-2].[O-2].[La+3].[La+3] MRELNEQAGSRDBK-UHFFFAOYSA-N 0.000 description 1
- FYDKNKUEBJQCCN-UHFFFAOYSA-N lanthanum(3+);trinitrate Chemical compound [La+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O FYDKNKUEBJQCCN-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- KTUFCUMIWABKDW-UHFFFAOYSA-N oxo(oxolanthaniooxy)lanthanum Chemical compound O=[La]O[La]=O KTUFCUMIWABKDW-UHFFFAOYSA-N 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 239000003209 petroleum derivative Substances 0.000 description 1
- 235000011007 phosphoric acid Nutrition 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 238000004230 steam cracking Methods 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 239000012224 working solution Substances 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
- B01J20/08—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04 comprising aluminium oxide or hydroxide; comprising bauxite
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- B01D—SEPARATION
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- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
- B01J20/041—Oxides or hydroxides
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- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G25/00—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents
- C10G25/003—Specific sorbent material, not covered by C10G25/02 or C10G25/03
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
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- Y10S95/00—Gas separation: processes
- Y10S95/90—Solid sorbent
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Nanotechnology (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Catalysts (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR06/09197 | 2006-10-18 | ||
| FR0609197A FR2907348B1 (fr) | 2006-10-18 | 2006-10-18 | Utilisation d'alumines comme masse de captation de complexes organometalliques du silicium |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101186839A CN101186839A (zh) | 2008-05-28 |
| CN101186839B true CN101186839B (zh) | 2013-03-27 |
Family
ID=37946081
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2007101929585A Expired - Fee Related CN101186839B (zh) | 2006-10-18 | 2007-10-18 | 使用氧化铝作为有机金属硅络合物的捕获物质 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US7625430B2 (enExample) |
| EP (1) | EP1918005A1 (enExample) |
| JP (1) | JP5448322B2 (enExample) |
| CN (1) | CN101186839B (enExample) |
| BR (1) | BRPI0704030A (enExample) |
| CA (1) | CA2606889C (enExample) |
| FR (1) | FR2907348B1 (enExample) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BRPI0802431B1 (pt) * | 2008-07-28 | 2017-02-07 | Petróleo Brasileiro S/A - Petrobras | processo de remoção de compostos de silício de correntes de hidrocarbonetos |
| JP5564519B2 (ja) | 2010-01-27 | 2014-07-30 | 日立Ｇｅニュークリア・エナジー株式会社 | 放射性気体廃棄物の処理方法、処理設備、及び不純物除去材、並びにシロキサンの分解除去方法 |
| JP2013032987A (ja) | 2011-08-02 | 2013-02-14 | Hitachi Automotive Systems Ltd | 水素センサ装置 |
| US9259681B2 (en) * | 2013-10-31 | 2016-02-16 | Haldex Brake Products Corporation | Air dryer |
| US20160046881A1 (en) * | 2014-08-13 | 2016-02-18 | Exxonmobil Research And Engineering Company | Desulfurization of naphtha blends |
| EP3585866A1 (en) * | 2017-02-21 | 2020-01-01 | ExxonMobil Research and Engineering Company | Desulfurization of a naphtha boiling range feed |
| CN118002157B (zh) * | 2022-10-31 | 2025-10-03 | 中国石油化工股份有限公司 | 一种捕硅催化剂，其制备方法及应用 |
| CN115814565B (zh) * | 2022-11-30 | 2024-05-31 | 攀钢集团攀枝花钢铁研究院有限公司 | 一种推板窑煅烧制备钒氮合金的钾钠吸收方法及吸收剂 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4645587A (en) * | 1984-12-07 | 1987-02-24 | Union Oil Company Of California | Process for removing silicon compounds from hydrocarbon streams |
| CN1478862A (zh) * | 2002-08-29 | 2004-03-03 | 中国石油化工股份有限公司 | 从馏分油中脱除有机硅化合物的方法 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4176047A (en) * | 1978-04-10 | 1979-11-27 | Continental Oil Company | Removal of organic compounds from coker gasoline |
| JPS59162122A (ja) * | 1983-03-08 | 1984-09-13 | Mitsui Toatsu Chem Inc | 四弗化ケイ素の精製法 |
| JPS60222144A (ja) * | 1984-04-20 | 1985-11-06 | Matsushita Electric Works Ltd | ガスフイルタ |
| US4747937A (en) * | 1986-11-24 | 1988-05-31 | Uop Inc. | Process for the removal of hydrogenatable hydrocarbonaceous compounds from a hydrocarbonaceous stream and hydrogenating these compounds |
| JPH05262501A (ja) * | 1991-12-02 | 1993-10-12 | Shin Etsu Chem Co Ltd | 加水分解性の有機ケイ素化合物を含有する塩化水素の精製方法 |
| FR2732622B1 (fr) * | 1995-04-10 | 1997-05-09 | Rhone Poulenc Chimie | Procede pour l'adsorption de composes organometalliques chelates et billes d'alumine comprenant un compose organometallique chelate |
| FR2736281B1 (fr) * | 1995-07-07 | 1997-08-01 | Rhone Poulenc Chimie | Procede pour l'adsorption de composes organometalliques chelates et adsorbants a base d'alumine comprenant un compose organometallique chelate |
| JP3710528B2 (ja) * | 1995-09-20 | 2005-10-26 | 日揮ユニバーサル株式会社 | 触媒毒除去剤、それを用いた工場排ガスの処理方法および流通式反応装置 |
| US6159898A (en) * | 1997-05-23 | 2000-12-12 | Uop Llc | Alumina bodies containing alkali or alkaline earth metal compounds |
| DE19730126A1 (de) * | 1997-07-14 | 1999-01-21 | Basf Ag | Aluminiumoxid enthaltender Feststoff mit großer Oberfläche |
| FR2774606B1 (fr) * | 1998-02-11 | 2000-03-17 | Rhodia Chimie Sa | Procede d'elimination de composes halogenes contenus dans un gaz ou un liquide |
| FR2823131B1 (fr) * | 2001-04-04 | 2004-10-22 | Pro Catalyse | Procede d'elimination des molecules oxygenees organiques presentes dans un effluent organique, utilisant des agglomeres d'alumine |
| US6790920B2 (en) * | 2002-09-12 | 2004-09-14 | Kraton Polymers U.S. Llc | Process for removal of silicon compounds from solvents by selective absorption |
| JP3776904B2 (ja) * | 2003-10-16 | 2006-05-24 | 大陽日酸株式会社 | シロキサン除去方法 |
| US7306652B2 (en) * | 2005-03-30 | 2007-12-11 | Parker-Hannifin Corporation | Siloxane removal process |
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2006
- 2006-10-18 FR FR0609197A patent/FR2907348B1/fr not_active Expired - Fee Related
-
2007
- 2007-09-28 EP EP07291185A patent/EP1918005A1/fr not_active Withdrawn
- 2007-10-11 BR BRPI0704030-0A patent/BRPI0704030A/pt not_active IP Right Cessation
- 2007-10-15 CA CA2606889A patent/CA2606889C/fr not_active Expired - Fee Related
- 2007-10-15 JP JP2007267388A patent/JP5448322B2/ja not_active Expired - Fee Related
- 2007-10-17 US US11/907,817 patent/US7625430B2/en not_active Expired - Fee Related
- 2007-10-18 CN CN2007101929585A patent/CN101186839B/zh not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4645587A (en) * | 1984-12-07 | 1987-02-24 | Union Oil Company Of California | Process for removing silicon compounds from hydrocarbon streams |
| CN1478862A (zh) * | 2002-08-29 | 2004-03-03 | 中国石油化工股份有限公司 | 从馏分油中脱除有机硅化合物的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101186839A (zh) | 2008-05-28 |
| JP2008101207A (ja) | 2008-05-01 |
| CA2606889A1 (fr) | 2008-04-18 |
| EP1918005A1 (fr) | 2008-05-07 |
| CA2606889C (fr) | 2014-05-20 |
| US7625430B2 (en) | 2009-12-01 |
| BRPI0704030A (pt) | 2008-06-03 |
| US20080092738A1 (en) | 2008-04-24 |
| FR2907348B1 (fr) | 2008-12-12 |
| FR2907348A1 (fr) | 2008-04-25 |
| JP5448322B2 (ja) | 2014-03-19 |
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