CN101151343A - 可辐射固化的填充干燥剂的粘合剂/密封剂 - Google Patents
可辐射固化的填充干燥剂的粘合剂/密封剂 Download PDFInfo
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Abstract
Description
实施例1组分 | 重量份数 | |
1-a | 1-b | |
Sartomer SR833S | 50 | 50 |
微米级硅石 | 50 | 25 |
硫酸钙 | 0 | 25 |
Irgacure 651 | 0.5 | 0.5 |
粘合厚度(密耳) | 2 | 2 |
寿命(hrs) | 42 | 207 |
实施例2组分 | 重量份数 | ||
2-a | 2-b | 2-c | |
聚异丁烯(Mn=2300) | 35 | 35 | 35 |
Sartomer SR833S | 15 | 15 | 15 |
微米级硅石 | 50 | 25 | 25 |
硫酸钙 | 0 | 25 | 0 |
CaO | 0 | 0 | 25 |
Irgacure 651 | 0.5 | 0.5 | 0.5 |
粘合厚度(密耳) | 1 | 1 | 8.3 |
寿命(hrs) | 28 | 326 | 252 |
实施例3组分 | 重量份数 | ||
3-a | 3-b | 3-c | |
Epon 862 | 39 | 32 | 28 |
DCPD二乙烯基醚 | 17 | 21 | 19 |
光敏引发剂 | 0.25(CD1012) | 3(UV9380C) | 3(UV9380C) |
光敏剂 | 0.75(苝) | 0.15(ITX) | 0.15(ITX) |
滑石 | 45 | 23 | 20 |
分子筛 | 0 | 23 | 33 |
粘合厚度(密耳) | 2 | 3.5 | 2.8 |
寿命(hrs) | 27 | 92 | 52 |
表1.基于钙按纽寿命测量的密封剂/粘合剂的阻隔性能比较 | ||||||
实施例 | 组成,以重量份计 | 粘合层厚度(密耳) | 寿命 | |||
树脂 | 填料 | 光敏引发剂 | ||||
无干燥剂 | 干燥剂 | |||||
1-a自由基固化 | 50 | 50硅石 | 0.5 | 2 | 42 | |
1-b自由基固化 | 50 | 25硅石 | 25CaSO4 | 0.5 | 2 | 207 |
2-a自由基固化 | 50 | 50硅石 | 0.5 | 1 | 28 | |
2-b自由基固化 | 50 | 25硅石 | 25CaSO4 | 0.5 | 1 | 326 |
2-c自由基固化 | 50 | 25硅石 | 25CaO | 0.5 | 8.3 | 252 |
3-a阳离子固化 | 54 | 45滑石 | 1 | 2 | 26 | |
3-b阳离子固化 | 52 | 23滑石 | 23分子筛 | 1.5 | 2 | 92 |
3-c阳离子固化 | 46 | 20滑石 | 33分子筛 | 1 | 2 | 50 |
表2.如图2所述的基于钙按纽寿命测量的密封剂/粘合剂的阻隔性能比较 | ||||||
实施例 | 按重量计组合物份数 | 粘合层厚度(密耳) | 寿命 | |||
树脂 | 填料 | 光敏引发剂 | ||||
无干燥剂 | 干燥剂 | |||||
4-a自由基固化 | 100 | 0.3 | 1.3 | 88 | ||
4-b自由基固化 | 100 | 50分子筛 | 0.3 | 2.6 | 1225 | |
4-c自由基固化 | 100 | 50CaSO4 | 0.3 | 1.6 | 600 | |
4-d自由基固化 | 100 | 50CaO | 0.3 | 5.1 | 232 | |
4-e自由基固化 | 100 | 50CaCl2 | 0.3 | 5.6 | 191 | |
4-f自由基固化 | 100 | 50Al2O3 | 0.3 | 3.2 | 160 | |
4-g自由基固化 | 100 | 50K2CO3 | 0.3 | 3.5 | 170 | |
4-h自由基固化 | 100 | 50MgO | 0.3 | 1.9 | 126 |
表3:密封剂5(a)(无干燥剂)、5(b)(有分子筛)和5(c)(有球状硅石) | |||
组分 | 重量份数 | ||
5-a | 5-b | 5-c | |
Q43 | 2.96 | 2.96 | 2.96 |
TAIC | 1.93 | 1.93 | 1.93 |
(3-巯丙基)三甲氧基硅烷 | 0.15 | 0.15 | 0.15 |
Irgacure 651 | 0.097 | 0.097 | 0.097 |
Irganox 3052 | 基于总树脂的500ppm | ||
分子筛 | 2.5 | ||
微米级硅石 | 2.5 |
表4:密封剂6-a(无干燥剂)密封剂6-b(有干燥剂) | ||
组分 | 重量份数 | |
6-a | 6-b | |
马来酰亚胺树脂X | 80 | 80 |
马来酰亚胺树脂Y | 20 | 20 |
Irgacure 651 | 2 | 2 |
硫酸钙 | 0 | 43 |
湿气渗透,50℃/100%RH下(g·密耳/100in2·天) | 116 | 61 |
表5:密封剂7(a)(有干燥剂)和密封剂7(b)(无干燥剂) | ||
组分 | 重量份数 | |
7(a) | 7(b) | |
RDGE | 18.36 | 18.36 |
EPON 862 | 18.36 | 18.36 |
SR1012 | 0.74 | 0.74 |
ITX | 0.26 | 0.26 |
硅烷助粘剂 | 1.27 | 1.27 |
硫酸钙 | 15.20 | |
微米级硅石 | 45.81 | 72.27 |
总填料 | 61.01 | 72.27 |
合计: | 100 | 111.25 |
树脂或填料 | 份数 |
EPON 862(BPFDGE) | 24.7 |
脂环族乙烯基醚 | 17.2 |
硅烷助粘剂 | 0.2 |
锍盐光敏引发剂 | 0.9 |
熔凝硅石触变胶(thixotrope) | 2 |
微米级硅石 | 27.5 |
粉末4埃分子筛(平均粒径<5微米) | 27.5 |
Claims (49)
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Application Number | Priority Date | Filing Date | Title |
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US11/098,117 | 2005-04-04 | ||
US11/098,117 US7687119B2 (en) | 2005-04-04 | 2005-04-04 | Radiation-curable desiccant-filled adhesive/sealant |
US11/393,496 US7462651B2 (en) | 2005-04-04 | 2006-03-30 | Radiation-curable desiccant-filled adhesive/sealant |
PCT/US2006/011898 WO2006107748A1 (en) | 2005-04-04 | 2006-03-30 | Radiation-curable desiccant-filled adhesive/sealant |
US11/393,496 | 2006-03-30 |
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