CN100547014C - 高折射率聚硅氧烷及其制备 - Google Patents

高折射率聚硅氧烷及其制备 Download PDF

Info

Publication number
CN100547014C
CN100547014C CNB028166167A CN02816616A CN100547014C CN 100547014 C CN100547014 C CN 100547014C CN B028166167 A CNB028166167 A CN B028166167A CN 02816616 A CN02816616 A CN 02816616A CN 100547014 C CN100547014 C CN 100547014C
Authority
CN
China
Prior art keywords
sub
sup
polysiloxane
refractive index
units
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB028166167A
Other languages
English (en)
Chinese (zh)
Other versions
CN1636031A (zh
Inventor
P·切瓦里尔
区端力
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Silicones Corp
Original Assignee
Dow Corning Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Corning Corp filed Critical Dow Corning Corp
Publication of CN1636031A publication Critical patent/CN1636031A/zh
Application granted granted Critical
Publication of CN100547014C publication Critical patent/CN100547014C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/14—Polysiloxanes containing silicon bound to oxygen-containing groups
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
    • C09D183/04—Polysiloxanes
    • C09D183/08—Polysiloxanes containing silicon bound to organic groups containing atoms other than carbon, hydrogen, and oxygen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C07F7/121—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
    • C07F7/122—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving the formation of Si-C linkages
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/22—Polysiloxanes containing silicon bound to organic groups containing atoms other than carbon, hydrogen and oxygen
    • C08G77/24—Polysiloxanes containing silicon bound to organic groups containing atoms other than carbon, hydrogen and oxygen halogen-containing groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/38—Polysiloxanes modified by chemical after-treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/38—Polysiloxanes modified by chemical after-treatment
    • C08G77/382—Polysiloxanes modified by chemical after-treatment containing atoms other than carbon, hydrogen, oxygen or silicon
    • C08G77/385—Polysiloxanes modified by chemical after-treatment containing atoms other than carbon, hydrogen, oxygen or silicon containing halogens
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
    • C09D183/04—Polysiloxanes
    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
    • G02B1/04—Optical elements characterised by the material of which they are made; Optical coatings for optical elements made of organic materials, e.g. plastics

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Silicon Polymers (AREA)
  • Paints Or Removers (AREA)
CNB028166167A 2001-07-28 2002-07-18 高折射率聚硅氧烷及其制备 Expired - Fee Related CN100547014C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB0118473.8 2001-07-28
GBGB0118473.8A GB0118473D0 (en) 2001-07-28 2001-07-28 High refractive index polysiloxanes and their preparation

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN2009101680340A Division CN101633735B (zh) 2001-07-28 2002-07-18 高折射率聚硅氧烷及其制备

Publications (2)

Publication Number Publication Date
CN1636031A CN1636031A (zh) 2005-07-06
CN100547014C true CN100547014C (zh) 2009-10-07

Family

ID=9919401

Family Applications (2)

Application Number Title Priority Date Filing Date
CN2009101680340A Expired - Fee Related CN101633735B (zh) 2001-07-28 2002-07-18 高折射率聚硅氧烷及其制备
CNB028166167A Expired - Fee Related CN100547014C (zh) 2001-07-28 2002-07-18 高折射率聚硅氧烷及其制备

Family Applications Before (1)

Application Number Title Priority Date Filing Date
CN2009101680340A Expired - Fee Related CN101633735B (zh) 2001-07-28 2002-07-18 高折射率聚硅氧烷及其制备

Country Status (9)

Country Link
US (1) US7429638B2 (enExample)
EP (1) EP1417252B1 (enExample)
JP (1) JP2004536210A (enExample)
KR (3) KR20040030870A (enExample)
CN (2) CN101633735B (enExample)
AU (1) AU2002321283A1 (enExample)
CA (1) CA2455331A1 (enExample)
GB (1) GB0118473D0 (enExample)
WO (1) WO2003011944A2 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104487516A (zh) * 2012-07-19 2015-04-01 东丽株式会社 聚硅氧烷组合物、电子器件及光学器件

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0118473D0 (en) 2001-07-28 2001-09-19 Dow Corning High refractive index polysiloxanes and their preparation
JP5296297B2 (ja) 2005-04-04 2013-09-25 東レ・ファインケミカル株式会社 縮合多環式炭化水素基を有するシリコーン共重合体及びその製造方法
JP4800383B2 (ja) * 2005-05-26 2011-10-26 ダウ・コーニング・コーポレイション 小さい形状を成形するための方法およびシリコーン封止剤組成物
KR101325792B1 (ko) * 2006-01-17 2013-11-04 다우 코닝 코포레이션 열 안정성 투명 실리콘 수지 조성물 및 이의 제조 방법 및용도
EP1979774A1 (en) * 2006-02-01 2008-10-15 Dow Corning Corporation Impact resistant optical waveguide and method of manufacture thereof
EP1987084B1 (en) * 2006-02-24 2014-11-05 Dow Corning Corporation Light emitting device encapsulated with silicones and curable silicone compositions for preparing the silicones
US8222364B2 (en) * 2006-04-11 2012-07-17 Dow Corning Corporation Composition including a siloxane and a method of forming the same
US20070272934A1 (en) * 2006-05-23 2007-11-29 Kee Yean Ng LED device with improved life performance
US20070284687A1 (en) * 2006-06-13 2007-12-13 Rantala Juha T Semiconductor optoelectronics devices
TWI473255B (zh) * 2006-07-13 2015-02-11 Silecs Oy 半導體光電裝置
JP5035770B2 (ja) * 2007-02-16 2012-09-26 東レ・ファインケミカル株式会社 縮合多環式炭化水素基を有するシリコーン共重合体、及び、その製造方法
KR101430261B1 (ko) * 2007-02-23 2014-08-14 삼성전자주식회사 유기 실리콘 나노클러스터, 이의 제조방법, 이를 이용한박막형성 방법
JP5318383B2 (ja) * 2007-08-07 2013-10-16 デクセリアルズ株式会社 光学部品封止材及び発光装置
EP2422845B1 (en) 2010-08-24 2013-04-24 Polyphotonix Limited Lightguide phototherapy apparatus
EP2422844A1 (en) 2010-08-24 2012-02-29 Polyphotonix Limited Wearable phototherapy device
US8258636B1 (en) 2011-05-17 2012-09-04 Rohm And Haas Electronic Materials Llc High refractive index curable liquid light emitting diode encapsulant formulation
US8257988B1 (en) 2011-05-17 2012-09-04 Rohm And Haas Electronic Materials Llc Method of making light emitting diodes
KR20140048240A (ko) * 2011-07-07 2014-04-23 다우 코닝 도레이 캄파니 리미티드 오르가노폴리실록산 및 그 제조 방법
JPWO2013005858A1 (ja) * 2011-07-07 2015-02-23 東レ・ダウコーニング株式会社 硬化性シリコーン組成物、その硬化物、および光半導体装置
US8455607B2 (en) 2011-08-17 2013-06-04 Rohm And Haas Electronic Materials Llc Curable liquid composite light emitting diode encapsulant
US8450445B2 (en) 2011-08-17 2013-05-28 Rohm And Haas Electronic Materials Llc Light emitting diode manufacturing method
JP6022236B2 (ja) * 2012-06-28 2016-11-09 東レ・ダウコーニング株式会社 コーティング剤、電気・電子機器、および電気・電子機器の金属部の保護方法
JP2014077117A (ja) * 2012-09-21 2014-05-01 Dow Corning Toray Co Ltd 高屈折性表面処理剤、それを用いて表面処理された微細部材および光学材料
TWI689533B (zh) * 2014-03-28 2020-04-01 美商道康寧公司 包含與多氟聚醚矽烷反應的固化聚有機矽氧烷中間物之共聚物組成物及其相關形成方法
JP7357505B2 (ja) * 2018-11-21 2023-10-06 信越化学工業株式会社 ヨウ素含有熱硬化性ケイ素含有材料、これを含むｅｕｖリソグラフィー用レジスト下層膜形成用組成物、及びパターン形成方法
JP7368324B2 (ja) 2019-07-23 2023-10-24 信越化学工業株式会社 ケイ素含有レジスト下層膜形成用組成物及びパターン形成方法
US11685702B2 (en) * 2019-12-20 2023-06-27 Jsi Silicone Co. Method for producing arene compounds and arene compounds produced by the same
DE102020118247A1 (de) * 2020-07-10 2022-01-13 OSRAM Opto Semiconductors Gesellschaft mit beschränkter Haftung Precursor zur Herstellung eines Polysiloxans, Polysiloxan, Polysiloxanharz, Verfahren zur Herstellung eines Polysiloxans, Verfahren zur Herstellung eines Polysiloxanharzes und optoelektronisches Bauelement

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6084050A (en) * 1997-01-09 2000-07-04 Nippon Telegraph And Telephone Corporation Thermo-optic devices

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2528355A (en) * 1949-09-14 1950-10-31 Dow Corning Halogenated xenyl trichlorosilanes
US5260469A (en) * 1992-03-26 1993-11-09 Ppg Industries, Inc. Organo-siloxane with modified solubility
US5233007A (en) * 1992-04-14 1993-08-03 Allergan, Inc. Polysiloxanes, methods of making same and high refractive index silicones made from same
WO1994008557A1 (en) 1992-10-22 1994-04-28 The Procter & Gamble Company Hair care compositions providing conditioning and enhanced shine
JPH0782378A (ja) * 1993-09-10 1995-03-28 Nippon Telegr & Teleph Corp <Ntt> シロキサン共重合体およびその合成方法
US5384383A (en) * 1994-01-31 1995-01-24 Dow Corning Corporation Pristine phenylpropylalkylsiloxanes
US5539137A (en) * 1995-06-07 1996-07-23 General Electic Company Aryl substituted silicone fluids having high refractive indices and method for making
DE69911529T2 (de) * 1998-02-05 2004-08-05 Nippon Sheet Glass Co., Ltd. Gegenstand mit unebener oberfläche, verfahren zu dessen herstellung und zusammenstellung dafür
JPH11310755A (ja) 1998-04-27 1999-11-09 Seiko Epson Corp コーティング用組成物及び積層体
JP2000231001A (ja) * 1999-02-10 2000-08-22 Konica Corp 光学用レンズ
US6285513B1 (en) * 1999-02-10 2001-09-04 Konica Corporation Optical element
JP4127599B2 (ja) 2001-02-07 2008-07-30 Ｔｄｋ株式会社 焼結体の製造方法及びこれにより製造される焼結体と磁歪材料
GB0118473D0 (en) 2001-07-28 2001-09-19 Dow Corning High refractive index polysiloxanes and their preparation

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6084050A (en) * 1997-01-09 2000-07-04 Nippon Telegraph And Telephone Corporation Thermo-optic devices

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104487516A (zh) * 2012-07-19 2015-04-01 东丽株式会社 聚硅氧烷组合物、电子器件及光学器件
CN104487516B (zh) * 2012-07-19 2017-10-24 东丽株式会社 聚硅氧烷组合物、电子器件及光学器件

Also Published As

Publication number Publication date
US20040236057A1 (en) 2004-11-25
KR20040030870A (ko) 2004-04-09
GB0118473D0 (en) 2001-09-19
EP1417252A2 (en) 2004-05-12
EP1417252B1 (en) 2015-07-01
KR20090016019A (ko) 2009-02-12
CN1636031A (zh) 2005-07-06
WO2003011944A2 (en) 2003-02-13
CN101633735B (zh) 2011-07-20
KR20100024506A (ko) 2010-03-05
JP2004536210A (ja) 2004-12-02
AU2002321283A1 (en) 2003-02-17
WO2003011944A3 (en) 2003-05-08
CA2455331A1 (en) 2003-02-13
US7429638B2 (en) 2008-09-30
CN101633735A (zh) 2010-01-27

Similar Documents

Publication Publication Date Title
CN100547014C (zh) 高折射率聚硅氧烷及其制备
Sellinger et al. Silsesquioxanes as synthetic platforms. Thermally curable and photocurable inorganic/organic hybrids
Matějka et al. Cyclization and self-organization in polymerization of trialkoxysilanes
Shea et al. A mechanistic investigation of gelation. The sol− gel polymerization of precursors to bridged polysilsesquioxanes
Uhlig et al. 29 Si NMR Some Practical Aspects
CN103890100B (zh) 硅氧烷系组合物及其固化物以及其用途
TWI622594B (zh) 多面體寡聚矽倍半氧烷與其製備方法、包括其的塗佈組成物及抗反射膜
JPH08311205A (ja) カルボシラン−デンドリマー類、カルボシラン−ハイブリツド材料、これらの製造方法およびこのカルボシラン−デンドリマー類から被覆材を製造する方法
JPH06184310A (ja) 高屈折率のフェノール変性シロキサン
JP2000026610A (ja) 硼素―および／またはアルミニウム―含有混合物、混成材料およびコ―チング
WO2020175159A1 (ja) 無機酸化物粒子、無機酸化物粒子分散液及びその製造方法、並びに表面修飾剤の製造方法
CN111484621A (zh) 聚硅氧硅氮烷化合物、其制备方法和包含其的组合物及其固化产物
CN104870527A (zh) 金属氧化物纳米颗粒与硅倍半氧烷聚合物的复合物及其制造方法、以及使用该复合物而制造的复合材料
JPH07224075A (ja) 純粋なフェニルプロピルアルキルシロキサン
CN119013333A (zh) 化合物、组合物、表面处理剂、物品和物品的制造方法
CN108137812A (zh) 含氢硅烷基有机硅树脂的制造方法
CN102439070A (zh) 反应性无机簇
CN101899156A (zh) 一种多链梯形聚烷基硅倍半氧烷的制备方法
JP4162060B2 (ja) 低誘電率シリカ系被膜形成用塗布液および低誘電率被膜付基材
Li et al. Cesium carbonate-catalyzed oxidation of substituted phenylsilanes for the efficient synthesis of polyhedral oligomeric silsesquioxanes
JPH06346025A (ja) コーティング用組成物
Hanuhov et al. Evaluation of opto-mechanical properties of UV-cured and thermally-cured sol-gel hybrids monoliths as a function of organic content and curing process
JPH09176323A (ja) フッ素化シリコーン樹脂及びその製造方法
Dirè et al. Hybrid organic/inorganic materials for photonic applications via assembling of nanostructured molecular units
Baney et al. Polysilsesquioxanes

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CP03 Change of name, title or address
CP03 Change of name, title or address

Address after: michigan

Patentee after: Dow organosilicon company

Address before: Michigan

Patentee before: Dow Corning Corporation

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20091007

Termination date: 20200718