CN100494156C - 生产水含量减少的(甲基)丙烯酸的方法 - Google Patents

生产水含量减少的(甲基)丙烯酸的方法 Download PDF

Info

Publication number
CN100494156C
CN100494156C CNB2004100953352A CN200410095335A CN100494156C CN 100494156 C CN100494156 C CN 100494156C CN B2004100953352 A CNB2004100953352 A CN B2004100953352A CN 200410095335 A CN200410095335 A CN 200410095335A CN 100494156 C CN100494156 C CN 100494156C
Authority
CN
China
Prior art keywords
methyl
aldehyde
materials flow
vinylformic acid
tower
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB2004100953352A
Other languages
English (en)
Chinese (zh)
Other versions
CN1636958A (zh
Inventor
A·本德里
M·S·德库西
A·索菲克
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rohm and Haas Co
Original Assignee
Rohm and Haas Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rohm and Haas Co filed Critical Rohm and Haas Co
Publication of CN1636958A publication Critical patent/CN1636958A/zh
Application granted granted Critical
Publication of CN100494156C publication Critical patent/CN100494156C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/52Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/487Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CNB2004100953352A 2003-11-26 2004-11-19 生产水含量减少的(甲基)丙烯酸的方法 Expired - Fee Related CN100494156C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US52525803P 2003-11-26 2003-11-26
US60/525,258 2003-11-26

Related Child Applications (2)

Application Number Title Priority Date Filing Date
CN201210297096.3A Division CN102786408B (zh) 2003-11-26 2004-11-19 生产水含量减少的(甲基)丙烯酸的方法
CN2009101414037A Division CN101555200B (zh) 2003-11-26 2004-11-19 生产水含量减少的(甲基)丙烯酸的方法

Publications (2)

Publication Number Publication Date
CN1636958A CN1636958A (zh) 2005-07-13
CN100494156C true CN100494156C (zh) 2009-06-03

Family

ID=34465394

Family Applications (3)

Application Number Title Priority Date Filing Date
CNB2004100953352A Expired - Fee Related CN100494156C (zh) 2003-11-26 2004-11-19 生产水含量减少的(甲基)丙烯酸的方法
CN201210297096.3A Expired - Fee Related CN102786408B (zh) 2003-11-26 2004-11-19 生产水含量减少的(甲基)丙烯酸的方法
CN2009101414037A Expired - Fee Related CN101555200B (zh) 2003-11-26 2004-11-19 生产水含量减少的(甲基)丙烯酸的方法

Family Applications After (2)

Application Number Title Priority Date Filing Date
CN201210297096.3A Expired - Fee Related CN102786408B (zh) 2003-11-26 2004-11-19 生产水含量减少的(甲基)丙烯酸的方法
CN2009101414037A Expired - Fee Related CN101555200B (zh) 2003-11-26 2004-11-19 生产水含量减少的(甲基)丙烯酸的方法

Country Status (8)

Country Link
US (3) US7393976B2 (https=)
EP (1) EP1535894B1 (https=)
JP (3) JP4090465B2 (https=)
KR (2) KR100710858B1 (https=)
CN (3) CN100494156C (https=)
BR (1) BRPI0405080B1 (https=)
DE (1) DE602004017107D1 (https=)
TW (1) TWI263634B (https=)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7615806B2 (en) 2005-10-31 2009-11-10 Freescale Semiconductor, Inc. Method for forming a semiconductor structure and structure thereof
DE102006062258A1 (de) * 2006-12-22 2008-06-26 Basf Se Verfahren zum Übertragen von Wärme auf ein wenigstens ein (Meth)acrylmonomeres enthaltendes flüssiges Gemsich
JP5739600B2 (ja) * 2007-12-17 2015-06-24 三菱レイヨン株式会社 ヒドロキシエチルメタクリレートの製造方法
EP2135656A1 (en) * 2008-05-30 2009-12-23 Rohm and Haas Company Method for production of purified (Meth)acrylic acid
DE102008043609A1 (de) * 2008-11-10 2010-05-12 Evonik Röhm Gmbh Verfahren zur Reduzierung des Wassergehalts in (Meth)acrylsäure
JP5731390B2 (ja) 2009-09-30 2015-06-10 株式会社日本触媒 ポリアクリル酸(塩)系吸水性樹脂およびその製造方法
KR20140004697A (ko) * 2010-12-29 2014-01-13 롬 앤드 하스 캄파니 (메트)아크릴산 제조 공정에서 장치 오염을 줄이는 방법
CN106471041B (zh) * 2014-07-03 2019-12-20 科思创德国股份有限公司 纯化聚碳酸酯多元醇的方法及其纯化装置
EP3333150B1 (en) * 2015-08-07 2020-09-16 Daikin Industries, Ltd. Method for purifying acrylic acid derivative
DE102016116078B3 (de) 2016-08-29 2018-01-04 Epc Engineering Consulting Gmbh Verfahren zur Herstellung eines Polycarbonats unter Einsatz einer Strippvorrichtung
GB201621985D0 (en) 2016-12-22 2017-02-08 Johnson Matthey Davy Technologies Ltd Process
GB201621975D0 (en) 2016-12-22 2017-02-08 Johnson Matthey Davy Technologies Ltd Process
FR3064630B1 (fr) * 2017-04-04 2019-09-13 Arkema France Procede de purification d'acide (meth)acrylique incluant une colonne de distillation a paroi separatrice
FR3094716B1 (fr) 2019-04-02 2021-06-04 Arkema France Production d’acide acrylique de grade polymere
EP3990425B1 (en) * 2019-06-25 2025-01-22 Evonik Operations GmbH Process for distillative purification of unsaturated carboxylic anhydrides
CN110563943A (zh) * 2019-09-09 2019-12-13 中国科学院长春应用化学研究所 一种生物基聚合物及其制备方法
FR3108906B1 (fr) 2020-04-06 2022-03-04 Arkema France Procede de purification d’acide (meth)acrylique
JP7537681B2 (ja) * 2020-09-15 2024-08-21 株式会社日本触媒 アクリル酸の製造方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3725208A (en) * 1971-08-20 1973-04-03 Nippon Kayaku Kk Process for purification of acrylic acid from aldehydes by distillation with a reagent
CN1149573A (zh) * 1995-10-27 1997-05-14 罗姆和哈斯公司 纯品位丙烯酸的生产方法

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA962698A (en) * 1972-01-31 1975-02-11 The Standard Oil Company Process for purification of acrylic acid
DE4335172A1 (de) * 1993-10-15 1995-04-20 Basf Ag Verfahren zur Reinigung von Roh-(Meth)acrylsäure
US5523480A (en) * 1994-03-28 1996-06-04 Rohm And Haas Company Process for purifying unsaturated carboxylic acids using distillation and melt crystallization
US5571386A (en) * 1994-05-31 1996-11-05 Rohm And Haas Company Process for grade acrylic acid
JP3937462B2 (ja) * 1994-08-04 2007-06-27 三菱化学株式会社 アクリル酸精製法
US5482597A (en) * 1994-11-23 1996-01-09 Basf Aktiengesellschaft Purification of crude (meth)acrylic acid
JPH09208515A (ja) * 1996-02-07 1997-08-12 Idemitsu Petrochem Co Ltd アクリル酸の製造方法
DE19624674A1 (de) 1996-06-20 1998-01-02 Basf Ag Verfahren zur Entsorgung von bei der Acrylsäure- oder Methacrylsäure-Herstellung anfallenden Nebenkomponenten
JPH1087552A (ja) * 1996-09-11 1998-04-07 Mitsubishi Chem Corp 高純度アクリル酸の製造方法
DE19814449A1 (de) * 1998-03-31 1999-10-07 Basf Ag Verfahren zur Herstellung von (Meth)acrylsäure und (Meth)acrylsäureestern
TW553929B (en) * 1999-03-05 2003-09-21 Rohm & Haas Process for preparing (meth)acrylic acid
JP5073129B2 (ja) 1999-03-31 2012-11-14 株式会社日本触媒 (メタ)アクリル酸の精製方法
DE60000708T2 (de) * 1999-06-28 2003-07-24 Rohm And Haas Co., Philadelphia Verfahren zur Herstellung von (Meth)acrylsäure
US6639106B1 (en) 1999-07-23 2003-10-28 Rohm And Haas Company Process for preparing and purifying acrylic acid from propylene having improved capacity
JP3938646B2 (ja) * 2000-01-14 2007-06-27 株式会社日本触媒 アクリル酸の製造方法
JP4601120B2 (ja) * 2000-05-08 2010-12-22 出光興産株式会社 アクリル酸の製造方法
US6927268B2 (en) * 2000-06-21 2005-08-09 Nippon Shokubai Co., Ltd. Production process for water-absorbent resin
JP4765165B2 (ja) * 2000-12-13 2011-09-07 東亞合成株式会社 高純度アクリル酸の製造方法
JP4759153B2 (ja) * 2001-03-21 2011-08-31 株式会社日本触媒 (メタ)アクリル酸溶液の蒸留方法
JP4034559B2 (ja) * 2001-12-11 2008-01-16 三菱化学株式会社 (メタ)アクリル酸類の蒸留方法
JP4440518B2 (ja) * 2002-07-16 2010-03-24 株式会社日本触媒 アクリル酸の製造方法
JP3905810B2 (ja) * 2002-09-03 2007-04-18 株式会社日本触媒 アクリル酸製造プロセスにおける重合防止方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3725208A (en) * 1971-08-20 1973-04-03 Nippon Kayaku Kk Process for purification of acrylic acid from aldehydes by distillation with a reagent
CN1149573A (zh) * 1995-10-27 1997-05-14 罗姆和哈斯公司 纯品位丙烯酸的生产方法

Also Published As

Publication number Publication date
JP4850190B2 (ja) 2012-01-11
JP4090465B2 (ja) 2008-05-28
CN101555200B (zh) 2012-11-14
KR20050050552A (ko) 2005-05-31
US7393976B2 (en) 2008-07-01
EP1535894A1 (en) 2005-06-01
CN102786408A (zh) 2012-11-21
JP2011231133A (ja) 2011-11-17
US20110105708A1 (en) 2011-05-05
TWI263634B (en) 2006-10-11
BRPI0405080B1 (pt) 2015-04-22
KR100766830B1 (ko) 2007-10-17
JP2008120823A (ja) 2008-05-29
US20090030165A1 (en) 2009-01-29
DE602004017107D1 (de) 2008-11-27
CN101555200A (zh) 2009-10-14
KR20060107963A (ko) 2006-10-16
EP1535894B1 (en) 2008-10-15
US20050113605A1 (en) 2005-05-26
KR100710858B1 (ko) 2007-04-25
TW200524853A (en) 2005-08-01
CN1636958A (zh) 2005-07-13
CN102786408B (zh) 2014-12-03
BRPI0405080A (pt) 2005-07-19
JP2005154445A (ja) 2005-06-16

Similar Documents

Publication Publication Date Title
CN100494156C (zh) 生产水含量减少的(甲基)丙烯酸的方法
JP5199260B2 (ja) アクリル酸の生成方法
CN108137469B (zh) 改进的用于制备聚合物级的(甲基)丙烯酸的方法
TWI258384B (en) High capacity purification of thermally unstable compounds
KR20160122749A (ko) 아크릴산의 제조 공정 및 시스템
US10815182B2 (en) Process for purifying (meth)acrylic acid including a dividing-wall distillation column
US7300555B2 (en) Method for the rectifying separation of liquids containing (meth)acrylic monomers in a rectification column
EP1459794A2 (en) Apparatus and process for purification of acrylic acid family
SA03240268B1 (ar) طريقة لمنع البلمرة polymerization في عملية تصنيع حمض الاكريليك acrylic acid
US7253313B2 (en) Method for purifying (meth)acrylic acid by oxidising a gaseous substrate
RU2350598C2 (ru) Способ очистки (мет)акриловой кислоты
US20230109749A1 (en) Method for purifying (meth)acrylic acid
CN101119959A (zh) 通过质子溶剂萃取从含有(甲基)丙烯酸的混合物中回收有机化合物的方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20090603

Termination date: 20201119