CN100457879C - 制备富含非母育酚型高熔点不皂化物的植物油级分的方法 - Google Patents
制备富含非母育酚型高熔点不皂化物的植物油级分的方法 Download PDFInfo
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- CN100457879C CN100457879C CNB018218970A CN01821897A CN100457879C CN 100457879 C CN100457879 C CN 100457879C CN B018218970 A CNB018218970 A CN B018218970A CN 01821897 A CN01821897 A CN 01821897A CN 100457879 C CN100457879 C CN 100457879C
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- 235000021163 supper Nutrition 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 229960000984 tocofersolan Drugs 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
- QURCVMIEKCOAJU-UHFFFAOYSA-N trans-isoferulic acid Natural products COC1=CC=C(C=CC(O)=O)C=C1O QURCVMIEKCOAJU-UHFFFAOYSA-N 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- 239000010497 wheat germ oil Substances 0.000 description 1
- 239000002076 α-tocopherol Substances 0.000 description 1
- 235000004835 α-tocopherol Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D7/00—Edible oil or fat compositions containing an aqueous phase, e.g. margarines
- A23D7/005—Edible oil or fat compositions containing an aqueous phase, e.g. margarines characterised by ingredients other than fatty acid triglycerides
- A23D7/0056—Spread compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P3/00—Drugs for disorders of the metabolism
- A61P3/06—Antihyperlipidemics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
- C11B7/0008—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
- C11B7/0016—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents in hydrocarbons or halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
- C11C3/10—Ester interchange
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/12—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by hydrogenation
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Chemical & Material Sciences (AREA)
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- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Mycology (AREA)
- Pharmacology & Pharmacy (AREA)
- Medicinal Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Botany (AREA)
- Epidemiology (AREA)
- Wood Science & Technology (AREA)
- Nutrition Science (AREA)
- Microbiology (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Dermatology (AREA)
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- Diabetes (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Obesity (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Birds (AREA)
- Fats And Perfumes (AREA)
- Edible Oils And Fats (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Cosmetics (AREA)
- Seasonings (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Description
对象 | 实施例1菜籽 | 实施例2菜籽 | 实施例3牛油树脂 | 实施例3牛油树脂 |
起始油中的不皂化物含量,% | 0.9 | 0.9 | 12.5 | 12.5 |
混合物中的载体油含量,% | 2 | 5 | 10 | 20 |
富集级分的产率,% | 5.9 | 8.2 | 21.0 | 29.0 |
富集级分中不皂化物的含量,% | 14.5 | 10.9 | 53.0 | 38.1 |
富集倍数 | 16.1 | 12.1 | 4.2 | 3.0 |
不皂化物的回收率,% | 94.4 | 98.4 | 89.0 | 88.4 |
不皂化物的类型 | 牛油树脂 | 牛油树脂的液体级分 | 脱聚戊二烯烃化牛油树脂的液体级分 |
TTPAs和酯类 | 65% | 70% | 85% |
植物甾醇和其它 | 6% | 6% | 8% |
西非牛油树烃 | 29% | 24% | 7% |
参数 | 起始油 | 富集级分 |
总的不皂化物,% | 0.9 | 14.5 |
总的生育酚,ppm | 698 | 5593 |
总的反式脂肪酸,% | bdl | 1.0 |
对总的不皂化物计算的富集倍数 | 16.1 | |
对总的生育酚计算的富集倍数 | 8.0 |
参数 | 起始油 | 富集级分 |
总的不皂化物,% | 0.9 | 10.9 |
总的生育酚,ppm | 698 | 5322 |
总的反式脂肪酸,% | bdl | 22.8 |
对总的不皂化物计算的富集倍数 | 12.1 | |
对总的生育酚计算的富集倍数 | 7.6 | |
级分的产量,以g计 | 82 |
不皂化物的回收量,以g计 | 8.9 | |
总物质的回收率,以%计 | 98.9 |
配料 | CTFA/INCI名称 | %w/w |
牛油树脂级分II | 牛油树脂(Butyro-spermum Parkii)提取物 | 2.00 |
“Cremeol VP” | 植物油(和)氢化植物油(和)烛木蜡(Euphorbia Cerifera) | 73.40 |
“Cremeol HF-52” | 氢化植物油 | 13.00 |
蜂蜡 | 蜂蜡 | 7.80 |
巴西棕榈蜡 | 巴西棕榈蜡(Copernicia Cerifera) | 3.80 |
芳香剂 | 适量 |
向日葵 | 牛油树坚果 | |
Body Fat 62<sup>1</sup>(g/100g) | 19.66<sup>3</sup> | 19.66<sup>3</sup> |
Solex<sup>2</sup>(g/100g) | 58.98<sup>4</sup> | 29.17<sup>4</sup> |
牛油树坚果油(g/100g) | 29.81 | |
脂溶性成分(g/100g) | 1.36 | 1.36 |
水相(g/100g) | 20.00 | 20.00 |
饱和脂肪酸(wt%,甘油酯的形式): | 25.9 | 34.4 |
-月桂酸(C12:0) | 4.0 | 4.6 |
-肉豆蔻酸(C14:0) | 1.8 | 2.1 |
-棕榈酸(C16:0) | 15.6 | 16.3 |
-硬脂酸(C18:0) | 4.1 | 11.0 |
-花生酸(C20:0) | 0.4 | 0.4 |
单不饱和脂肪酸(wt%,甘油酯的形式): | 22.5 | 31.9 |
-十六碳烯酸(C16:1,9c) | 0.1 | 0.1 |
-油酸(C18:1,9c) | 22.2 | 31.6 |
-顺9-二十碳烯酸(C20:1,9c) | 0.2 | 0.2 |
多不饱和脂肪酸(wt%,甘油酯的形式): | 50.2 | 31.9 |
-亚油酸(C18:2,9c,12c) | 49.9 | 31.7 |
-α-亚麻酸(C18:3,9c,12c,15c) | 0.3 | 0.2 |
反式脂肪酸(wt%,甘油酯的形式) | 0.4 | 0.7 |
非-甘油酯类(脂肪相的wt%): | 1.1 | 12.6 |
-三萜烯乙酸酯 | 2.2 | |
-三萜烯肉桂酸酯 | 5.9 | |
-三萜烯脂肪酸酯 | 3.5 | |
-游离三萜烯醇和甾醇 | 0.3 | 0.3 |
-西非牛油树烃<sup>5</sup> | 0.7 |
Claims (35)
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DKPA200001917 | 2000-12-21 | ||
DKPA200001917 | 2000-12-21 | ||
US26059101P | 2001-01-09 | 2001-01-09 | |
US60/260,591 | 2001-01-09 |
Publications (2)
Publication Number | Publication Date |
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CN1511189A CN1511189A (zh) | 2004-07-07 |
CN100457879C true CN100457879C (zh) | 2009-02-04 |
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CNB018218970A Expired - Fee Related CN100457879C (zh) | 2000-12-21 | 2001-12-20 | 制备富含非母育酚型高熔点不皂化物的植物油级分的方法 |
Country Status (7)
Country | Link |
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EP (1) | EP1343860B1 (zh) |
JP (1) | JP4351843B2 (zh) |
CN (1) | CN100457879C (zh) |
AU (2) | AU2002256554B2 (zh) |
CA (1) | CA2431495A1 (zh) |
NZ (1) | NZ526811A (zh) |
WO (1) | WO2002050221A1 (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103814056A (zh) * | 2011-11-03 | 2014-05-21 | 纳美仕有限公司 | 树脂组合物 |
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JP5280029B2 (ja) * | 2007-09-19 | 2013-09-04 | サントリーホールディングス株式会社 | セサミン類とγ−オリザノールとを含有する組成物 |
JP5554985B2 (ja) * | 2009-12-25 | 2014-07-23 | 日清オイリオグループ株式会社 | 化粧料用組成物、化粧料及び当該化粧料の製造方法 |
CN101914076B (zh) * | 2010-07-26 | 2012-08-22 | 江阴市向阳科技有限公司 | 一种无毒环保型环氧增塑剂制备方法 |
ITMI20110507A1 (it) * | 2011-03-29 | 2012-09-30 | Biophil Italia Spa | Composizione per uso cosmetico a base di trigliceridi di origine vegetale |
FR2978451B1 (fr) * | 2011-07-28 | 2015-01-30 | Expanscience Lab | Extraction solide / liquide avec un solvant comprenant au moins 5 atomes de carbone et 1 ou 2 atomes d'oxygene |
FR2985665B1 (fr) * | 2012-01-13 | 2015-10-02 | Expanscience Lab | Utilisation de peau d'avocat pour obtenir un insaponifiable d'avocat enrichi en hydrocarbures aliphatiques satures et en sterols |
US9499768B2 (en) | 2012-09-07 | 2016-11-22 | Aak Ab (Publ) | Method for processing a vegetable fat composition |
CN103461513A (zh) * | 2013-09-18 | 2013-12-25 | 贵州大学 | 苏麻夸克奶酪及其制备方法 |
US9809618B2 (en) * | 2013-09-30 | 2017-11-07 | Aak Ab | Enrichment of triterpine esters |
CN110312783B (zh) * | 2017-02-23 | 2023-09-15 | 不二制油集团控股株式会社 | 牛油树油精及其制造法 |
JP7000071B2 (ja) * | 2017-08-15 | 2022-01-19 | 昭和産業株式会社 | 加熱調理用油脂組成物 |
CN109745237A (zh) * | 2019-03-18 | 2019-05-14 | 佛山市宏奇生物科技有限公司 | 一种水解霍霍巴酯的制备工艺 |
CN114269161A (zh) * | 2019-06-21 | 2022-04-01 | 阿比尔技术公司 | 从植物物质中萃取的化合物及其制备方法 |
CN112042767B (zh) * | 2020-08-29 | 2022-06-14 | 江南大学 | 一种具有降低血脂和胆固醇的食用植物调和油 |
BR112023019338A2 (pt) * | 2021-03-22 | 2023-12-12 | Aak Ab Publ | Composição análoga a laticínios, produto alimentar, uso de uma composição de gordura em uma composição análoga a laticínios, e, processo para fabricar uma composição análoga a laticínios ou um produto alimentar |
CN113588814A (zh) * | 2021-07-08 | 2021-11-02 | 华东理工大学 | 一种植物油的品质分析方法 |
JP7409579B1 (ja) | 2022-03-28 | 2024-01-09 | 不二製油株式会社 | シア脂分別画分 |
FR3135729A1 (fr) * | 2022-04-26 | 2023-11-24 | La Fabrique Vegetale | EXTRAIT de beurre de karité enrichi en insaponifiable détriterpéné |
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2001
- 2001-12-20 CA CA002431495A patent/CA2431495A1/en not_active Abandoned
- 2001-12-20 NZ NZ526811A patent/NZ526811A/en not_active IP Right Cessation
- 2001-12-20 AU AU2002256554A patent/AU2002256554B2/en not_active Ceased
- 2001-12-20 EP EP01271427A patent/EP1343860B1/en not_active Expired - Lifetime
- 2001-12-20 JP JP2002552101A patent/JP4351843B2/ja not_active Expired - Fee Related
- 2001-12-20 CN CNB018218970A patent/CN100457879C/zh not_active Expired - Fee Related
- 2001-12-20 WO PCT/DK2001/000849 patent/WO2002050221A1/en active IP Right Grant
- 2001-12-20 AU AU5655402A patent/AU5655402A/xx active Pending
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GB2023635A (en) * | 1978-05-31 | 1980-01-03 | Lesieur Cotelle | Process for the production of a liquid edible oil from fatty materials having a high content of saturated fatty acids and the oil produced by the process |
CN1061238A (zh) * | 1990-11-09 | 1992-05-20 | 商业部无锡粮食科学研究设计所 | 从氢化食用油分提代可可脂的方法 |
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CN103814056A (zh) * | 2011-11-03 | 2014-05-21 | 纳美仕有限公司 | 树脂组合物 |
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NZ526811A (en) | 2004-11-26 |
AU2002256554B2 (en) | 2005-01-20 |
CN1511189A (zh) | 2004-07-07 |
CA2431495A1 (en) | 2002-06-27 |
JP4351843B2 (ja) | 2009-10-28 |
WO2002050221A1 (en) | 2002-06-27 |
AU5655402A (en) | 2002-07-01 |
EP1343860B1 (en) | 2012-01-25 |
JP2004524389A (ja) | 2004-08-12 |
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