CL2017002736A1 - Método para la fabricación de hidróxido de litio y carbonato de litio y dispositivo para el mismo. - Google Patents
Método para la fabricación de hidróxido de litio y carbonato de litio y dispositivo para el mismo.Info
- Publication number
- CL2017002736A1 CL2017002736A1 CL2017002736A CL2017002736A CL2017002736A1 CL 2017002736 A1 CL2017002736 A1 CL 2017002736A1 CL 2017002736 A CL2017002736 A CL 2017002736A CL 2017002736 A CL2017002736 A CL 2017002736A CL 2017002736 A1 CL2017002736 A1 CL 2017002736A1
- Authority
- CL
- Chile
- Prior art keywords
- monovalent
- selective type
- lithium
- dialysis membrane
- aqueous solution
- Prior art date
Links
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 title abstract 12
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 title abstract 2
- 229910052808 lithium carbonate Inorganic materials 0.000 title abstract 2
- 238000000502 dialysis Methods 0.000 abstract 6
- 239000012528 membrane Substances 0.000 abstract 6
- 150000001450 anions Chemical class 0.000 abstract 4
- 239000007864 aqueous solution Substances 0.000 abstract 4
- 150000001768 cations Chemical class 0.000 abstract 4
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 abstract 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- 238000000909 electrodialysis Methods 0.000 abstract 2
- 150000002500 ions Chemical class 0.000 abstract 2
- 229910001386 lithium phosphate Inorganic materials 0.000 abstract 2
- 239000012466 permeate Substances 0.000 abstract 2
- TWQULNDIKKJZPH-UHFFFAOYSA-K trilithium;phosphate Chemical compound [Li+].[Li+].[Li+].[O-]P([O-])([O-])=O TWQULNDIKKJZPH-UHFFFAOYSA-K 0.000 abstract 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/08—Carbonates; Bicarbonates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/42—Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
- B01D61/44—Ion-selective electrodialysis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/42—Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
- B01D61/44—Ion-selective electrodialysis
- B01D61/445—Ion-selective electrodialysis with bipolar membranes; Water splitting
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/42—Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
- B01D61/44—Ion-selective electrodialysis
- B01D61/46—Apparatus therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/42—Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
- B01D61/44—Ion-selective electrodialysis
- B01D61/46—Apparatus therefor
- B01D61/463—Apparatus therefor comprising the membrane sequence AC or CA, where C is a cation exchange membrane
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/42—Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
- B01D61/44—Ion-selective electrodialysis
- B01D61/46—Apparatus therefor
- B01D61/465—Apparatus therefor comprising the membrane sequence AB or BA, where B is a bipolar membrane
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/42—Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
- B01D61/44—Ion-selective electrodialysis
- B01D61/46—Apparatus therefor
- B01D61/48—Apparatus therefor having one or more compartments filled with ion-exchange material, e.g. electrodeionisation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/42—Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
- B01D61/44—Ion-selective electrodialysis
- B01D61/46—Apparatus therefor
- B01D61/50—Stacks of the plate-and-frame type
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/02—Oxides; Hydroxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/04—Halides
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/14—Alkali metal compounds
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/18—Alkaline earth metal compounds or magnesium compounds
- C25B1/20—Hydroxides
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2311/00—Details relating to membrane separation process operations and control
- B01D2311/25—Recirculation, recycling or bypass, e.g. recirculation of concentrate into the feed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2311/00—Details relating to membrane separation process operations and control
- B01D2311/26—Further operations combined with membrane separation processes
- B01D2311/263—Chemical reaction
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W10/00—Technologies for wastewater treatment
- Y02W10/30—Wastewater or sewage treatment systems using renewable energies
- Y02W10/37—Wastewater or sewage treatment systems using renewable energies using solar energy
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Urology & Nephrology (AREA)
- Electrochemistry (AREA)
- Metallurgy (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Biomedical Technology (AREA)
- Environmental & Geological Engineering (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Removal Of Specific Substances (AREA)
- Water Treatment By Electricity Or Magnetism (AREA)
Abstract
<p>La presente invención se refiere a un método para fabricar hidróxido de litio y carbonato de litio, y a un dispositivo para el mismo. La presente invención proporciona un método para fabricar hidróxido de litio, que comprende: una etapa de disolver fosfato de litio en un ácido; una etapa de preparar un dispositivo de electrodiálisis de tipo selectivo para iones monovalentes dispuesto en el orden de una celda catódica que contiene un separador catódico, una membrana de diálisis de tipo selectivo para aniones monovalentes para dejar permear de manera selectiva un anión monovalente, una membrana de diálisis de tipo selectivo para cationes monovalentes para dejar permear de manera selectiva un catión monovalente, y una celda anódica que contiene un separador anódico, inyectar el fosfato de litio disuelto en el ácido entre el separador anódico de la celda anódica y la membrana de diálisis de tipo selectivo para cationes monovalentes, y entre el separador catódico de la celda catódica y la membrana de diálisis de tipo selectivo para aniones monovalentes, respectivamente, e inyectar agua entre la membrana de diálisis de tipo selectivo para cationes monovalentes y la membrana de diálisis de tipo selectivo para aniones monovalentes; una etapa de obtener una disolución acuosa de cloruro de litio, y al mismo tiempo, obtener una disolución acuosa de ácido fosfórico formada como subproducto, mediante la aplicación de una corriente eléctrica al dispositivo de electrodiálisis de tipo selectivo para iones monovalentes; y una etapa de convertir la disolución acuosa de cloruro de litio obtenida en una disolución acuosa de hidróxido de litio.</p>
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR20150061914 | 2015-04-30 | ||
| KR1020150080872A KR101700684B1 (ko) | 2015-04-30 | 2015-06-08 | 수산화리튬, 및 탄산리튬의 제조 방법 및 그 장치 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CL2017002736A1 true CL2017002736A1 (es) | 2018-06-01 |
Family
ID=57529505
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CL2017002736A CL2017002736A1 (es) | 2015-04-30 | 2017-10-30 | Método para la fabricación de hidróxido de litio y carbonato de litio y dispositivo para el mismo. |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US10759671B2 (es) |
| EP (1) | EP3290393B1 (es) |
| JP (1) | JP6602893B2 (es) |
| KR (1) | KR101700684B1 (es) |
| CN (1) | CN107787302B (es) |
| AU (1) | AU2016254855B2 (es) |
| CA (1) | CA2984567C (es) |
| CL (1) | CL2017002736A1 (es) |
| PL (1) | PL3290393T3 (es) |
| RU (1) | RU2684384C1 (es) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10661227B2 (en) | 2015-05-13 | 2020-05-26 | Research Institute Of Industrial Science & Technology | Method for producing lithium hydroxide and lithium carbonate |
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| KR101888181B1 (ko) * | 2016-12-23 | 2018-08-13 | 주식회사 포스코 | 수산화리튬 및 탄산리튬의 제조방법 |
| US11365128B2 (en) | 2017-06-15 | 2022-06-21 | Energysource Minerals Llc | Process for selective adsorption and recovery of lithium from natural and synthetic brines |
| CZ308122B6 (cs) * | 2018-05-29 | 2020-01-15 | Membrain S.R.O. | Způsob výroby chemických sloučenin lithia metodou elektrodialýzy a zařízení k provádění tohoto způsobu |
| WO2020033988A1 (en) * | 2018-08-17 | 2020-02-20 | Lithtech Industries Pty Ltd | An improved electrochemical cell arrangement and method for separating impurities |
| CN112673119A (zh) * | 2018-08-17 | 2021-04-16 | 利特科技工业有限公司 | 一种改进的锂加工方法 |
| KR102145110B1 (ko) * | 2018-11-07 | 2020-08-14 | 전웅 | 리튬 추출 방법 |
| CN109534369B (zh) * | 2018-12-07 | 2023-07-28 | 杭州水处理技术研究开发中心有限公司 | 一种膜集成制备氯化锂设备及其方法 |
| FI3898517T3 (fi) * | 2018-12-20 | 2023-09-05 | Lanxess Deutschland Gmbh | Erittäin puhtaan litiumkarbonaatin valmistus suolaliuoksista |
| EP3911772A4 (en) * | 2019-01-18 | 2022-10-05 | St-Georges Eco-Mining Corp. | MINERAL RECOVERY PROCESSES |
| CN110616438B (zh) * | 2019-08-19 | 2021-09-28 | 南京宁智高新材料研究院有限公司 | 一种电化学制备高纯电池级氢氧化锂的装置及其方法 |
| KR102401348B1 (ko) * | 2019-12-20 | 2022-05-23 | 재단법인 포항산업과학연구원 | 리튬 함유 용액으로부터 리튬 추출 방법 |
| EP4098758A4 (en) * | 2020-01-29 | 2023-01-04 | Uong Chon | LITHIUM EXTRACTION PROCESS |
| JP7156322B2 (ja) * | 2020-02-17 | 2022-10-19 | 住友金属鉱山株式会社 | 水酸化リチウムの製造方法 |
| CN112299451A (zh) * | 2020-03-25 | 2021-02-02 | 意定(上海)信息科技有限公司 | 一种通过磷酸锂的形式从含锂低镁卤水中制备氢氧化锂的方法 |
| CN111825108A (zh) * | 2020-06-16 | 2020-10-27 | 四川兴晟锂业有限责任公司 | 一种去除中间物料硫酸锂溶液中钙离子的氢氧化锂母液及其方法 |
| CN117125683A (zh) * | 2020-11-21 | 2023-11-28 | 周思齐 | 一种盐湖卤水生产电池级磷酸锂的方法 |
| KR102242686B1 (ko) * | 2020-12-14 | 2021-04-21 | 한국지질자원연구원 | 리튬농축액 제조방법 및 이로부터 제조된 리튬농축액을 이용한 리튬화합물 제조방법 |
| RU2769609C2 (ru) * | 2021-03-31 | 2022-04-04 | Общество с ограниченной ответственностью "Экостар-Наутех" | Способ получения моногидрата гидроксида лития высокой степени чистоты из материалов, содержащих соли лития |
| CN113666396B (zh) * | 2021-08-25 | 2022-12-30 | 中国科学技术大学 | 一种由盐湖卤水制取氯化锂的离子精馏方法 |
| US20230098644A1 (en) * | 2021-09-24 | 2023-03-30 | American Battery Technology Company | Systems and methods for lithium extraction from sedimentary deposits |
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2015
- 2015-06-08 KR KR1020150080872A patent/KR101700684B1/ko active IP Right Grant
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2016
- 2016-04-29 AU AU2016254855A patent/AU2016254855B2/en active Active
- 2016-04-29 US US15/570,400 patent/US10759671B2/en active Active
- 2016-04-29 JP JP2017556892A patent/JP6602893B2/ja active Active
- 2016-04-29 CN CN201680025927.8A patent/CN107787302B/zh active Active
- 2016-04-29 RU RU2017141578A patent/RU2684384C1/ru active
- 2016-04-29 CA CA2984567A patent/CA2984567C/en active Active
- 2016-04-29 EP EP16786799.3A patent/EP3290393B1/en active Active
- 2016-04-29 PL PL16786799T patent/PL3290393T3/pl unknown
-
2017
- 2017-10-30 CL CL2017002736A patent/CL2017002736A1/es unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10661227B2 (en) | 2015-05-13 | 2020-05-26 | Research Institute Of Industrial Science & Technology | Method for producing lithium hydroxide and lithium carbonate |
Also Published As
| Publication number | Publication date |
|---|---|
| CA2984567A1 (en) | 2016-11-03 |
| CN107787302A (zh) | 2018-03-09 |
| KR101700684B1 (ko) | 2017-01-31 |
| EP3290393A1 (en) | 2018-03-07 |
| RU2684384C1 (ru) | 2019-04-08 |
| EP3290393B1 (en) | 2022-01-19 |
| AU2016254855B2 (en) | 2019-12-12 |
| AU2016254855A1 (en) | 2017-11-23 |
| JP2018522709A (ja) | 2018-08-16 |
| CA2984567C (en) | 2020-12-01 |
| EP3290393A4 (en) | 2019-01-23 |
| CN107787302B (zh) | 2020-12-04 |
| PL3290393T3 (pl) | 2022-04-25 |
| US10759671B2 (en) | 2020-09-01 |
| JP6602893B2 (ja) | 2019-11-06 |
| US20180148342A1 (en) | 2018-05-31 |
| KR20160129657A (ko) | 2016-11-09 |
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