CH245276A - Process for the preparation of a new derivative of a ring-substituted aromatic oxy compound. - Google Patents

Process for the preparation of a new derivative of a ring-substituted aromatic oxy compound.

Info

Publication number
CH245276A
CH245276A CH245276DA CH245276A CH 245276 A CH245276 A CH 245276A CH 245276D A CH245276D A CH 245276DA CH 245276 A CH245276 A CH 245276A
Authority
CH
Switzerland
Prior art keywords
preparation
ring
substituted aromatic
oxy compound
new derivative
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellschaft Ciba
Original Assignee
Ciba Geigy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ciba Geigy filed Critical Ciba Geigy
Publication of CH245276A publication Critical patent/CH245276A/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/12—Preparation of carboxylic acid amides by reactions not involving the formation of carboxamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Herstellung eines neuen Derivates einer lernsubstituierten       aromatisehen        Ogyverbindung.       Es wurde     gefunden,    dass man zu einem  neuen Derivat einer kernsubstituierten aro  matischen     Oxyverbindung    gelangt, wenn  man das Kondensationsprodukt aus     Ölsäure-          N-methylolamid    und Phenol mit Formaldehyd  und     Diäthanolamin    kondensiert.  



  Die Kondensation wird zweckmässig in  der Wärme, z. B. bei 60-l00 , ausgeführt.  Das neue Erzeugnis bildet ein dickflüssi  ges Öl, das nach dem Lösen     in    Eisessig mit  Wasser eine klare, schäumende     Löung    er  gibt. Es kann als     Textilhilfsstoff    Anwen  dung finden.  



  <I>Beispiel:</I>  23,2 Teile des Kondensationsproduktes  aus     Olsäure-N-methylolamid    - und Phenol  werden mit 15 Teilen     Diäthanolamin    ver  mischt, worauf man 10     Volumteile    40,3     vo-          lumprozentige        wässrige        Formaldehydlösung     innert 1 Stunde bei Raumtemperatur hinzu  fliessen lässt und anschliessend 4 Stunden auf  85-90  erhitzt. Das mit Wasser gewaschene  Kondensationserzeugnis bildet nach dem  Trocknen ein dickflüssiges Öl, das nach dem  Lösen in Eisessig mit Wasser eine klare;  schäumende Lösung ergibt. Es kann als       Textilhilfsstoff    Anwendung finden.

      Das oben benützte Kondensationserzeug  nis aus     ölsäure-N-methylolamid    und Phenol  kann durch Kondensation in Eisessig, z. B.  bei 45-50 , unter Zusatz von entwässertem  Zinkchlorid hergestellt werden.



  Process for the preparation of a new derivative of a learning-substituted aromatic ogy compound. It has been found that a new derivative of a ring-substituted aromatic oxy compound is obtained if the condensation product of oleic acid-N-methylolamide and phenol is condensed with formaldehyde and diethanolamine.



  The condensation is expedient in the heat, for. B. at 60-100 executed. The new product forms a viscous oil, which after dissolving in glacial acetic acid with water gives a clear, foaming solution. It can be used as a textile auxiliary material.



  <I> Example: </I> 23.2 parts of the condensation product of oleic acid-N-methylolamide and phenol are mixed with 15 parts of diethanolamine, whereupon 10 parts by volume of 40.3% by volume aqueous formaldehyde solution are added within 1 hour at room temperature lets flow and then heated to 85-90 for 4 hours. The condensation product, washed with water, forms a thick oil after drying, which after dissolving in glacial acetic acid with water becomes a clear; foaming solution results. It can be used as a textile auxiliary.

      The condensation product used above from oleic acid-N-methylolamide and phenol can by condensation in glacial acetic acid, for. B. at 45-50, with the addition of dehydrated zinc chloride.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Derivates einer kernsubstituierten aromati schen Oxyverbindung, dadurch gekennzeich net, dass man das Kondensationsprodukt aus Ölsäure-N-methylolamid und Phenol mit Formaldehyd und Diäthanolamin konden siert. Das neue Erzeugnis bildet ein dickflüssi ges Öl, das nach dem Lösen in Eisessig mit Wasser eine klare, schäumende Löung er gibt. Es kann als Textilhilfsstoff Anwen dung finden. PATENT CLAIM: Process for the preparation of a new derivative of a ring-substituted aromatic oxy compound, characterized in that the condensation product of oleic acid-N-methylolamide and phenol is condensed with formaldehyde and diethanolamine. The new product forms a viscous oil, which after dissolving in glacial acetic acid with water gives a clear, foaming solution. It can be used as a textile auxiliary material. UNTERANSPRUCH: Verfahren nach Patentanspruch, dadurch gekennzeichnet, dass man die Kondensation in der Wärme ausführt. SUBCLAIM: Process according to claim, characterized in that the condensation is carried out in the heat.
CH245276D 1944-05-10 1944-05-10 Process for the preparation of a new derivative of a ring-substituted aromatic oxy compound. CH245276A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH245276T 1944-05-10
CH242605T 1946-05-31

Publications (1)

Publication Number Publication Date
CH245276A true CH245276A (en) 1946-10-31

Family

ID=25728699

Family Applications (1)

Application Number Title Priority Date Filing Date
CH245276D CH245276A (en) 1944-05-10 1944-05-10 Process for the preparation of a new derivative of a ring-substituted aromatic oxy compound.

Country Status (1)

Country Link
CH (1) CH245276A (en)

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