CH208132A - Process for the production of a new, nitrogen-containing organic compound. - Google Patents

Process for the production of a new, nitrogen-containing organic compound.

Info

Publication number
CH208132A
CH208132A CH208132DA CH208132A CH 208132 A CH208132 A CH 208132A CH 208132D A CH208132D A CH 208132DA CH 208132 A CH208132 A CH 208132A
Authority
CH
Switzerland
Prior art keywords
new
production
nitrogen
organic compound
containing organic
Prior art date
Application number
Other languages
German (de)
Inventor
Limited Imperial Ch Industries
Original Assignee
Ici Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ici Ltd filed Critical Ici Ltd
Publication of CH208132A publication Critical patent/CH208132A/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C275/00—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C275/46—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups containing any of the groups, X being a hetero atom, Y being any atom, e.g. acylureas
    • C07C275/48—Y being a hydrogen or a carbon atom
    • C07C275/50—Y being a hydrogen or an acyclic carbon atom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pyridine Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Coloring (AREA)

Description

  

      Verfahren        zur        Herstellung        einer        neuen,     organischen Verbindung.    Die Erfindung bezieht sich auf ein Ver  fahren zur Herstellung einer neuen, stickstoff  haltigen organischen Verbindung, geeignet,  um     zelluloseartigen    Textilmaterialien Affinität  für     Säurewollfarbstoffe    zu erteilen.  



  Gemäss der Erfindung wird     Allophano-          methyldimethyl    -     cyclohexylammoniumchlorid     der Formel  
EMI0001.0011     
    erhalten, indem     Chloroaoetylharnstoff    ver  anlasst wird, sich mit     Dimethylcyelohexämin     zu verbinden.  



  Wenn gewünscht, kann die Reaktion in  Gegenwart eines Lösungs- oder Verdünnungs  mittels, z. B. Alkohol, durchgeführt werden.  <I>Beispiel:</I>  20 Teile     Ohloroacetylharnstoff,    20 Teile         Dymethyleyclohexylamin    und 100 Teile  Äthanol werden zusammen unter     Rückfluss-          kühlung    während fünf Stunden erhitzt. Es  bildet sich eine klare Lösung. Der Alkohol  wird hierauf bei Unterdruck     abdestilliert.    Es  verbleibt eine viskose, gelbe, an der Atmo  sphäre zerfliessende,- ölige Masse, welche beim  Stehen langsam Kristalle niederschlägt.

   Es  ist dies die neue Verbindung,     Allophano-          methyldimethyl-        cyclohexylammoniumchlorid.     Sie ist sehr leicht in Wasser löslich, lösbar  in heissem Alkohol und in Äther, Azeton  und Benzol unlöslich.



      Process for the production of a new, organic compound. The invention relates to a process for the production of a new, nitrogen-containing organic compound, suitable for giving cellulosic textile materials an affinity for acid wool dyes.



  According to the invention, allophanomethyldimethyl-cyclohexylammonium chloride is of the formula
EMI0001.0011
    obtained by causing chloroaoetylurea ver to combine with dimethylcyelohexaemine.



  If desired, the reaction can be carried out in the presence of a solvent or diluent, e.g. B. alcohol. <I> Example: </I> 20 parts of ohloroacetylurea, 20 parts of dymethyleyclohexylamine and 100 parts of ethanol are heated together under reflux for five hours. A clear solution forms. The alcohol is then distilled off under reduced pressure. What remains is a viscous, yellow, oily mass that dissolves in the atmosphere and slowly precipitates crystals when standing.

   This is the new compound, allophanomethyldimethylcyclohexylammonium chloride. It is very easily soluble in water, soluble in hot alcohol and insoluble in ether, acetone and benzene.

Claims (1)

PATENTANSPRUCPL: Verfahren zur Herstellung einer neuen, stickstoffhaltigen organischen Verbindung, geeignet, um zelluloseartigem Textilmaterial Affinität für Säurewollfarbstoffe zu erteilen, nämlich Allophanomethyldimethyl-cyclohexyl- ammoniumchlorid der Formel EMI0002.0001 dadurch gekennzeichnet, dass Chloroacetyl- harustoff veranlasst wird, sich mit Dirrtethyl- cyclohexylamin zu verbinden. PATENT CLAIM: A process for the production of a new, nitrogen-containing organic compound, suitable for giving cellulosic textile material an affinity for acid wool dyes, namely allophanomethyldimethyl-cyclohexylammonium chloride of the formula EMI0002.0001 characterized in that chloroacetyl-hydrogen is caused to combine with dirrtethyl-cyclohexylamine. Die neue Ver bindung ist eine viskose, gelbe, an der Atmo- sphäre zerfliessende, teilweise kristalline, halbfeste Masse, welche sich sehr leicht in Wasser löst, lösbar in heissem Alkohol und in Äther, Azeton und Benzol unlöslich ist. The new compound is a viscous, yellow, partially crystalline, semi-solid mass that dissolves in the atmosphere, which dissolves very easily in water, is soluble in hot alcohol and insoluble in ether, acetone and benzene.
CH208132D 1937-06-18 1938-06-17 Process for the production of a new, nitrogen-containing organic compound. CH208132A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB207203X 1937-06-18
GB208132X 1937-06-18

Publications (1)

Publication Number Publication Date
CH208132A true CH208132A (en) 1939-12-31

Family

ID=33031450

Family Applications (2)

Application Number Title Priority Date Filing Date
CH207203D CH207203A (en) 1937-06-18 1938-06-17 Process for the production of a new, nitrogen-containing organic compound.
CH208132D CH208132A (en) 1937-06-18 1938-06-17 Process for the production of a new, nitrogen-containing organic compound.

Family Applications Before (1)

Application Number Title Priority Date Filing Date
CH207203D CH207203A (en) 1937-06-18 1938-06-17 Process for the production of a new, nitrogen-containing organic compound.

Country Status (1)

Country Link
CH (2) CH207203A (en)

Also Published As

Publication number Publication date
CH207203A (en) 1939-10-15

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