CH196615A - Process for the production of a condensation product. - Google Patents

Process for the production of a condensation product.

Info

Publication number
CH196615A
CH196615A CH196615DA CH196615A CH 196615 A CH196615 A CH 196615A CH 196615D A CH196615D A CH 196615DA CH 196615 A CH196615 A CH 196615A
Authority
CH
Switzerland
Prior art keywords
production
condensation product
pyridine
water
stearoylmethylamide
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH196615A publication Critical patent/CH196615A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00Carboxylic acid amides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Herstellung eines Kondensationsproduktes.    Es wurde gefunden, dass man ein neues  Kondensationsprodukt erhält, wenn man auf       Stearoylmethylamid    ein     Mol    des     3-Sulfochlo-          rids    der     Benzoesäure    in Gegenwart von     Py-          ridin    einwirken lässt. Das neue Produkt bildet  ein weisses Pulver, das sich in Wasser unter  Bildung stark schäumender Lösungen löst und  als     Hilfsstoff    in der Textilindustrie verwen  det werden kann.  



  <I>Beispiel:</I>  3 Teile     Stearoylmethylamid    werden mit  4.4 Teilen     Benzoesäure-3-sulfochlorid    in 30  Teilen     Pyridin    während 1 Stunde auf 80-90    erhitzt, wonach sich eine Probe in Wasser  klar auflöst. Nach weitgehender     Entfernung     des     Pyridins    im Vakuum wird der helle, fiüs-         sige    Rückstand mit 400 Teilen Wasser auf  genommen, mit verdünnter     Sodalösung    neu  tralisiert und das Reaktionsprodukt mit Na  triumchlorid     ausgesalzen.    Dasselbe wird ab  gesaugt und getrocknet.



  Process for the production of a condensation product. It has been found that a new condensation product is obtained if one mole of the 3-sulfochloride of benzoic acid is allowed to act on stearoylmethylamide in the presence of pyridine. The new product forms a white powder that dissolves in water to form strongly foaming solutions and can be used as an auxiliary in the textile industry.



  <I> Example: </I> 3 parts of stearoylmethylamide are heated with 4.4 parts of benzoic acid 3-sulfochloride in 30 parts of pyridine to 80-90 for 1 hour, after which a sample dissolves clearly in water. After extensive removal of the pyridine in vacuo, the pale, liquid residue is taken up in 400 parts of water, neutralized with dilute soda solution and the reaction product is salted out with sodium chloride. The same is sucked off and dried.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines Konden sationsproduktes, dadurch gekennzeichnet, dass man auf Stearoylmethylamid ein Mol des 3-Sulfochlorids der Benzoesäure in Gegenwart von Pyridin einwirken lässt. Das neue Pro dukt bildet ein weisses Pulver, das sich in Wasser unter Bildung stark schäumender Lösungen löst und als Hilfsstoff in der Textil industrie verwendet werden kann. PATENT CLAIM: Process for the production of a condensation product, characterized in that one mole of the 3-sulfochloride of benzoic acid is allowed to act on stearoylmethylamide in the presence of pyridine. The new product forms a white powder that dissolves in water to form strongly foaming solutions and can be used as an auxiliary in the textile industry.
CH196615D 1936-11-11 1936-11-11 Process for the production of a condensation product. CH196615A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH196615T 1936-11-11

Publications (1)

Publication Number Publication Date
CH196615A true CH196615A (en) 1938-03-31

Family

ID=4440463

Family Applications (1)

Application Number Title Priority Date Filing Date
CH196615D CH196615A (en) 1936-11-11 1936-11-11 Process for the production of a condensation product.

Country Status (1)

Country Link
CH (1) CH196615A (en)

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