CA3132151A1 - System and method for regenerating and restoring kinetic properties of resin - Google Patents

System and method for regenerating and restoring kinetic properties of resin Download PDF

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Publication number
CA3132151A1
CA3132151A1 CA3132151A CA3132151A CA3132151A1 CA 3132151 A1 CA3132151 A1 CA 3132151A1 CA 3132151 A CA3132151 A CA 3132151A CA 3132151 A CA3132151 A CA 3132151A CA 3132151 A1 CA3132151 A1 CA 3132151A1
Authority
CA
Canada
Prior art keywords
resin
vessel
cleaning
resins
chemical
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CA3132151A
Other languages
English (en)
French (fr)
Inventor
Thomas O. Miller
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ionx Solutions LLC
Original Assignee
Ionx Solutions LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ionx Solutions LLC filed Critical Ionx Solutions LLC
Publication of CA3132151A1 publication Critical patent/CA3132151A1/en
Pending legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/70—Regeneration or reactivation of ion-exchangers; Apparatus therefor for large scale industrial processes or applications
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J47/00—Ion-exchange processes in general; Apparatus therefor
    • B01J47/02—Column or bed processes
    • B01J47/022—Column or bed processes characterised by the construction of the column or container
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/05—Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds
    • B01J49/06—Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds containing cationic exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/05—Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds
    • B01J49/07—Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds containing anionic exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/05—Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds
    • B01J49/09—Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds of mixed beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/50—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
    • B01J49/53—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents for cationic exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/50—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
    • B01J49/57—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents for anionic exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/60—Cleaning or rinsing ion-exchange beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/80—Automatic regeneration
    • B01J49/85—Controlling or regulating devices therefor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatment Of Water By Ion Exchange (AREA)
CA3132151A 2018-08-29 2020-01-13 System and method for regenerating and restoring kinetic properties of resin Pending CA3132151A1 (en)

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
US201862724587P 2018-08-29 2018-08-29
US16/292,131 2019-03-04
US16/292,131 US10532351B1 (en) 2018-08-29 2019-03-04 Method for restoring kinetic properties of resin
US16/676,128 US10737260B2 (en) 2018-08-29 2019-11-06 System and method for restoring kinetic properties of resin
US16/676,128 2019-11-06
PCT/US2020/013382 WO2020180397A1 (en) 2018-08-29 2020-01-13 System and method for regenerating and restoring kinetic properties of resin

Publications (1)

Publication Number Publication Date
CA3132151A1 true CA3132151A1 (en) 2020-09-10

Family

ID=69141194

Family Applications (1)

Application Number Title Priority Date Filing Date
CA3132151A Pending CA3132151A1 (en) 2018-08-29 2020-01-13 System and method for regenerating and restoring kinetic properties of resin

Country Status (9)

Country Link
US (5) US10532351B1 (https=)
EP (1) EP3934806A4 (https=)
JP (1) JP2022523820A (https=)
KR (1) KR102917719B1 (https=)
CN (1) CN113543881A (https=)
AU (1) AU2020233564A1 (https=)
CA (1) CA3132151A1 (https=)
IL (1) IL285777A (https=)
WO (1) WO2020180397A1 (https=)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10532351B1 (en) * 2018-08-29 2020-01-14 Thomas O. Miller Method for restoring kinetic properties of resin
US12311349B2 (en) * 2019-03-04 2025-05-27 lonx Solutions, LLC System and method for regenerating and restoring kinetic properties of resin
US12521710B2 (en) 2021-01-12 2026-01-13 Ionx Solutions, Llc System and method for regenerating and restoring kinetic properties of resin
US20240165603A1 (en) * 2021-03-29 2024-05-23 Ionx Solutions, Llc System and method for on-site cleaning and restoration of kinetic properties of ion exchange resin
CN115101229B (zh) * 2022-06-14 2025-01-24 华能海南昌江核电有限公司 一种放射性废树脂再生式去污处理方法
TW202432511A (zh) 2022-12-23 2024-08-16 日商住友化學股份有限公司 化合物、包含源自該化合物的結構單元的樹脂、抗蝕劑組成物以及抗蝕劑圖案的製造方法

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US3139401A (en) 1962-01-05 1964-06-30 Hach Chemical Co Method for removing rust from water softeners
GB1054578A (en) 1964-11-12 1967-01-11 United Kingdom Atomic Energy Authority Improvements in or relating to Ion Exchange Methods and Apparatus
US3749249A (en) * 1971-03-05 1973-07-31 Ecodyne Corp Method and apparatus
JPS4937888A (https=) * 1972-08-11 1974-04-08
US4220531A (en) * 1978-04-14 1980-09-02 Gordon B. Nute Apparatus for deionizing liquids with ion exchange resins
US4151079A (en) * 1978-06-05 1979-04-24 Nalco Chemical Company Regeneration of ion exchange resins
JPS5524570A (en) * 1978-08-11 1980-02-21 Ebara Infilco Co Ltd Removing method for phosphates in solution
JPS5926143A (ja) * 1982-08-05 1984-02-10 Ebara Infilco Co Ltd イオン交換樹脂の除鉄回生方法
US4500430A (en) 1982-09-22 1985-02-19 Dasgupta Purnendu K Continuously rejuvenated ion exchanger
JPS59139944A (ja) * 1983-01-31 1984-08-11 Hitachi Ltd 懸濁固形物付着イオン交換樹脂の洗浄方法
US4511675A (en) 1983-04-19 1985-04-16 Auerswald David C Method for regenerating water polishers using ammonium sulphate
US4880513A (en) * 1986-06-20 1989-11-14 The Graver Company Method and apparatus for generating acid and base regenerants and the use thereof to regenerate ion-exchange resins
US4913803A (en) * 1988-04-07 1990-04-03 Radiological & Chemical Technology, Inc. Particle separation system
US5082567A (en) * 1990-11-08 1992-01-21 Occidental Chemical Corporation Regeneration of cationic exchange resins
JP3348109B2 (ja) * 1992-01-02 2002-11-20 コノコ・インコーポレーテッド 水酸化ナトリウムで陽イオン交換樹脂からアルカノールアミンを選択的に再生するためのモニターおよび制御システム
JPH06134322A (ja) * 1992-10-23 1994-05-17 I C I Japan Kk イオン交換樹脂
US5858119A (en) * 1995-05-17 1999-01-12 Mayne; Michael D. Ion exchange resin cleaning method
JP2002159867A (ja) 2000-11-27 2002-06-04 Kurita Water Ind Ltd アニオン交換樹脂の再生方法
JP2002361244A (ja) * 2001-06-08 2002-12-17 Hitachi Electric Systems Ltd 水道水軟水化装置
WO2003086629A1 (en) 2002-04-12 2003-10-23 Ionics, Incorporated Ion exchange regeneration and upw treatment system
US7482387B2 (en) * 2004-02-17 2009-01-27 Institute Of Nuclear Energy Method for processing spent ion-exchange resins
JP2006184045A (ja) * 2004-12-27 2006-07-13 Ebara Kogyo Senjo Kk 化学除染用イオン交換樹脂塔
US8585906B2 (en) * 2006-07-14 2013-11-19 Rayne Dealership Corporation Regeneration of ion exchange resin and recovery of regenerant solution
JP5298639B2 (ja) * 2008-05-26 2013-09-25 栗田工業株式会社 水溶性樹脂成分含有アルカリ廃液の処理方法および処理装置
US8063112B2 (en) 2008-12-08 2011-11-22 Cansolv Technologies Inc. Process for the regeneration of an ion exchange resin using sulfurous acid
US8870445B2 (en) 2008-12-12 2014-10-28 II Gordon C. Burns Liquid accelerator and chemical mixing apparatus and method
ES2566536T3 (es) * 2010-07-01 2016-04-13 Emd Millipore Corporation Dispositivo y procedimiento de electrodesionización que comprende el control de la corriente eléctrica mediante la medición de la expansión del material de intercambio iónico
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JP6015737B2 (ja) * 2014-11-13 2016-10-26 栗田工業株式会社 再生型イオン交換装置の運転方法
EP3218312A4 (en) * 2014-11-14 2018-05-30 FilterBoxx Water and Environmental Corp. Ion-exchange purification method and apparatus
CA2971420C (en) 2014-12-19 2021-01-05 The Procter & Gamble Company A spatially controllable eductor for managing solid additives and processes using same
JP6315611B2 (ja) * 2015-11-30 2018-04-25 壽化工機株式会社 混床式樹脂充填塔の混合樹脂の分離方法、混床式樹脂充填塔、及び水処理装置
CN107442185A (zh) * 2017-09-28 2017-12-08 荣成市固废综合处理与应用产业园有限公司 一种阳离子树脂铁中毒在线复苏装置及复苏方法
CN207271271U (zh) * 2017-09-28 2018-04-27 荣成市固废综合处理与应用产业园有限公司 一种阳离子树脂铁中毒在线复苏装置
US10532351B1 (en) 2018-08-29 2020-01-14 Thomas O. Miller Method for restoring kinetic properties of resin

Also Published As

Publication number Publication date
EP3934806A4 (en) 2022-12-07
US11433387B2 (en) 2022-09-06
US11911755B2 (en) 2024-02-27
EP3934806A1 (en) 2022-01-12
WO2020180397A1 (en) 2020-09-10
US20200070143A1 (en) 2020-03-05
US10532351B1 (en) 2020-01-14
AU2020233564A1 (en) 2021-09-16
JP2022523820A (ja) 2022-04-26
CN113543881A (zh) 2021-10-22
US12239971B2 (en) 2025-03-04
IL285777A (en) 2021-10-31
KR20210130807A (ko) 2021-11-01
US10737260B2 (en) 2020-08-11
KR102917719B1 (ko) 2026-01-23
US20200368736A1 (en) 2020-11-26
US20240189808A1 (en) 2024-06-13
US20230173477A1 (en) 2023-06-08

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