CA2913112C - Nanocrystalline zirconia and methods of processing thereof - Google Patents
Nanocrystalline zirconia and methods of processing thereof Download PDFInfo
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- CA2913112C CA2913112C CA2913112A CA2913112A CA2913112C CA 2913112 C CA2913112 C CA 2913112C CA 2913112 A CA2913112 A CA 2913112A CA 2913112 A CA2913112 A CA 2913112A CA 2913112 C CA2913112 C CA 2913112C
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- zirconia
- dental
- ceramic
- opalescent
- manufacturing
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- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 title claims abstract description 387
- 238000000034 method Methods 0.000 title description 22
- 238000012545 processing Methods 0.000 title description 17
- 230000010494 opalescence Effects 0.000 claims abstract description 50
- 238000002834 transmittance Methods 0.000 claims abstract description 44
- 239000011351 dental ceramic Substances 0.000 claims abstract description 41
- 230000001747 exhibiting effect Effects 0.000 claims abstract description 4
- 239000000725 suspension Substances 0.000 claims description 62
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 claims description 39
- 239000011148 porous material Substances 0.000 claims description 31
- 238000005245 sintering Methods 0.000 claims description 31
- 239000000463 material Substances 0.000 claims description 30
- 238000004519 manufacturing process Methods 0.000 claims description 29
- 238000010438 heat treatment Methods 0.000 claims description 24
- 239000000919 ceramic Substances 0.000 claims description 21
- 238000003801 milling Methods 0.000 claims description 18
- 238000005266 casting Methods 0.000 claims description 17
- 239000002105 nanoparticle Substances 0.000 claims description 16
- 239000002245 particle Substances 0.000 claims description 16
- 238000001035 drying Methods 0.000 claims description 14
- 230000005540 biological transmission Effects 0.000 claims description 13
- RUDFQVOCFDJEEF-UHFFFAOYSA-N yttrium(III) oxide Inorganic materials [O-2].[O-2].[O-2].[Y+3].[Y+3] RUDFQVOCFDJEEF-UHFFFAOYSA-N 0.000 claims description 13
- 239000002270 dispersing agent Substances 0.000 claims description 12
- 239000007787 solid Substances 0.000 claims description 12
- 238000001652 electrophoretic deposition Methods 0.000 claims description 11
- 238000003825 pressing Methods 0.000 claims description 11
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 9
- 238000001746 injection moulding Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 238000007493 shaping process Methods 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- 238000007569 slipcasting Methods 0.000 claims description 6
- 239000000654 additive Substances 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000009750 centrifugal casting Methods 0.000 claims description 4
- 239000007943 implant Substances 0.000 claims description 4
- 238000003754 machining Methods 0.000 claims description 4
- 238000001272 pressureless sintering Methods 0.000 claims description 4
- 230000000087 stabilizing effect Effects 0.000 claims description 4
- 230000000996 additive effect Effects 0.000 claims description 3
- 229910002082 tetragonal zirconia polycrystal Inorganic materials 0.000 claims description 3
- CLLLODNOQBVIMS-UHFFFAOYSA-N 2-(2-methoxyethoxy)acetic acid Chemical compound COCCOCC(O)=O CLLLODNOQBVIMS-UHFFFAOYSA-N 0.000 claims description 2
- 229920002873 Polyethylenimine Polymers 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- -1 poly(ethyleneimine) Polymers 0.000 claims description 2
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 claims 4
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims 3
- YHBWXWLDOKIVCJ-UHFFFAOYSA-N 2-[2-(2-methoxyethoxy)ethoxy]acetic acid Chemical compound COCCOCCOCC(O)=O YHBWXWLDOKIVCJ-UHFFFAOYSA-N 0.000 claims 1
- 230000003287 optical effect Effects 0.000 description 15
- 210000003298 dental enamel Anatomy 0.000 description 12
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- 241000894007 species Species 0.000 description 7
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- 229910010293 ceramic material Inorganic materials 0.000 description 5
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- 229910001233 yttria-stabilized zirconia Inorganic materials 0.000 description 5
- 238000007792 addition Methods 0.000 description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 4
- 239000011230 binding agent Substances 0.000 description 4
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- 230000008569 process Effects 0.000 description 4
- 238000001878 scanning electron micrograph Methods 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- OCKGFTQIICXDQW-ZEQRLZLVSA-N 5-[(1r)-1-hydroxy-2-[4-[(2r)-2-hydroxy-2-(4-methyl-1-oxo-3h-2-benzofuran-5-yl)ethyl]piperazin-1-yl]ethyl]-4-methyl-3h-2-benzofuran-1-one Chemical compound C1=C2C(=O)OCC2=C(C)C([C@@H](O)CN2CCN(CC2)C[C@H](O)C2=CC=C3C(=O)OCC3=C2C)=C1 OCKGFTQIICXDQW-ZEQRLZLVSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 238000000149 argon plasma sintering Methods 0.000 description 3
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- 239000011521 glass Substances 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- MRELNEQAGSRDBK-UHFFFAOYSA-N lanthanum(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[La+3].[La+3] MRELNEQAGSRDBK-UHFFFAOYSA-N 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 239000006070 nanosuspension Substances 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- 230000008520 organization Effects 0.000 description 2
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- XYJRXVWERLGGKC-UHFFFAOYSA-D pentacalcium;hydroxide;triphosphate Chemical compound [OH-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O XYJRXVWERLGGKC-UHFFFAOYSA-D 0.000 description 2
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- 238000002490 spark plasma sintering Methods 0.000 description 2
- 230000006641 stabilisation Effects 0.000 description 2
- 238000011105 stabilization Methods 0.000 description 2
- 238000001429 visible spectrum Methods 0.000 description 2
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- 238000007088 Archimedes method Methods 0.000 description 1
- 101100350285 Escherichia coli (strain K12) ompF gene Proteins 0.000 description 1
- 241000282412 Homo Species 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
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- 230000003247 decreasing effect Effects 0.000 description 1
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- 239000002670 dental porcelain Substances 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- WVMPCBWWBLZKPD-UHFFFAOYSA-N dilithium oxido-[oxido(oxo)silyl]oxy-oxosilane Chemical compound [Li+].[Li+].[O-][Si](=O)O[Si]([O-])=O WVMPCBWWBLZKPD-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000004438 eyesight Effects 0.000 description 1
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- 230000004048 modification Effects 0.000 description 1
- 239000002159 nanocrystal Substances 0.000 description 1
- 229910002077 partially stabilized zirconia Inorganic materials 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000011164 primary particle Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
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- 210000001525 retina Anatomy 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000002798 spectrophotometry method Methods 0.000 description 1
- 229910002076 stabilized zirconia Inorganic materials 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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Classifications
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- A61C13/083—Porcelain or ceramic teeth
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- A61C8/00—Means to be fixed to the jaw-bone for consolidating natural teeth or for fixing dental prostheses thereon; Dental implants; Implanting tools
- A61C8/0012—Means to be fixed to the jaw-bone for consolidating natural teeth or for fixing dental prostheses thereon; Dental implants; Implanting tools characterised by the material or composition, e.g. ceramics, surface layer, metal alloy
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- A61K6/802—Preparations for artificial teeth, for filling teeth or for capping teeth comprising ceramics
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- A61K6/802—Preparations for artificial teeth, for filling teeth or for capping teeth comprising ceramics
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| EP3357866A4 (en) * | 2015-09-30 | 2019-06-19 | Nippon Shokubai Co., Ltd. | ZIRCONIUM-NANOPARTICLES |
| FR3048354B1 (fr) * | 2016-03-04 | 2021-12-10 | Michael Sadoun | Preforme destinee a la fabrication d'une prothese dentaire |
| DE102016110622A1 (de) * | 2016-06-09 | 2017-12-14 | Michael Gahlert | Knochenersatzmaterial aus Zirkondioxidkeramik |
| US9822039B1 (en) | 2016-08-18 | 2017-11-21 | Ivoclar Vivadent Ag | Metal oxide ceramic nanomaterials and methods of making and using same |
| US10532008B2 (en) | 2017-02-22 | 2020-01-14 | James R. Glidewell Dental Ceramics, Inc. | High strength and translucency dental zirconia ceramic materials, devices and methods |
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| CN107021752A (zh) * | 2017-05-12 | 2017-08-08 | 青岛大学 | 一种陶瓷钢领制备方法 |
| CN107151139A (zh) * | 2017-05-12 | 2017-09-12 | 青岛大学 | 一种陶瓷粘胶纤维切断刀制备方法 |
| CN107010945A (zh) * | 2017-05-12 | 2017-08-04 | 青岛大学 | 一种氧化锆全瓷牙种植体制备方法 |
| CN107162586A (zh) * | 2017-05-12 | 2017-09-15 | 青岛大学 | 一种氧化锆种植牙基台制备方法 |
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| RU2712642C1 (ru) * | 2019-03-15 | 2020-01-30 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Томский государственный университет систем управления и радиоэлектроники" (ТУСУР) | Способ изготовления стоматологического остеоинтегрируемого имплантата |
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| US12233572B2 (en) * | 2019-09-10 | 2025-02-25 | Rolls-Royce High Temperature Composites, Inc. | Methods to eliminate mudcracks in CMC matrix by humidity controlled atmosphere |
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| JP6912689B1 (ja) * | 2019-12-26 | 2021-08-04 | クラレノリタケデンタル株式会社 | 加工性ジルコニア複合焼結体の製造方法、加工性ジルコニア複合焼結体の原料組成物及び加工性ジルコニア複合仮焼体 |
| RU2735890C1 (ru) * | 2020-06-23 | 2020-11-09 | Мааз Магомедович Гадисов | Способ изготовления зубного имплантата |
| FR3112770A1 (fr) * | 2020-07-23 | 2022-01-28 | Mathym | Céramique d’oxyde métallique, ses précurseurs, sa préparation et son utilisation |
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| KR102711498B1 (ko) * | 2021-11-30 | 2024-09-26 | 아주대학교산학협력단 | 세가지 치과용 지르코니아의 표면 형상 변화와 잔류 응력 개선을 위한 샌드블라스팅 표면처리방법 |
| CN118451051A (zh) * | 2021-12-22 | 2024-08-06 | 可乐丽则武齿科株式会社 | 氧化锆组合物、氧化锆预烧体和氧化锆烧结体以及它们的制造方法 |
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2014
- 2014-06-12 CN CN201480036313.0A patent/CN105338948B/zh active Active
- 2014-06-12 CA CA2913112A patent/CA2913112C/en active Active
- 2014-06-12 KR KR1020167000186A patent/KR102215498B1/ko active Active
- 2014-06-12 BR BR112015032559-9A patent/BR112015032559B1/pt not_active IP Right Cessation
- 2014-06-12 JP JP2016523772A patent/JP6416247B2/ja active Active
- 2014-06-12 EP EP14738952.2A patent/EP3013306B1/en not_active Revoked
- 2014-06-12 WO PCT/US2014/042140 patent/WO2014209626A1/en not_active Ceased
- 2014-06-12 US US14/891,756 patent/US10004668B2/en active Active
- 2014-06-12 ES ES14738952T patent/ES2815073T3/es active Active
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| Publication number | Publication date |
|---|---|
| KR20160023766A (ko) | 2016-03-03 |
| EP3013306B1 (en) | 2020-07-22 |
| US20160095798A1 (en) | 2016-04-07 |
| JP2016523286A (ja) | 2016-08-08 |
| US10004668B2 (en) | 2018-06-26 |
| US20180133112A1 (en) | 2018-05-17 |
| CN105338948B (zh) | 2019-02-01 |
| CN105338948A (zh) | 2016-02-17 |
| US20200222287A1 (en) | 2020-07-16 |
| BR112015032559A8 (pt) | 2020-01-07 |
| ES2815073T3 (es) | 2021-03-29 |
| JP2019005627A (ja) | 2019-01-17 |
| WO2014209626A1 (en) | 2014-12-31 |
| BR112015032559A2 (pt) | 2017-07-25 |
| BR112015032559B1 (pt) | 2020-06-16 |
| JP6679687B2 (ja) | 2020-04-15 |
| JP6416247B2 (ja) | 2018-10-31 |
| EP3013306A1 (en) | 2016-05-04 |
| CA2913112A1 (en) | 2014-12-31 |
| US10610460B2 (en) | 2020-04-07 |
| KR102215498B1 (ko) | 2021-02-15 |
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