CA2904650C - Method of isolating blue anthocyanin fractions - Google Patents

Method of isolating blue anthocyanin fractions Download PDF

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Publication number
CA2904650C
CA2904650C CA2904650A CA2904650A CA2904650C CA 2904650 C CA2904650 C CA 2904650C CA 2904650 A CA2904650 A CA 2904650A CA 2904650 A CA2904650 A CA 2904650A CA 2904650 C CA2904650 C CA 2904650C
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CA
Canada
Prior art keywords
fraction
anthocyanin
blue
fractions
anthocyanins
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CA2904650A
Other languages
English (en)
French (fr)
Other versions
CA2904650A1 (en
Inventor
Rebecca J. Robbins
J. Christopher Johnson
Thomas M. Collins
Neda AHMADIANI
M. Monica Giusti
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mars Inc
Ohio State University
Original Assignee
Mars Inc
Ohio State University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mars Inc, Ohio State University filed Critical Mars Inc
Publication of CA2904650A1 publication Critical patent/CA2904650A1/en
Application granted granted Critical
Publication of CA2904650C publication Critical patent/CA2904650C/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof containing fruit or vegetable juices
    • A23L2/04Extraction of juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/52Adding ingredients
    • A23L2/58Colouring agents
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/78Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by ion-exchange
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/40Colouring or decolouring of foods
    • A23L5/42Addition of dyes or pigments, e.g. in combination with optical brighteners
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/40Colouring or decolouring of foods
    • A23L5/42Addition of dyes or pigments, e.g. in combination with optical brighteners
    • A23L5/43Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/26Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction, e.g. ion-exchange, ion-pair, ion-suppression or ion-exclusion
    • B01D15/361Ion-exchange
    • B01D15/362Cation-exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/42Selective adsorption, e.g. chromatography characterised by the development mode, e.g. by displacement or by elution
    • B01D15/424Elution mode
    • B01D15/426Specific type of solvent
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D311/00Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/58Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07HSUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H17/00Compounds containing heterocyclic radicals directly attached to hetero atoms of saccharide radicals
    • C07H17/04Heterocyclic radicals containing only oxygen as ring hetero atoms
    • C07H17/06Benzopyran radicals
    • C07H17/065Benzo[b]pyrans
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Cosmetics (AREA)
CA2904650A 2013-03-15 2014-03-14 Method of isolating blue anthocyanin fractions Active CA2904650C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201361790842P 2013-03-15 2013-03-15
US61/790,842 2013-03-15
PCT/US2014/027319 WO2014152417A2 (en) 2013-03-15 2014-03-14 Method of isolating blue anthocyanin fractions

Publications (2)

Publication Number Publication Date
CA2904650A1 CA2904650A1 (en) 2014-09-25
CA2904650C true CA2904650C (en) 2016-07-12

Family

ID=50733323

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2904650A Active CA2904650C (en) 2013-03-15 2014-03-14 Method of isolating blue anthocyanin fractions

Country Status (11)

Country Link
US (2) US9598581B2 (OSRAM)
EP (1) EP2986675B1 (OSRAM)
JP (1) JP5981675B2 (OSRAM)
CN (1) CN105229084B (OSRAM)
AU (1) AU2014239875B2 (OSRAM)
BR (1) BR112015021402B1 (OSRAM)
CA (1) CA2904650C (OSRAM)
GB (1) GB2527453B (OSRAM)
MX (1) MX362026B (OSRAM)
RU (1) RU2629257C2 (OSRAM)
WO (1) WO2014152417A2 (OSRAM)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5981675B2 (ja) 2013-03-15 2016-08-31 マース インコーポレーテッドMars Incorporated 青色アントシアニン画分の単離方法
CN104961783B (zh) * 2015-04-17 2018-07-10 浙江惠松制药有限公司 一种有效提取花青素和花色苷的方法
CA2990818C (en) * 2015-06-30 2020-06-02 Mars, Incorporated Acylated anthocyanin based colourant composition and methods of use thereof
CA3048457C (en) 2016-12-29 2023-03-07 Mars, Incorporated Edible ink formulations including calcium carbonate
PL3813540T3 (pl) 2018-06-28 2025-03-24 Mars, Incorporated Ulepszone formulacje tuszów jadalnych zawierające węglan wapnia
BR112020026624A2 (pt) 2018-06-28 2021-03-30 Wm. Wrigley Jr. Company Composições opacificantes sem titânio
EP3843555A4 (en) 2018-08-31 2022-07-13 Mars, Incorporated ANTHOCYANINE-BASED DYE COMPOSITIONS AND METHODS OF USE THEREOF
EP4037499A1 (en) 2019-10-01 2022-08-10 Mars Incorporated Enzymatic treatment of anthocyanins
EP3939437A1 (en) * 2020-07-17 2022-01-19 GNT Group B.V. A composition comprising spirulina extract

Family Cites Families (52)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3361631A (en) 1963-09-30 1968-01-02 Sandoz Ag Method of sugar coating pharmaceutical tablets
DE1482489A1 (de) 1965-01-13 1970-03-12 Boehringer Mannheim Gmbh Vollautomatisches Dragierverfahren
NL6601426A (OSRAM) 1965-02-12 1966-08-15
US4172902A (en) 1978-05-26 1979-10-30 The United States Of America As Represented By The Secretary Of Agriculture Stable foods and beverages containing the anthocyanin, peonidin 3-(dicaffeylsophoroside)-5-glucoside
JPS6025181B2 (ja) 1982-10-04 1985-06-17 フロイント産業株式会社 パンコ−チング装置
US4681766A (en) 1986-01-07 1987-07-21 Warner-Lambert Company Coatings for chewing gums containing gum arabic and a soluble calcium salt
JPH083047B2 (ja) 1986-06-21 1996-01-17 サントリー株式会社 天然青色系色素組成物及びそれを用いた着色剤
EP0719093B1 (en) 1993-09-15 2000-03-08 Wm. Wrigley Jr. Company Hard coated chewing gum with improved shelf life, with mixed polyol coatings
JPH07188572A (ja) 1993-12-27 1995-07-25 Kyodo Nyugyo Kk マロ−由来の天然色素
US6190686B1 (en) 1996-01-22 2001-02-20 Chr. Hansen A/S Water dispersible compositions containing natural hydrophobic pigment, method of preparing same and their use
US6541048B2 (en) 1999-09-02 2003-04-01 Wm. Wrigley Jr. Company Coated chewing gum products containing an acid blocker and process of preparing
EP1183954A4 (en) 2000-03-16 2005-02-09 San Ei Gen Ffi Inc DECOLORATION INHIBITORS
EP1293539B1 (en) 2000-05-26 2012-08-29 San-Ei Gen F.F.I., Inc. Method for preparting a deodorized colorant of brassicaceae plant
US6572900B1 (en) 2000-06-09 2003-06-03 Wm. Wrigley, Jr. Company Method for making coated chewing gum products including a high-intensity sweetener
ATE323744T1 (de) 2001-07-26 2006-05-15 Hansens Lab Lebensmittelfärbende substanzen auf anthocyaninbasis
US6881430B2 (en) 2001-07-26 2005-04-19 Chr. Hansen A/S Food coloring substances and method for their preparation
JP4590034B2 (ja) 2002-01-31 2010-12-01 三菱商事フードテック株式会社 硬質糖衣製剤、糖衣液及び硬質糖衣製剤の製造方法
WO2003064538A1 (en) 2002-02-01 2003-08-07 San-Ei Gen F.F.I., Inc. Purified purple corn color and method of preparing the same
DE10227151B4 (de) 2002-06-18 2007-03-15 Wild Flavors Berlin Gmbh & Co. Kg Extrakt aus Nebenprodukten der Nussverarbeitung, Verfahren zu dessen Herstellung und dessen Verwendung
FR2842993B1 (fr) 2002-07-31 2006-02-17 Mars Inc Nouvelle composition de confiserie
US7378118B2 (en) 2002-08-14 2008-05-27 Wm. Wrigley Jr. Company Methods for manufacturing coated confectionary products
US20040105919A1 (en) 2002-12-02 2004-06-03 Mars, Incorporated Processing system having a process injection apparatus
WO2005007088A2 (en) * 2003-07-03 2005-01-27 Unibar Corporation Stabilized anthocyanin extract from garcinia indica
US7279189B2 (en) 2004-07-02 2007-10-09 Colormaker, Inc. Stabilized natural blue and green colorants
JP2008505657A (ja) 2004-07-10 2008-02-28 ザ リサーチ ファウンデイション オブ ステイト ユニバーシティー オブ ニューヨーク 組換え微生物によるフラボノイドの生成
JP5598830B2 (ja) 2004-10-29 2014-10-01 サントリーホールディングス株式会社 アントシアニンの3’位への芳香族アシル基転移酵素をコードする遺伝子を用いたアントシアニン色素の安定化ならびに青色化方法
EP1828331B1 (en) 2004-12-22 2019-01-30 Colarôme Inc. Natural water-insoluble encapsulation compositions and processes for preparing same
RU2302423C2 (ru) * 2005-06-10 2007-07-10 Закрытое акционерное общество "Научно-производственное объединение "ТЕХКОН" Способ выделения биологически активных антоцианов
WO2008111589A1 (ja) 2007-03-12 2008-09-18 National University Corporation Kagawa University 精製アントシアニンの製造方法
FR2914311B1 (fr) 2007-03-28 2011-02-11 Diana Naturals Modification de la nuance colorante d'anthocyanes pour l'obtention de substances colorantes
EP2070422A1 (en) 2007-12-05 2009-06-17 Südzucker Aktiengesellschaft Mannheim/Ochsenfurt Confectionery products promoting dental health
WO2009100165A2 (en) * 2008-02-06 2009-08-13 The Ohio State University Research Foundation High-purity fractionation of anthocyanins from fruits and vegetables
US8575334B2 (en) 2008-02-06 2013-11-05 The Ohio State University Research Foundation High-purity fractionation of anthocyanins from fruits and vegetables
US8557319B2 (en) 2008-03-28 2013-10-15 Wild Flavors, Inc. Stable natural color process, products and use thereof
FR2930557B1 (fr) 2008-04-29 2013-08-30 Lvmh Rech Matieres colorantes d'origine vegetale et leur utilisation pour colorer des compositions, en particulier des compositions cosmetiques
US20090298952A1 (en) 2008-05-07 2009-12-03 Brimmer Karen S Platable soluble dyes
US8642340B2 (en) 2008-12-18 2014-02-04 Dianaplantsciences, Inc. Plant cell culture for production of natural products with reduced glucosinolate contamination
DK2385766T4 (da) 2009-01-07 2022-05-23 Oterra As Sammensætning, der omfatter calciumcarbonat som et hvidt pigment
WO2010114568A1 (en) * 2009-04-03 2010-10-07 Dianaplantsciences, Inc. Methods for creating color variation in anthocyanins produced by cell culture
GB0908397D0 (en) 2009-05-15 2009-06-24 Univ Leeds Natural hair dyes
CA2781256C (en) 2009-11-25 2017-11-07 Sensient Colors Inc. Natural blue-shade colorants and methods of making and using same
JP2012067241A (ja) 2010-09-27 2012-04-05 Riken Vitamin Co Ltd クチナシ青色素の製造方法
US9427007B2 (en) 2010-11-05 2016-08-30 Chr. Hansen Natural Colors A/S Multiple emulsions for colorants
US20130165531A1 (en) 2011-06-13 2013-06-27 E.P.C. (Beijing) Plant Pharmaceutical Technology Co., Ltd. Anthocyanin based colorant compositions
EP2545787B1 (de) 2011-07-11 2016-04-13 RUDOLF WILD GmbH & CO. KG Anthocyanhaltige Zusammensetzung
EP2731462B1 (en) 2011-07-15 2015-10-21 Nestec S.A. Food-grade blue encapsulate and process for the production thereof
WO2013106179A1 (en) 2011-12-19 2013-07-18 Sensient Colors Llc Color compositions and methods of making color compositions comprising starch as a matrix
US20130184359A1 (en) 2012-01-13 2013-07-18 Karim Nafisi-Movaghar Processes for Extracting Colors from Hibiscus Plants
IN2015DN00808A (OSRAM) 2012-08-09 2015-07-03 Nestec Sa
CA2903474C (en) 2013-03-15 2021-04-20 Mars, Incorporated Stabilization of natural blue anthocyanin-containing colorants and products made
MX344806B (es) 2013-03-15 2017-01-09 Mars Inc Colorantes azules naturales que contienen antocianina.
JP5981675B2 (ja) 2013-03-15 2016-08-31 マース インコーポレーテッドMars Incorporated 青色アントシアニン画分の単離方法

Also Published As

Publication number Publication date
US20160017150A1 (en) 2016-01-21
WO2014152417A2 (en) 2014-09-25
BR112015021402A2 (OSRAM) 2017-08-22
CN105229084A (zh) 2016-01-06
MX362026B (es) 2019-01-04
EP2986675A2 (en) 2016-02-24
AU2014239875A1 (en) 2015-11-05
JP2016519177A (ja) 2016-06-30
RU2629257C2 (ru) 2017-08-28
HK1215040A1 (zh) 2016-08-12
GB201517443D0 (en) 2015-11-18
BR112015021402A8 (pt) 2021-09-08
CN105229084B (zh) 2017-09-01
AU2014239875B2 (en) 2016-02-04
MX2015011349A (es) 2016-06-06
US10119029B2 (en) 2018-11-06
GB2527453A (en) 2015-12-23
EP2986675B1 (en) 2016-10-05
WO2014152417A3 (en) 2014-11-20
US20170204269A1 (en) 2017-07-20
CA2904650A1 (en) 2014-09-25
GB2527453B (en) 2017-03-15
BR112015021402B1 (pt) 2021-11-03
RU2015144064A (ru) 2017-04-27
US9598581B2 (en) 2017-03-21
JP5981675B2 (ja) 2016-08-31

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Effective date: 20150908