CA2709072C - Procede de valorisation du petrole lourd comprenant la recuperation de catalyseur use - Google Patents

Procede de valorisation du petrole lourd comprenant la recuperation de catalyseur use Download PDF

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Publication number
CA2709072C
CA2709072C CA2709072A CA2709072A CA2709072C CA 2709072 C CA2709072 C CA 2709072C CA 2709072 A CA2709072 A CA 2709072A CA 2709072 A CA2709072 A CA 2709072A CA 2709072 C CA2709072 C CA 2709072C
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Prior art keywords
heavy oil
solvent
filtration
stream
catalyst
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CA2709072A
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CA2709072A1 (fr
Inventor
Seyi A. Odueyungbo
Lalit S. Shah
Christopher A. Powers
James R. Stoy
Fred D. Brent
Bruce E. Reynolds
Andre R. Da Costa
Paul F. Bryan
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Chevron USA Inc
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Chevron USA Inc
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Priority claimed from US12/004,014 external-priority patent/US8722556B2/en
Priority claimed from US12/004,015 external-priority patent/US8765622B2/en
Application filed by Chevron USA Inc filed Critical Chevron USA Inc
Priority to CA2943442A priority Critical patent/CA2943442C/fr
Publication of CA2709072A1 publication Critical patent/CA2709072A1/fr
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G31/00—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for
    • C10G31/09—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for by filtration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D63/00—Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/06—Tubular membrane modules
    • B01D63/069—Tubular membrane modules comprising a bundle of tubular membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/145—Ultrafiltration
    • B01D61/146—Ultrafiltration comprising multiple ultrafiltration steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/147—Microfiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/147—Microfiltration
    • B01D61/1471—Microfiltration comprising multiple microfiltration steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
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    • B—PERFORMING OPERATIONS; TRANSPORTING
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    • B01J23/90—Regeneration or reactivation
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    • B01J23/94—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides of the iron group metals or copper
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    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
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    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
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    • B01J35/45—Nanoparticles
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G21/00—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
    • C10G21/06—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents characterised by the solvent used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G31/00—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for
    • C10G31/06—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for by heating, cooling, or pressure treatment
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G49/00—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00
    • C10G49/02—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00 characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G49/00—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00
    • C10G49/22—Separation of effluents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/04—Specific process operations in the feed stream; Feed pretreatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
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    • B01D2311/06—Specific process operations in the permeate stream
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
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    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/24—Chromium, molybdenum or tungsten
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    • B01J23/74—Iron group metals
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    • B—PERFORMING OPERATIONS; TRANSPORTING
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    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/755—Nickel
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
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    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • C22B7/009—General processes for recovering metals or metallic compounds from spent catalysts
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

L'invention concerne un procédé pour valoriser du pétrole lourd et le convertir en produits d'hydrocarbures à point d'ébullition bas. Le procédé utilise un catalyseur en suspension comprenant des particules de catalyseur ayant une taille moyenne de particule s'échelonnant entre 1 et 20 microns. Dans le procédé de valorisation, le catalyseur en suspension usé dans le pétrole lourd est généré en tant que flux d'effluent. Dans un aspect de l'invention, le procédé comprend en outre la récupération du catalyseur usé par la séparation du pétrole lourd et des particules de catalyseur en suspension. Dans un mode de réalisation, le catalyseur en suspension dans le pétrole lourd est combiné avec du solvant pour former un flux combiné suspension-solvant. Le flux combiné suspension-solvant est filtré dans une zone de déshuilage par l'intermédiaire d'une filtration sur membrane. Les hydrocarbures, à savoir, le solvant et le pétrole lourd résiduel, peuvent être ultérieurement séparés des particules de catalyseur dans une zone de séchage. Les métaux de valeur peuvent être récupérés à partir des particules de catalyseur afin d'être réutilisés ultérieurement dans une unité de synthèse de catalyseur, en générant un catalyseur en suspension frais.
CA2709072A 2007-12-20 2008-12-19 Procede de valorisation du petrole lourd comprenant la recuperation de catalyseur use Active CA2709072C (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CA2943442A CA2943442C (fr) 2007-12-20 2008-12-19 Procede de valorisation du petrole lourd comprenant la recuperation de catalyseur use

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US12/004,015 2007-12-20
US12/004,014 US8722556B2 (en) 2007-12-20 2007-12-20 Recovery of slurry unsupported catalyst
US12/004,014 2007-12-20
US12/004,015 US8765622B2 (en) 2007-12-20 2007-12-20 Recovery of slurry unsupported catalyst
PCT/US2008/087682 WO2009086107A2 (fr) 2007-12-20 2008-12-19 Procédé de valorisation du pétrole lourd comprenant la récupération de catalyseur usé

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CA2943442A Division CA2943442C (fr) 2007-12-20 2008-12-19 Procede de valorisation du petrole lourd comprenant la recuperation de catalyseur use

Publications (2)

Publication Number Publication Date
CA2709072A1 CA2709072A1 (fr) 2009-07-09
CA2709072C true CA2709072C (fr) 2016-11-29

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Application Number Title Priority Date Filing Date
CA2943442A Active CA2943442C (fr) 2007-12-20 2008-12-19 Procede de valorisation du petrole lourd comprenant la recuperation de catalyseur use
CA3089421A Active CA3089421C (fr) 2007-12-20 2008-12-19 Procede de valorisation du petrole lourd comprenant la recuperation de catalyseur use
CA3212718A Pending CA3212718A1 (fr) 2007-12-20 2008-12-19 Procede de valorisation du petrole lourd comprenant la recuperation de catalyseur use
CA2709072A Active CA2709072C (fr) 2007-12-20 2008-12-19 Procede de valorisation du petrole lourd comprenant la recuperation de catalyseur use

Family Applications Before (3)

Application Number Title Priority Date Filing Date
CA2943442A Active CA2943442C (fr) 2007-12-20 2008-12-19 Procede de valorisation du petrole lourd comprenant la recuperation de catalyseur use
CA3089421A Active CA3089421C (fr) 2007-12-20 2008-12-19 Procede de valorisation du petrole lourd comprenant la recuperation de catalyseur use
CA3212718A Pending CA3212718A1 (fr) 2007-12-20 2008-12-19 Procede de valorisation du petrole lourd comprenant la recuperation de catalyseur use

Country Status (5)

Country Link
KR (1) KR101584200B1 (fr)
CN (1) CN101918516B (fr)
BR (1) BRPI0821358A2 (fr)
CA (4) CA2943442C (fr)
WO (1) WO2009086107A2 (fr)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102413908B (zh) * 2009-04-29 2015-09-23 巴斯夫欧洲公司 借助膜过滤调节催化剂的方法
CN201793528U (zh) * 2010-05-27 2011-04-13 北京中天元环境工程有限责任公司 一种催化裂化油浆过滤设备
HRP20240945T1 (hr) * 2010-12-30 2024-10-25 Chevron U.S.A. Inc. Katalizatori za hidropreradu i postupci njihove priprave
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WO2009086107A3 (fr) 2009-09-24
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