CA2266906A1 - Compositions and insulation bodies having low thermal conductivity - Google Patents
Compositions and insulation bodies having low thermal conductivity Download PDFInfo
- Publication number
- CA2266906A1 CA2266906A1 CA002266906A CA2266906A CA2266906A1 CA 2266906 A1 CA2266906 A1 CA 2266906A1 CA 002266906 A CA002266906 A CA 002266906A CA 2266906 A CA2266906 A CA 2266906A CA 2266906 A1 CA2266906 A1 CA 2266906A1
- Authority
- CA
- Canada
- Prior art keywords
- composition
- gel
- equal
- less
- particulate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 389
- 238000009413 insulation Methods 0.000 title claims abstract description 56
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 58
- 238000012856 packing Methods 0.000 claims abstract description 56
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 29
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 19
- 229910052774 Proactinium Inorganic materials 0.000 claims abstract description 12
- 239000006229 carbon black Substances 0.000 claims description 97
- 239000003795 chemical substances by application Substances 0.000 claims description 82
- 239000002245 particle Substances 0.000 claims description 48
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 23
- 229910044991 metal oxide Inorganic materials 0.000 claims description 8
- 150000004706 metal oxides Chemical class 0.000 claims description 8
- 239000002131 composite material Substances 0.000 claims description 5
- 239000010439 graphite Substances 0.000 claims description 5
- 229910002804 graphite Inorganic materials 0.000 claims description 5
- 238000005057 refrigeration Methods 0.000 claims description 3
- 238000000352 supercritical drying Methods 0.000 claims description 3
- 239000000499 gel Substances 0.000 description 179
- 235000019241 carbon black Nutrition 0.000 description 80
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 65
- IJOOHPMOJXWVHK-UHFFFAOYSA-N chlorotrimethylsilane Chemical compound C[Si](C)(C)Cl IJOOHPMOJXWVHK-UHFFFAOYSA-N 0.000 description 59
- 239000008187 granular material Substances 0.000 description 55
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 42
- 238000000034 method Methods 0.000 description 40
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 36
- 239000007787 solid Substances 0.000 description 29
- 239000005051 trimethylchlorosilane Substances 0.000 description 29
- 239000002904 solvent Substances 0.000 description 26
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 24
- 239000000463 material Substances 0.000 description 24
- 239000007789 gas Substances 0.000 description 23
- 150000001721 carbon Chemical class 0.000 description 20
- 238000001879 gelation Methods 0.000 description 19
- 239000002243 precursor Substances 0.000 description 19
- 150000003839 salts Chemical class 0.000 description 19
- -1 sulfophenyl group Chemical group 0.000 description 19
- 239000011148 porous material Substances 0.000 description 18
- 125000000962 organic group Chemical group 0.000 description 17
- 230000004888 barrier function Effects 0.000 description 16
- 239000002002 slurry Substances 0.000 description 16
- 238000009826 distribution Methods 0.000 description 13
- 238000000227 grinding Methods 0.000 description 11
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 11
- 229910052753 mercury Inorganic materials 0.000 description 11
- 230000002378 acidificating effect Effects 0.000 description 10
- 238000012993 chemical processing Methods 0.000 description 10
- 239000008367 deionised water Substances 0.000 description 10
- 229910021641 deionized water Inorganic materials 0.000 description 10
- 239000012954 diazonium Substances 0.000 description 10
- 150000001989 diazonium salts Chemical class 0.000 description 10
- 238000001035 drying Methods 0.000 description 10
- 230000008569 process Effects 0.000 description 10
- 238000012546 transfer Methods 0.000 description 10
- 230000032683 aging Effects 0.000 description 9
- 239000012530 fluid Substances 0.000 description 9
- 238000005259 measurement Methods 0.000 description 9
- 238000012986 modification Methods 0.000 description 9
- 230000004048 modification Effects 0.000 description 9
- 238000005406 washing Methods 0.000 description 9
- 230000000694 effects Effects 0.000 description 8
- 239000000377 silicon dioxide Substances 0.000 description 8
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 7
- 229910052782 aluminium Inorganic materials 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 7
- 239000011888 foil Substances 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- 239000000843 powder Substances 0.000 description 7
- 230000002829 reductive effect Effects 0.000 description 7
- 239000011240 wet gel Substances 0.000 description 7
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 6
- 150000004703 alkoxides Chemical class 0.000 description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 6
- 150000001450 anions Chemical class 0.000 description 6
- 239000003575 carbonaceous material Substances 0.000 description 6
- 238000005266 casting Methods 0.000 description 6
- 238000004448 titration Methods 0.000 description 6
- 229920000877 Melamine resin Polymers 0.000 description 5
- 239000004743 Polypropylene Substances 0.000 description 5
- 239000004809 Teflon Substances 0.000 description 5
- 229920006362 Teflon® Polymers 0.000 description 5
- 239000004964 aerogel Substances 0.000 description 5
- 125000003118 aryl group Chemical group 0.000 description 5
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 5
- 239000012774 insulation material Substances 0.000 description 5
- 229910052751 metal Inorganic materials 0.000 description 5
- 239000002184 metal Substances 0.000 description 5
- 229920001155 polypropylene Polymers 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 238000012545 processing Methods 0.000 description 5
- 230000005855 radiation Effects 0.000 description 5
- 230000000717 retained effect Effects 0.000 description 5
- 239000007790 solid phase Substances 0.000 description 5
- 235000011149 sulphuric acid Nutrition 0.000 description 5
- DGXAGETVRDOQFP-UHFFFAOYSA-N 2,6-dihydroxybenzaldehyde Chemical compound OC1=CC=CC(O)=C1C=O DGXAGETVRDOQFP-UHFFFAOYSA-N 0.000 description 4
- 239000004965 Silica aerogel Substances 0.000 description 4
- 239000004115 Sodium Silicate Substances 0.000 description 4
- 239000004775 Tyvek Substances 0.000 description 4
- 229920000690 Tyvek Polymers 0.000 description 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
- 239000012298 atmosphere Substances 0.000 description 4
- 238000007796 conventional method Methods 0.000 description 4
- 238000000354 decomposition reaction Methods 0.000 description 4
- 125000000524 functional group Chemical group 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000011159 matrix material Substances 0.000 description 4
- 239000012071 phase Substances 0.000 description 4
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 4
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 4
- 229910052911 sodium silicate Inorganic materials 0.000 description 4
- 238000010998 test method Methods 0.000 description 4
- 125000004400 (C1-C12) alkyl group Chemical group 0.000 description 3
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- 150000001412 amines Chemical class 0.000 description 3
- 125000002091 cationic group Chemical group 0.000 description 3
- IVJISJACKSSFGE-UHFFFAOYSA-N formaldehyde;1,3,5-triazine-2,4,6-triamine Chemical compound O=C.NC1=NC(N)=NC(N)=N1 IVJISJACKSSFGE-UHFFFAOYSA-N 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 230000000977 initiatory effect Effects 0.000 description 3
- 239000000976 ink Substances 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- 125000001624 naphthyl group Chemical group 0.000 description 3
- 230000001698 pyrogenic effect Effects 0.000 description 3
- 239000012429 reaction media Substances 0.000 description 3
- 238000007789 sealing Methods 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000000741 silica gel Substances 0.000 description 3
- 229910002027 silica gel Inorganic materials 0.000 description 3
- HVBSAKJJOYLTQU-UHFFFAOYSA-N 4-aminobenzenesulfonic acid Chemical compound NC1=CC=C(S(O)(=O)=O)C=C1 HVBSAKJJOYLTQU-UHFFFAOYSA-N 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- 229910006069 SO3H Inorganic materials 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 229910052681 coesite Inorganic materials 0.000 description 2
- 229910052906 cristobalite Inorganic materials 0.000 description 2
- 238000006073 displacement reaction Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 150000004820 halides Chemical class 0.000 description 2
- 239000011810 insulating material Substances 0.000 description 2
- 125000003010 ionic group Chemical group 0.000 description 2
- 239000003605 opacifier Substances 0.000 description 2
- 239000011236 particulate material Substances 0.000 description 2
- 239000008188 pellet Substances 0.000 description 2
- 125000005496 phosphonium group Chemical group 0.000 description 2
- 125000001453 quaternary ammonium group Chemical group 0.000 description 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 2
- 238000003980 solgel method Methods 0.000 description 2
- 229910052682 stishovite Inorganic materials 0.000 description 2
- 125000001424 substituent group Chemical group 0.000 description 2
- 229910052905 tridymite Inorganic materials 0.000 description 2
- YUUDLHZAWCQVDJ-UHFFFAOYSA-N 4-sulfobenzenediazonium;hydroxide Chemical compound [OH-].OS(=O)(=O)C1=CC=C([N+]#N)C=C1 YUUDLHZAWCQVDJ-UHFFFAOYSA-N 0.000 description 1
- 229920013683 Celanese Polymers 0.000 description 1
- 241000721047 Danaus plexippus Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229910005451 FeTiO3 Inorganic materials 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 239000004235 Orange GGN Substances 0.000 description 1
- 229910018828 PO3H2 Inorganic materials 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 241000872198 Serjania polyphylla Species 0.000 description 1
- 229920006328 Styrofoam Polymers 0.000 description 1
- 150000004645 aluminates Chemical class 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 239000010426 asphalt Substances 0.000 description 1
- 150000001555 benzenes Chemical class 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 125000002843 carboxylic acid group Chemical group 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 238000007385 chemical modification Methods 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 229910052593 corundum Inorganic materials 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000010981 drying operation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- GBVVPXXNNHWBPE-UHFFFAOYSA-N formaldehyde;1,3,5-triazine-2,4,6-triamine Chemical compound O=C.O=C.NC1=NC(N)=NC(N)=N1 GBVVPXXNNHWBPE-UHFFFAOYSA-N 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical group 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 1
- 235000013980 iron oxide Nutrition 0.000 description 1
- VBMVTYDPPZVILR-UHFFFAOYSA-N iron(2+);oxygen(2-) Chemical class [O-2].[Fe+2] VBMVTYDPPZVILR-UHFFFAOYSA-N 0.000 description 1
- 229910052743 krypton Inorganic materials 0.000 description 1
- DNNSSWSSYDEUBZ-UHFFFAOYSA-N krypton atom Chemical compound [Kr] DNNSSWSSYDEUBZ-UHFFFAOYSA-N 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 238000010943 off-gassing Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- 238000005453 pelletization Methods 0.000 description 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N phosphonic acid group Chemical group P(O)(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 1
- 239000006069 physical mixture Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000002985 plastic film Substances 0.000 description 1
- 229920006255 plastic film Polymers 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000000452 restraining effect Effects 0.000 description 1
- 238000001878 scanning electron micrograph Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 235000010288 sodium nitrite Nutrition 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000008261 styrofoam Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229950000244 sulfanilic acid Drugs 0.000 description 1
- 125000000626 sulfinic acid group Chemical group 0.000 description 1
- 125000000542 sulfonic acid group Chemical group 0.000 description 1
- 239000002352 surface water Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000012956 testing procedure Methods 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 229910052724 xenon Inorganic materials 0.000 description 1
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 1
- 229910001845 yogo sapphire Inorganic materials 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Thermal Insulation (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Silicon Compounds (AREA)
- Carbon And Carbon Compounds (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
- Colloid Chemistry (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/721,797 | 1996-09-27 | ||
| US08/721,797 US5877100A (en) | 1996-09-27 | 1996-09-27 | Compositions and insulation bodies having low thermal conductivity |
| PCT/US1997/016520 WO1998013135A1 (en) | 1996-09-27 | 1997-09-18 | Compositions and insulation bodies having low thermal conductivity |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2266906A1 true CA2266906A1 (en) | 1998-04-02 |
Family
ID=24899342
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002266906A Abandoned CA2266906A1 (en) | 1996-09-27 | 1997-09-18 | Compositions and insulation bodies having low thermal conductivity |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US5877100A (enExample) |
| EP (1) | EP0930935A1 (enExample) |
| JP (2) | JP2001502367A (enExample) |
| KR (1) | KR20000048699A (enExample) |
| CN (1) | CN1104944C (enExample) |
| AU (1) | AU713901B2 (enExample) |
| CA (1) | CA2266906A1 (enExample) |
| HU (1) | HUP0000067A3 (enExample) |
| TR (1) | TR199901377T2 (enExample) |
| TW (1) | TW371273B (enExample) |
| WO (1) | WO1998013135A1 (enExample) |
Families Citing this family (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6043172A (en) * | 1998-01-14 | 2000-03-28 | Global Consulting, Inc. | Ceramic fiber insulation material |
| US6485805B1 (en) * | 1998-01-15 | 2002-11-26 | Cabot Corporation | Multilayer insulation composite |
| DE69914385T2 (de) * | 1998-03-06 | 2004-11-04 | Matsushita Electric Industrial Co., Ltd., Kadoma | Wiederverwendung von vernetztem Phenolharz |
| US6544618B1 (en) * | 1999-05-06 | 2003-04-08 | Cabot Corporation | Thermally reflective layer-porous metal oxide film insulation composite |
| US6824820B1 (en) | 1999-06-07 | 2004-11-30 | 3M Innovative Properties Company | Polyurea-based adhesives, articles therefrom and methods of their preparation and use |
| CN1306993C (zh) * | 2000-12-22 | 2007-03-28 | 思攀气凝胶公司 | 带有纤维胎的气凝胶复合材料 |
| US7222821B2 (en) * | 2001-11-21 | 2007-05-29 | Matos Jeffrey A | Method and apparatus for treating fuel to temporarily reduce its combustibility |
| US8042771B2 (en) | 2007-05-25 | 2011-10-25 | Karl F. Milde, Jr. | Method and apparatus for treating fuel to temporarily reduce its combustibility |
| US20040018336A1 (en) * | 2002-07-29 | 2004-01-29 | Brian Farnworth | Thermally insulating products for footwear and other apparel |
| KR20060019576A (ko) * | 2003-07-04 | 2006-03-03 | 마쯔시다덴기산교 가부시키가이샤 | 진공 단열재 및 이를 이용한 기기 |
| US20060035054A1 (en) * | 2004-01-05 | 2006-02-16 | Aspen Aerogels, Inc. | High performance vacuum-sealed insulations |
| JP4245514B2 (ja) * | 2004-05-24 | 2009-03-25 | 日信工業株式会社 | 炭素繊維複合材料及びその製造方法、炭素繊維複合金属材料の製造方法、炭素繊維複合非金属材料の製造方法 |
| US7833916B2 (en) * | 2004-06-29 | 2010-11-16 | Aspen Aerogels, Inc. | Energy efficient and insulated building envelopes |
| EP1789719A2 (en) * | 2004-09-01 | 2007-05-30 | Aspen Aerogels Inc. | High performance vacuum-sealed insulations |
| US8011151B2 (en) * | 2009-03-12 | 2011-09-06 | Robert William Pollack | Multi-layer building insulation and wallboard sheet with multi-layer insulation |
| WO2006091812A2 (en) * | 2005-02-25 | 2006-08-31 | Aspen Aerogels, Inc. | Insulated roofing systems |
| US8003028B2 (en) * | 2005-07-26 | 2011-08-23 | The Boeing Company | Composite of aerogel and phase change material |
| US8163075B2 (en) | 2006-10-31 | 2012-04-24 | Sensient Colors Llc | Inks comprising modified pigments and methods for making and using the same |
| US7953247B2 (en) | 2007-05-21 | 2011-05-31 | Snap-On Incorporated | Method and apparatus for wheel alignment |
| CN101855302B (zh) | 2007-08-23 | 2014-10-01 | 森馨颜色公司 | 自分散颜料及制造和使用该自分散颜料的方法 |
| US20090173570A1 (en) * | 2007-12-20 | 2009-07-09 | Levit Natalia V | Acoustically absorbent ceiling tile having barrier facing with diffuse reflectance |
| US20090173569A1 (en) * | 2007-12-20 | 2009-07-09 | E. I. Du Pont De Nemours And Company | Acoustic absorber with barrier facing |
| DE102008040367A1 (de) | 2008-07-11 | 2010-02-25 | Evonik Degussa Gmbh | Bauteil zur Herstellung von Vakuumisolationssystemen |
| DE102008046444A1 (de) | 2008-09-09 | 2010-03-11 | Evonik Röhm Gmbh | Fassadenplatte, System und Verfahren zur Energiegewinnung |
| JP2012523479A (ja) | 2009-04-07 | 2012-10-04 | センシエント カラーズ エルエルシー | 自己分散性粒子並びにその製造方法及び使用方法 |
| WO2011020671A1 (de) | 2009-08-20 | 2011-02-24 | Evonik Röhm Gmbh | Dämmplatte aus kunststoff, system und verfahren zur wärmedämmung |
| JP5669617B2 (ja) * | 2011-02-21 | 2015-02-12 | 株式会社トクヤマ | エアロゲル及び該エアロゲルを用いた断熱材 |
| FR2996849B1 (fr) * | 2012-10-17 | 2015-10-16 | Hutchinson | Composition pour gel organique ou son pyrolysat, son procede de preparation, electrode constituee du pyrolysat et supercondensateur l'incorporant. |
| FR2996850B1 (fr) * | 2012-10-17 | 2016-01-08 | Hutchinson | Composition thermiquement isolante pour gel monolithique organique ou son pyrolysat, son utilisation et son procede de preparation. |
| US9557009B2 (en) | 2013-11-06 | 2017-01-31 | General Electric Company | Gas reservoir and a method to supply gas to plasma tubes |
| US9330876B2 (en) | 2013-11-06 | 2016-05-03 | General Electric Company | Systems and methods for regulating pressure of a filled-in gas |
| KR102168978B1 (ko) * | 2014-02-12 | 2020-10-22 | 허친슨 | 유기 에어로겔을 포함하는 진공 단열 패널 |
| US10501326B2 (en) | 2015-09-10 | 2019-12-10 | Lg Chem, Ltd. | Silica aerogel-including blanket and method for preparing the same |
| WO2017043721A1 (ko) * | 2015-09-10 | 2017-03-16 | 주식회사 엘지화학 | 실리카 에어로겔 포함 블랑켓 및 이의 제조방법 |
| US11264697B2 (en) | 2016-10-18 | 2022-03-01 | American Aerogel Corporation | Linked antenna pair for transmission through shielded shipping container |
| US10822807B2 (en) | 2019-02-18 | 2020-11-03 | Royal Building Products (Usa) Inc. | Assembly for improved insulation |
| WO2024081368A1 (en) | 2022-10-13 | 2024-04-18 | Aspen Aerogels, Inc. | Compressed aerogel composite and method of making |
Family Cites Families (77)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2745173A (en) * | 1951-07-14 | 1956-05-15 | Gen Electric | Method of thermal insulation |
| US2973282A (en) * | 1955-07-23 | 1961-02-28 | Degussa | Process for the surface treatment of finely-divided oxides or oxide mixtures |
| US3453127A (en) * | 1963-10-18 | 1969-07-01 | Monsanto Co | Flatted coating compositions containing silica aerogel and processes for preparing same |
| NL6411993A (enExample) * | 1963-10-18 | 1965-04-20 | ||
| GB1268626A (en) * | 1968-07-10 | 1972-03-29 | British Aircraft Corp Ltd | Improvements in and relating to thermal insulation elements |
| GB1350661A (en) * | 1970-06-10 | 1974-04-18 | Micropore International Ltd | Thermal insulating materials |
| US3869334A (en) * | 1971-06-10 | 1975-03-04 | Micropore Insulation Limited | Insulating materials |
| US3790243A (en) * | 1972-03-30 | 1974-02-05 | Beverage Air Sales Co | Closure for refrigerated housing |
| DE2414478C3 (de) * | 1974-03-26 | 1978-07-13 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Aerogelartige strukturierte Kieselsäure und Verfahren zu ihrer Herstellung |
| FR2360536A1 (fr) * | 1976-08-05 | 1978-03-03 | Air Liquide | Materiau isolant a faible conductibilite thermique constitue d'une structure granulaire compactee |
| DE2928695C2 (de) * | 1979-07-16 | 1984-05-30 | Grünzweig + Hartmann und Glasfaser AG, 6700 Ludwigshafen | Wärmeisolierkörper sowie Verfahren zu seiner Herstellung |
| US4284674A (en) * | 1979-11-08 | 1981-08-18 | American Can Company | Thermal insulation |
| GB2100269B (en) * | 1981-06-12 | 1985-06-12 | Nat Res Dev | Preparation of particulate gels |
| US4444821A (en) * | 1982-11-01 | 1984-04-24 | General Electric Company | Vacuum thermal insulation panel |
| SE8403888L (sv) * | 1983-08-04 | 1985-02-05 | Micropore International Ltd | Vermeisolerande kropp och sett att framstella denna |
| JPS6071881A (ja) * | 1983-09-28 | 1985-04-23 | 松下電器産業株式会社 | 断熱構造体 |
| US4583351A (en) * | 1984-03-21 | 1986-04-22 | Fallas David M | Automatic case packing apparatus |
| DE3418637A1 (de) * | 1984-05-18 | 1985-11-21 | Wacker-Chemie GmbH, 8000 München | Waermedaemmformkoerper mit umhuellung |
| DE3429671A1 (de) * | 1984-08-11 | 1986-02-20 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von aerogelen |
| FR2584698B1 (fr) * | 1985-07-15 | 1990-05-18 | Rhone Poulenc Spec Chim | Procede de preparation de particules de silice spheroidales |
| DE3533805C2 (de) * | 1985-09-21 | 1996-02-29 | Basf Ag | Verfahren zur Herstellung von Isolierscheiben mit hoher Wärme- und/oder Schallisolierung |
| US4681788A (en) * | 1986-07-31 | 1987-07-21 | General Electric Company | Insulation formed of precipitated silica and fly ash |
| US4726974A (en) * | 1986-10-08 | 1988-02-23 | Union Carbide Corporation | Vacuum insulation panel |
| US4798753A (en) * | 1986-12-19 | 1989-01-17 | General Electric Company | Insulating panels containing insulating powders and insulating gases |
| GB2210036B (en) * | 1987-03-26 | 1992-01-29 | Matsushita Electric Works Ltd | Method for manufacturing fine porous member |
| DE3814968A1 (de) * | 1988-05-03 | 1989-11-16 | Basf Ag | Daemmstoff der dichte 0,1 bis 0,4 g/cm(pfeil hoch)3(pfeil hoch) |
| US4997804A (en) * | 1988-05-26 | 1991-03-05 | The United States Of America As Represented By The United States Department Of Energy | Low density, resorcinol-formaldehyde aerogels |
| US4954327A (en) * | 1988-08-12 | 1990-09-04 | Blount David H | Production of silica aerogels |
| DE3914850A1 (de) * | 1989-05-05 | 1990-11-08 | Basf Ag | Thermisches isoliermaterial auf der basis von pigmenthaltigen kieselsaeureaerogelen |
| US5316816A (en) * | 1989-05-10 | 1994-05-31 | Degussa Aktiengesellschaft | Form body for heat insulation and vacuum insulation panel with asymmetric design |
| DE3924244A1 (de) * | 1989-07-21 | 1991-01-31 | Henkel Kgaa | Verfahren zur herstellung von si0(pfeil abwaerts)2(pfeil abwaerts)-aerogelen (i) |
| DE3924243A1 (de) * | 1989-07-21 | 1991-01-24 | Henkel Kgaa | Verfahren zur herstellung von si0(pfeil abwaerts)2(pfeil abwaerts)-aerogelen (ii) |
| US5032439A (en) * | 1989-08-25 | 1991-07-16 | Massachusetts Institute Of Technology | Thermal insulations using vacuum panels |
| US5091233A (en) * | 1989-12-18 | 1992-02-25 | Whirlpool Corporation | Getter structure for vacuum insulation panels |
| US5082335A (en) * | 1989-12-18 | 1992-01-21 | Whirlpool Corporation | Vacuum insulation system for insulating refrigeration cabinets |
| US5018328A (en) * | 1989-12-18 | 1991-05-28 | Whirlpool Corporation | Multi-compartment vacuum insulation panels |
| US5084320A (en) * | 1990-01-22 | 1992-01-28 | Barito Robert W | Evacuated thermal insulation |
| IT1240673B (it) * | 1990-04-24 | 1993-12-17 | Tenav | Microsfere di aerogels di ossidi inorganici a stretta distribuzione dei diametri dei pori e metodo per la loro preparazione |
| US5409683A (en) * | 1990-08-23 | 1995-04-25 | Regents Of The University Of California | Method for producing metal oxide aerogels |
| DE69128073T2 (de) * | 1990-08-23 | 1998-02-26 | Univ California As Represented | Verfahren zur herstellung von metalloxidaerogelen mit dichte weniger als 0,02 g/cm3 |
| US5252408A (en) * | 1990-09-24 | 1993-10-12 | Aladdin Industries, Inc. | Vacuum insulated panel and method of forming a vacuum insulated panel |
| US5076984A (en) * | 1990-10-10 | 1991-12-31 | Raytheon Company | Method for fabricating thermal insulation |
| DE4038784A1 (de) * | 1990-12-05 | 1992-06-11 | Basf Ag | Verbundschaumstoffe mit niedriger waermeleitfaehigkeit |
| US5086085A (en) * | 1991-04-11 | 1992-02-04 | The United States Of America As Represented By The Department Of Energy | Melamine-formaldehyde aerogels |
| US5306555A (en) * | 1991-09-18 | 1994-04-26 | Battelle Memorial Institute | Aerogel matrix composites |
| US5376424A (en) * | 1991-10-02 | 1994-12-27 | Fujimori Kogyo Co., Ltd. | Vacuum thermal insulating panel and method for preparing same |
| US5401596A (en) * | 1991-10-14 | 1995-03-28 | Stoilov; Georgi T. | Hermetically sealed dry accumulator |
| US5273801A (en) * | 1991-12-31 | 1993-12-28 | Whirlpool Corporation | Thermoformed vacuum insulation container |
| SE507295C2 (sv) * | 1992-01-18 | 1998-05-11 | Thyssen Nordseewerke Gmbh | Värmeisoleringsformkroppar |
| DE4201306A1 (de) * | 1992-01-20 | 1993-07-22 | Basf Ag | Formteile oder platten aus silica-aerogelen |
| US5565142A (en) * | 1992-04-01 | 1996-10-15 | Deshpande; Ravindra | Preparation of high porosity xerogels by chemical surface modification. |
| JP2911693B2 (ja) * | 1992-11-13 | 1999-06-23 | 大陽東洋酸素株式会社 | 真空断熱構造体 |
| DE4300598A1 (de) * | 1993-01-13 | 1994-07-14 | Basf Ag | Kohlenstoff-Partikel enthaltende SiO¶2¶-Aerogele und Verfahren zu ihrer Herstellung |
| US5331789A (en) * | 1993-03-23 | 1994-07-26 | Whirlpool Corporation | Vacuum processing machine and method |
| US5364577A (en) * | 1993-03-23 | 1994-11-15 | Whirlpool Corporation | Vacuum panel manufacturing process |
| US5327703A (en) * | 1993-03-23 | 1994-07-12 | Whirlpool Corporation | Vacuum panel assembly method |
| US5395805A (en) * | 1993-03-25 | 1995-03-07 | Regents Of The University Of California | Method for making monolithic metal oxide aerogels |
| US5420168A (en) * | 1993-04-01 | 1995-05-30 | The Regents Of The University Of California | Method of low pressure and/or evaporative drying of aerogel |
| DE4316540A1 (de) * | 1993-05-18 | 1994-11-24 | Hoechst Ag | Verfahren zur unterkritischen Trocknung von Aerogelen |
| GB9312868D0 (en) * | 1993-06-22 | 1993-08-04 | Ici Plc | Microvoid polyurethane materials |
| GB9312869D0 (en) * | 1993-06-22 | 1993-08-04 | Ici Plc | Evacuated insulation panels |
| US5478867A (en) * | 1993-07-07 | 1995-12-26 | The Dow Chemical Company | Microporous isocyanate-based polymer compositions and method of preparation |
| US5376449A (en) * | 1993-07-09 | 1994-12-27 | Martin Marietta Energy Systems, Inc. | Silica powders for powder evacuated thermal insulating panel and method |
| US5397807A (en) * | 1993-10-14 | 1995-03-14 | The Dow Chemical Company | Compatibilized carbon black and a process and a method for using |
| DE4336269C2 (de) * | 1993-10-23 | 1995-09-21 | Veitsch Radex Ag | Verwendung einer feuerfesten keramischen Masse |
| JPH07239088A (ja) * | 1994-02-24 | 1995-09-12 | Matsushita Electric Ind Co Ltd | 真空断熱体および断熱箱体 |
| JPH0834678A (ja) * | 1994-07-27 | 1996-02-06 | Matsushita Electric Works Ltd | エアロゲルパネル |
| DE4430669A1 (de) * | 1994-08-29 | 1996-03-07 | Hoechst Ag | Verfahren zur Herstellung von faserverstärkten Xerogelen, sowie ihre Verwendung |
| JPH08105592A (ja) * | 1994-10-04 | 1996-04-23 | Matsushita Refrig Co Ltd | 真空断熱体および真空断熱体の製造方法 |
| JPH08105687A (ja) * | 1994-10-05 | 1996-04-23 | Hitachi Ltd | 真空断熱材 |
| DE4437424A1 (de) * | 1994-10-20 | 1996-04-25 | Hoechst Ag | Aerogelhaltige Zusammensetzung, Verfahren zu ihrer Herstellung sowie ihre Verwendung |
| DE4439217A1 (de) * | 1994-11-03 | 1996-05-09 | Hoechst Ag | Verfahren zur Herstellung von Aerogelen |
| DE4441567A1 (de) * | 1994-11-23 | 1996-05-30 | Hoechst Ag | Aerogelhaltiges Verbundmaterial, Verfahren zu seiner Herstellung sowie seine Verwendung |
| FI972164L (fi) * | 1994-11-23 | 1997-07-21 | Hoechst Ag | Aerogeelipitoinen komposiittimateriaali, menetelmä sen valmistamiseksi ja sen käyttö |
| JPH08159377A (ja) * | 1994-12-02 | 1996-06-21 | Matsushita Refrig Co Ltd | 真空断熱体 |
| US5807494A (en) * | 1994-12-15 | 1998-09-15 | Boes; Ralph Ulrich | Gel compositions comprising silica and functionalized carbon products |
| WO1996027754A1 (en) * | 1995-03-07 | 1996-09-12 | Matsushita Refrigeration Company | Vacuum heat-insulator and heat-insulating box using the insulator |
-
1996
- 1996-09-27 US US08/721,797 patent/US5877100A/en not_active Expired - Lifetime
-
1997
- 1997-09-09 TW TW086113047A patent/TW371273B/zh active
- 1997-09-18 JP JP10515721A patent/JP2001502367A/ja not_active Withdrawn
- 1997-09-18 TR TR1999/01377T patent/TR199901377T2/xx unknown
- 1997-09-18 AU AU44218/97A patent/AU713901B2/en not_active Ceased
- 1997-09-18 CA CA002266906A patent/CA2266906A1/en not_active Abandoned
- 1997-09-18 WO PCT/US1997/016520 patent/WO1998013135A1/en not_active Ceased
- 1997-09-18 HU HU0000067A patent/HUP0000067A3/hu unknown
- 1997-09-18 CN CN97199944A patent/CN1104944C/zh not_active Expired - Fee Related
- 1997-09-18 KR KR1019990702654A patent/KR20000048699A/ko not_active Ceased
- 1997-09-18 EP EP97942540A patent/EP0930935A1/en not_active Withdrawn
-
2008
- 2008-09-04 JP JP2008227589A patent/JP2009058130A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| US5877100A (en) | 1999-03-02 |
| CN1104944C (zh) | 2003-04-09 |
| WO1998013135A1 (en) | 1998-04-02 |
| HUP0000067A3 (en) | 2002-11-28 |
| AU713901B2 (en) | 1999-12-16 |
| AU4421897A (en) | 1998-04-17 |
| TR199901377T2 (xx) | 1999-11-22 |
| JP2001502367A (ja) | 2001-02-20 |
| CN1238713A (zh) | 1999-12-15 |
| JP2009058130A (ja) | 2009-03-19 |
| HUP0000067A2 (hu) | 2000-06-28 |
| EP0930935A1 (en) | 1999-07-28 |
| TW371273B (en) | 1999-10-01 |
| KR20000048699A (ko) | 2000-07-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| AU713901B2 (en) | Compositions and insulation bodies having low thermal conductivity | |
| KR100477291B1 (ko) | 저밀도 겔 조성물의 제조 방법 | |
| EP0871540B1 (en) | Gel composition containing carbonaceous compound | |
| US5705535A (en) | Method for the subcritical drying of aerogels | |
| US20080081014A1 (en) | Rapid preparation process of aerogel | |
| CN112424144B (zh) | 在环境压力下使基于二氧化硅的成型隔绝材料体疏水化的方法 | |
| EP2889526A1 (en) | Vacuum heat-insulating material and method for manufacturing vacuum heat-insulating material | |
| US12378128B2 (en) | Method for producing aerogels and aerogels obtained using said method | |
| WO2005110919A1 (ja) | シリカエアロゲルの製造方法 | |
| CN105283495A (zh) | 包含无机气凝胶及三聚氰胺泡绵的绝缘复合材料 | |
| KR20120033159A (ko) | 실리카 에어로겔 과립의 제조방법 | |
| JP3339393B2 (ja) | 疎水性エアロゲルの製法 | |
| Alviso et al. | Resorcinol-formaldehyde and carbon aerogel microspheres | |
| CZ110499A3 (cs) | Zrnitá kompozice a izolační tělesa mající nízkou tepelnou vodivost | |
| Liu et al. | Carbon-silica xerogel and aerogel composites | |
| JP2004307336A (ja) | 成形体の製造方法、成形体、その使用及び遮断材料及び支持パネル | |
| RU2836464C2 (ru) | Способ получения аэрогелей и полученные им аэрогели | |
| JPH10130003A (ja) | 金属酸化物エアロゲルの製造方法 | |
| JP2024072171A (ja) | エアロゲル複合体 | |
| MXPA97004382A (es) | Composicion en gel que contiene un compuestocarbonaceo | |
| MXPA99009251A (en) | Process for producing low density gel compositions |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| FZDE | Discontinued |