CA1100492A - Process and apparatus for continuous acid hydrolysis and saccharification - Google Patents

Process and apparatus for continuous acid hydrolysis and saccharification

Info

Publication number
CA1100492A
CA1100492A CA300,079A CA300079A CA1100492A CA 1100492 A CA1100492 A CA 1100492A CA 300079 A CA300079 A CA 300079A CA 1100492 A CA1100492 A CA 1100492A
Authority
CA
Canada
Prior art keywords
reactor
acid
hydrolysis
solid
sugars
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA300,079A
Other languages
English (en)
French (fr)
Inventor
Alain Regnault
Jean-Pierre Sachetto
Herve Tournier
Thomas Hamm
Jean-Michel Armanet
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Battelle Memorial Institute Inc
Original Assignee
Battelle Memorial Institute Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Battelle Memorial Institute Inc filed Critical Battelle Memorial Institute Inc
Application granted granted Critical
Publication of CA1100492A publication Critical patent/CA1100492A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K1/00—Glucose; Glucose-containing syrups
    • C13K1/02—Glucose; Glucose-containing syrups obtained by saccharification of cellulosic materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Organic Chemistry (AREA)
  • Saccharide Compounds (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
CA300,079A 1977-04-01 1978-03-30 Process and apparatus for continuous acid hydrolysis and saccharification Expired CA1100492A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH412077A CH609092A5 (US07943777-20110517-C00090.png) 1977-04-01 1977-04-01
CH4120/77 1977-04-01

Publications (1)

Publication Number Publication Date
CA1100492A true CA1100492A (en) 1981-05-05

Family

ID=4270183

Family Applications (1)

Application Number Title Priority Date Filing Date
CA300,079A Expired CA1100492A (en) 1977-04-01 1978-03-30 Process and apparatus for continuous acid hydrolysis and saccharification

Country Status (24)

Country Link
US (3) US4199371A (US07943777-20110517-C00090.png)
JP (1) JPS53124632A (US07943777-20110517-C00090.png)
AT (1) AT361418B (US07943777-20110517-C00090.png)
AU (1) AU518576B2 (US07943777-20110517-C00090.png)
BE (1) BE865584A (US07943777-20110517-C00090.png)
BR (1) BR7802044A (US07943777-20110517-C00090.png)
CA (1) CA1100492A (US07943777-20110517-C00090.png)
CH (1) CH609092A5 (US07943777-20110517-C00090.png)
CU (1) CU21104A (US07943777-20110517-C00090.png)
DE (1) DE2814067A1 (US07943777-20110517-C00090.png)
DK (1) DK144578A (US07943777-20110517-C00090.png)
EG (1) EG13177A (US07943777-20110517-C00090.png)
ES (1) ES468437A1 (US07943777-20110517-C00090.png)
FI (1) FI63965C (US07943777-20110517-C00090.png)
FR (1) FR2395314A1 (US07943777-20110517-C00090.png)
GB (1) GB1562682A (US07943777-20110517-C00090.png)
IT (1) IT1093515B (US07943777-20110517-C00090.png)
MX (1) MX5047E (US07943777-20110517-C00090.png)
NL (1) NL7803360A (US07943777-20110517-C00090.png)
NO (1) NO145694C (US07943777-20110517-C00090.png)
NZ (1) NZ186826A (US07943777-20110517-C00090.png)
OA (1) OA05924A (US07943777-20110517-C00090.png)
PL (1) PL205735A1 (US07943777-20110517-C00090.png)
SE (1) SE439648B (US07943777-20110517-C00090.png)

Families Citing this family (36)

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CH625251A5 (US07943777-20110517-C00090.png) * 1978-10-04 1981-09-15 Battelle Memorial Institute
NZ193139A (en) * 1979-03-23 1982-05-25 Univ California Hydrolysis of cellulosic and lignocellulosic material to produce monosaccharides ethanol and methane
US4384897A (en) * 1981-11-23 1983-05-24 The Regents Of The University Of California Method of treating biomass material
US4237110A (en) * 1979-04-30 1980-12-02 The Dow Chemical Company Process for separating and recovering concentrated hydrochloric acid from the crude product obtained from the acid hydrolysis of cellulose
FI58346C (fi) * 1979-12-18 1981-01-12 Tampella Oy Ab Foerfarande foer kontinuerlig foersockring av cellulosa av vaextmaterial
DE3437689A1 (de) * 1984-10-15 1986-04-17 Hoechst Ag, 6230 Frankfurt Vorrichtung zur reduktion von eisen und vanadium in phosphorsaurer loesung
US4933283A (en) * 1985-05-15 1990-06-12 Mobil Oil Corporation Process for converting cellulosic materials to hydrocarbon products
US6022419A (en) * 1996-09-30 2000-02-08 Midwest Research Institute Hydrolysis and fractionation of lignocellulosic biomass
BR9902607B1 (pt) * 1999-06-23 2010-08-24 aparelho e processo de prÉ-hidràlise de biomassa.
US20230304739A1 (en) * 2004-05-04 2023-09-28 Sibelco North America Inc. Rotary batch reactor vessel
BRPI0514717A (pt) * 2004-09-01 2008-06-24 Shell Int Research vaso reator substancialmente horizontal, reator, e, processos de contatar um reagente lìquido com um reagente gasoso e de fabricar um hidroperóxido orgánico
RS52032B (en) * 2004-11-29 2012-04-30 Inbicon A/S ENZYMATIC HYDROLYSIS OF BIOMASS WHICH HAS A HIGH CONTENT OF DRY MATERIAL
EP1690980A1 (en) * 2005-02-11 2006-08-16 Agrotechnology and Food Innovations B.V. Process and apparatus for conversion of biomass
US7910338B2 (en) * 2005-04-12 2011-03-22 E. I. Du Pont De Nemours And Company Integration of alternative feedstreams for biomass treatment and utilization
US20070029252A1 (en) * 2005-04-12 2007-02-08 Dunson James B Jr System and process for biomass treatment
US7585104B2 (en) * 2005-09-12 2009-09-08 Uop Llc Rotary processor
US7815741B2 (en) * 2006-11-03 2010-10-19 Olson David A Reactor pump for catalyzed hydrolytic splitting of cellulose
US7815876B2 (en) 2006-11-03 2010-10-19 Olson David A Reactor pump for catalyzed hydrolytic splitting of cellulose
PL3401410T3 (pl) 2010-06-26 2021-11-29 Virdia, Llc Sposoby wytwarzania mieszanek cukrów
IL206678A0 (en) 2010-06-28 2010-12-30 Hcl Cleantech Ltd A method for the production of fermentable sugars
IL207329A0 (en) 2010-08-01 2010-12-30 Robert Jansen A method for refining a recycle extractant and for processing a lignocellulosic material and for the production of a carbohydrate composition
IL207945A0 (en) 2010-09-02 2010-12-30 Robert Jansen Method for the production of carbohydrates
WO2012061085A2 (en) * 2010-10-24 2012-05-10 Hcl Cleantech Ltd Hydrolysis systems and methods
EP2694594A4 (en) 2011-04-07 2015-11-11 Virdia Ltd METHODS AND PRODUCTS FOR LIGNOCELLULOSE CONVERSION
US9617608B2 (en) 2011-10-10 2017-04-11 Virdia, Inc. Sugar compositions
US9493851B2 (en) 2012-05-03 2016-11-15 Virdia, Inc. Methods for treating lignocellulosic materials
GB2523234B (en) 2012-05-03 2016-03-30 Virdia Ltd A method of fractionating a liquid sample
DE102012020166A1 (de) * 2012-10-13 2014-04-30 Green Sugar Gmbh Produktinnovationen Aus Biomasse Verfahren zur Hydrolyse von pelletierfähigen Biomassen mittels Halogenwasserstoffsäuren
WO2016082816A1 (de) * 2014-11-26 2016-06-02 Green Sugar Gmbh Produktinnovationen Aus Biomasse Verfahren zur säureführung in hydrolyseanlagen zur sauren hydrolyse von pflanzlichen biomassen mittels konzentrierter salzsäure
WO2016099273A1 (en) 2014-12-18 2016-06-23 Avantium Knowledge Centre B.V. Process for the preparation of a saccharide-containing solution from a torrefied cellulosic biomass
EP3242871B1 (en) 2015-01-07 2019-11-06 Virdia, Inc. Methods for extracting and converting hemicellulose sugars
BR112017025322A8 (pt) 2015-05-27 2022-08-23 Virdia Inc Processos integrados para recuperação de hidrolisato celulósico após hidrólise de polpa de celulose
GB2548386A (en) 2016-03-17 2017-09-20 Alkymar As Mixing and processing apparatus
WO2018041975A1 (en) 2016-08-31 2018-03-08 Avantium Knowledge Centre B.V. Hydrolysis and hydrolysis reactor
KR20190096357A (ko) 2016-12-13 2019-08-19 아반티움 놀리지 센터 비.브이. 오염된 염산 조성물 정제 공정
FR3075202B1 (fr) * 2017-12-20 2020-08-28 Ifp Energies Now Procede de traitement de biomasse ligno-cellulosique

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1670727A (en) * 1920-02-05 1928-05-22 Kocher Rudolph Alfred Process and apparatus for converting carbohydrates
DE524156C (de) * 1929-11-05 1931-05-02 Siller & Rodenkirchen G M B H Rotierender Autoklav zur Gewinnung von Glukose aus Holzstoff
US1990097A (en) * 1929-12-09 1935-02-05 Scholler Heinrich Process of converting cellulose and the like into sugar with dilute acids under pressure
US2086701A (en) * 1933-08-30 1937-07-13 Dreyfus Henry Hydrolysis of cellulose
FR798559A (fr) * 1934-04-23 1936-05-20 Procédé et appareil pour l'hydrolyse des celluloses et ligno-celluloses
US2239095A (en) * 1939-06-21 1941-04-22 Eastman Kodak Co Saccharification of wood
US2375499A (en) * 1943-08-05 1945-05-08 Dow Chemical Co Rotary lime treating apparatus
FR904371A (fr) * 1943-12-17 1945-11-05 Procédé perfectionné d'hydrolyse des déchets de bois ou végétaux et appareil digesteur pour l'application du procédé
US2538457A (en) * 1946-11-02 1951-01-16 Monie S Hudson Treating wood
GB681345A (en) * 1948-07-27 1952-10-22 Glucol Soc Du Improvements in or relating to a method for the hydrolysis of cellulose materials
US2778751A (en) * 1952-03-21 1957-01-22 Bergin Ag Deutsche Hydrolysis of wood with concentrated hydrochloric acid
US2969277A (en) * 1956-05-17 1961-01-24 Dano Ingeniorforretning Og Mas Apparatus for the fermentation of solid organic materials
US2951775A (en) * 1956-12-12 1960-09-06 Udic Sa Selective saccharification of cellulosic materials
US2948593A (en) * 1957-04-15 1960-08-09 Larson John David Digester for converting inorganic material into assimilable plant food
US3212933A (en) * 1963-04-12 1965-10-19 Georgia Pacific Corp Hydrolysis of lignocellulose materials with solvent extraction of the hydrolysate
US3523911A (en) * 1969-02-26 1970-08-11 Harald F Funk Method of separating components of cellulosic material
US3676074A (en) * 1969-06-30 1972-07-11 Yamato Setubi Koji Kk Apparatus for treating organic waste
US4018567A (en) * 1973-05-14 1977-04-19 James P. La Point, Jr. Apparatus for separating the constituents of lead-acid storage batteries

Also Published As

Publication number Publication date
EG13177A (en) 1980-12-31
IT1093515B (it) 1985-07-19
ATA220578A (de) 1980-07-15
SE7803578L (sv) 1978-10-02
NO145694B (no) 1982-02-01
FR2395314B1 (US07943777-20110517-C00090.png) 1980-04-11
BE865584A (fr) 1978-10-02
MX5047E (es) 1983-03-02
ES468437A1 (es) 1979-01-01
CU21104A (es) 1981-01-10
FI780956A (fi) 1978-10-02
IT7821847A0 (it) 1978-03-31
US4257818A (en) 1981-03-24
OA05924A (fr) 1981-06-30
FI63965C (fi) 1983-09-12
PL205735A1 (pl) 1979-01-15
AT361418B (de) 1981-03-10
NZ186826A (en) 1979-06-19
DE2814067A1 (de) 1978-10-12
NO781128L (no) 1978-10-03
US4304608A (en) 1981-12-08
DK144578A (da) 1978-10-02
NO145694C (no) 1982-05-12
AU3466478A (en) 1979-10-04
BR7802044A (pt) 1978-12-19
JPS53124632A (en) 1978-10-31
AU518576B2 (en) 1981-10-08
FI63965B (fi) 1983-05-31
SE439648B (sv) 1985-06-24
CH609092A5 (US07943777-20110517-C00090.png) 1979-02-15
NL7803360A (nl) 1978-10-03
FR2395314A1 (fr) 1979-01-19
GB1562682A (en) 1980-03-12
US4199371A (en) 1980-04-22

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Legal Events

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